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isatoic anhydride synthesis
Yes, another error. Phthalimide reacts to form the alkaline salt, then hit with bleach and then HCl. ...
9-9-2014 at 13:37
by: Templar
isatoic anhydride synthesis
Corrected, thanks.

Ref attached recommends use of acetic acid for recrystallization. Might be un ...
8-9-2014 at 21:58
by: Templar
n-acetyl o-toluidine oxidation
Ah I see... I'm surprised, I didnt think permanganate would work without acidic/basic conditions. Th ...
8-9-2014 at 13:31
by: Templar
isatoic anhydride and acetylacetone
isatoic anhydride synthesis.
http://www.sciencemadness.org/talk/viewthread.php?tid=33344
8-9-2014 at 06:27
by: Templar
isatoic anhydride synthesis
Most of these reactions I have not had the time to research the mechanics for. Some do not have mech ...
8-9-2014 at 06:24
by: Templar
methyl iodide NZ
Picture of a bottle attached.

[file]33621[/file]

NOTE: shipments will be sent via a DG courie ...
8-9-2014 at 05:09
by: Templar
isatoic anhydride synthesis
Isatoic Anhydride Synthesis

-------------------------

Introduction:

Isatoic anhydride is a ...
8-9-2014 at 04:54
by: Templar
n-acetyl o-toluidine oxidation
Hello everyone,

I have been investigating oxidation of n acetyl ortho toluidine to n acetyl anthr ...
7-9-2014 at 04:06
by: Templar
Water Aspirator
get a cheap single or dual rotary vane vacuum pump from china used for refrigeration!

They are su ...
7-9-2014 at 01:42
by: Templar
Preparation of Acetyl Chloride
guys what was wrong with using cyanuric chloride with ethanoic acid as per the attached patent?
2-9-2014 at 16:38
by: Templar
Pd/C
Hello,

I was wanting to know if there are any definitive tests to verify if a 5% reduced Pd on ca ...
28-8-2014 at 18:17
by: Templar
Cleaning Sulfuric Acid- The Easy Way!
I have never had problems violating this "dont pour water in conc acids or bases" rule

Touch and ...
28-8-2014 at 10:04
by: Templar
selling sodium metal
You making this yourself or importing it? very jealous

half pound a lot on its own? pfft sodium w ...
28-8-2014 at 09:41
by: Templar
methyl iodide NZ
The war on drugs is a total failure, and an excellent excuse to strip citizens of the liberty to do ...
26-8-2014 at 06:13
by: Templar
methyl iodide NZ
Yes, 5 L is an accident waiting to happen. Just like the 20L of everything else I have in storage, t ...
25-8-2014 at 18:35
by: Templar
methyl iodide NZ
Yeah it is useful. But 5 litres is a lot.

WHere I am, they require EUD's for even ACETONE now

...
24-8-2014 at 19:50
by: Templar
methyl iodide NZ
Recycling. For what reasons will this not work?
24-8-2014 at 07:59
by: Templar
methyl iodide NZ
Hello everyone,

I have some 5L of sealed bottles of methyl iodide I was given from a closing down ...
23-8-2014 at 19:54
by: Templar
eBay seller deschem
Chinese glassware is very good for the price.

Find a reputable ebay seller, and buy off them. You ...
23-8-2014 at 19:50
by: Templar
New possible efficient and clean electrolytic hydrogenation/reduction of aromatic compounds
Shut down

Lol

Just post some refs, make a writeup, etc

Jus do it mayn
20-8-2014 at 16:11
by: Templar
Testing Strength of Organic Reducers
This is difficult... its not just the reducing potention of the reducing agent (boro,LAH, Al/Hg, Na/ ...
20-8-2014 at 02:58
by: Templar
isatoic anhydride and acetylacetone
Ah.. and doesnt require a lot of Na metal...

I thought this method was only viable for moderate c ...
19-8-2014 at 05:16
by: Templar
Experimental: Alternative to Al/Hg - the Al/Cu
Yes the nitrostyrene was well purified, light orange xtals.

A more cimprehensive writeup would li ...
18-8-2014 at 14:23
by: Templar
Experimental: Alternative to Al/Hg - the Al/Cu
Hmm I will try the aluminium strips then. It seems very strange though that Al turns would not work. ...
18-8-2014 at 03:14
by: Templar
Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=342147&tid=30297&author=pepsimax]The reaction definitely does work, with beta nitros ...
18-8-2014 at 00:31
by: Templar
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