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Destructive distillation of polypropylene
The resulting oil appears to be completely different to the list of products given. Almost no pentan ...
26-8-2019 at 01:58
by: 12thealchemist
Destructive distillation of polypropylene
In my case, they're polypropylene:

[file]76829[/file]

I've done destructive distillation of p ...
26-8-2019 at 01:07
by: 12thealchemist
Destructive distillation of polypropylene
Some years ago I collected together a large quantity of waste polypropylene (PP) plastic in the form ...
25-8-2019 at 06:38
by: 12thealchemist
Is there any way to make 3 amino phenol from salicamide?
The only issue is how to decarboxylate acetylsalicylic acid without cleaving the ester linkage - in ...
18-4-2019 at 01:42
by: 12thealchemist
Is there any way to make 3 amino phenol from salicamide?
The Hoffman rearrangement or degradation would work to convert salicamide into 2-aminophenol.

3-a ...
17-4-2019 at 04:44
by: 12thealchemist
LiAlH4 via electrolysis
I'm not sure at what temperature lithium metal will react with hydrogen, but I don't think it's at a ...
10-4-2019 at 12:26
by: 12thealchemist
T-butanol from Citric acid?
[rquote=608056&tid=147577&author=fusso]@12ta some of the C in backbone is missing[/rquote]
...
10-4-2019 at 00:34
by: 12thealchemist
T-butanol from Citric acid?
As I understand it, the proposed route looks something like this:

[file]74855[/file]

I have ...
9-4-2019 at 01:07
by: 12thealchemist
T-butanol from Citric acid?
What reducing agent do you plan to use to reduce a carboxylic acid to an alkane, or alcohol then alk ...
8-4-2019 at 12:24
by: 12thealchemist
Silver nanoparticles
[rquote=607275&tid=147281&author=woelen]If you used sterling silver (which normally is 0.925 ...
3-4-2019 at 09:29
by: 12thealchemist
Allotropes of Sulpher
I've also recrystallised sulphur from toluene to excellent effect - it's fairly soluble in boiling t ...
3-4-2019 at 08:44
by: 12thealchemist
chemical waste books
I have the offerings of popular YouTube channels?
2-4-2019 at 11:53
by: 12thealchemist
Silver nanoparticles
My Master's research has been focused mainly on univalent gallium chemistry, but as a byproduct of f ...
2-4-2019 at 09:05
by: 12thealchemist
Allotropes of Sulpher
There are many allotropes of sulphur. Rhombic and monoclinic are the most common. Rhombic sulphur is ...
2-4-2019 at 08:39
by: 12thealchemist
Make Potassium (from versuchschemie.de)
My understanding is that typically if the reaction has been successful, visible balls of potassium f ...
31-3-2019 at 13:06
by: 12thealchemist
Carbon disulfide synthesis (alternative routes)
I went through Reaxys a few months ago and compiled this:

[file]74726[/file]

I stripped out a ...
31-3-2019 at 09:00
by: 12thealchemist
Make Potassium (from versuchschemie.de)
[rquote=606983&tid=14970&author=S.C. Wack]Is there a superior high yielding process if the g ...
31-3-2019 at 08:55
by: 12thealchemist
Make Potassium (from versuchschemie.de)
The only issue with tetraglyme and higher glymes is increased cost. Triglyme is the smallest that ha ...
31-3-2019 at 06:29
by: 12thealchemist
Preparation of ionic phosphide from red P
Is it possible to use some sort of inert heat dissipant, like sand for Zn3P2 or calcium fluoride (fl ...
15-3-2019 at 05:44
by: 12thealchemist
Predicting the color of an organic compound
This might be of help: https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/spectrpy/uv-vis/uvsp ...
12-3-2019 at 09:32
by: 12thealchemist
Disodium 1,2-ethanediolate Production
[rquote=605060&tid=146345&author=fusso]Could toluene azeotrope with the water and boil at lo ...
12-3-2019 at 01:18
by: 12thealchemist
Does anyone know much about how the mg catalyzed alkali reduction purification with dioxane works?
I suspect that sterics are a factor as well as chelating. Assuming you need chelating properties, eu ...
7-3-2019 at 01:05
by: 12thealchemist
Make Potassium (from versuchschemie.de)
I don't see why it wouldn't work; I'd have tried it myself but I don't have the capabilities at the ...
7-3-2019 at 01:03
by: 12thealchemist
How to concentrate azeotropic HNO3?
[rquote=604619&tid=146120&author=fusso]Will H2SO4 dehydrate it into NO2 & O2?[/rquote]
...
6-3-2019 at 07:38
by: 12thealchemist
Make Potassium (from versuchschemie.de)
You are correct, the catalyst should be added once the initial gas evolution ceases. This will be wh ...
5-3-2019 at 01:30
by: 12thealchemist
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