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Preparation of Methyl Iodide Using HCl Gas
Actually KiWiki, theres a nice write up in the Prepublications section on the preparation of MeI usi ... |
19-12-2017 at 08:40
by: DJF90 |
Diethylamine Hydrochloride Synthesis
Apologies, I clearly misread the target wrong.
In any case, you might be better off running the ... |
17-12-2017 at 16:07
by: DJF90 |
Diethylamine Hydrochloride Synthesis
[rquote=490416&tid=24131&author=JJay]I'm doing a simple distillation right now, but I don't ... |
17-12-2017 at 15:23
by: DJF90 |
Large Li-ion battery packs, compact jump starters and truth in advertising?
The one I have doesn't require any "warm-up period" - you hook it up and turn the ignition. It has n ... |
16-12-2017 at 09:05
by: DJF90 |
Large Li-ion battery packs, compact jump starters and truth in advertising?
I have one of these: https://www.amazon.co.uk/gp/aw/d/B01KZFUW98?psc=1&ref=yo_pop_mb_pd
I bou ... |
15-12-2017 at 15:12
by: DJF90 |
Addition of HCl to Propenoic acid
[rquote=499905&tid=78823&author=LearnedAmateur]I know it's not the same mechanism as what is ... |
9-12-2017 at 14:44
by: DJF90 |
Preparation of Diethyl Sulfate
Magpie, the reference for the paper is [i]JACS[/i] [b]1924[/b] [i]46[/i] (4) pp. 999 to 1001. I've a ... |
8-12-2017 at 03:17
by: DJF90 |
Preparation of Diethyl Sulfate
Nice work Magpie. If you have the paper perhaps you could attach it to your post for convenience (al ... |
7-12-2017 at 11:40
by: DJF90 |
can anyone describe the smell of hbr or hydrobromic acid?
I find it smells quite fruity actually, but you'd want to avoid breathing it if possible |
5-12-2017 at 14:23
by: DJF90 |
Cobalt compounds
[rquote=499490&tid=78561&author=Tetra][rquote=499435&tid=78561&author=DraconicAcid][ ... |
5-12-2017 at 09:11
by: DJF90 |
The Trouble with Boron
Melting means less surface area which means incomplete dehydration to boric oxide. There is a prepar ... |
4-12-2017 at 11:19
by: DJF90 |
Preparation of Thionyl Chloride
[rquote=499360&tid=78645&author=AJKOER]
Per Watts, a curious lesser known path to SOCl2 cla ... |
4-12-2017 at 10:10
by: DJF90 |
Making an induction heater for fastener removal?
I feel your pain, Bert. With the information you've provided, I don't think you'll be able to acheiv ... |
4-12-2017 at 03:03
by: DJF90 |
Preparation of methyl tosylate, safe methylating agent
http://orgsyn.org/demo.aspx?prep=cv1p0145
See note 4. |
2-12-2017 at 13:54
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
[rquote=498651&tid=78225&author=clearly_not_atara]I know that esters sometimes react with am ... |
26-11-2017 at 07:58
by: DJF90 |
Preparation of Quinoline
I can vouch for the ZnCl2 complex method, and it gives a clean product by 1H-NMR. Instructions can b ... |
24-11-2017 at 10:23
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
So you're on a forum for amateur science asking for advice/solutions to your commercial problems? Do ... |
24-11-2017 at 05:22
by: DJF90 |
Preparation of S2Cl2
[rquote=497697&tid=78027&author=aga][rquote=497692&tid=78027&author=clearly_not_atar ... |
16-11-2017 at 12:14
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
[rquote=497566&tid=78225&author=Sigmatropic]What I'm saying is that, based on pKa values, on ... |
15-11-2017 at 09:31
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
[rquote=497493&tid=78225&author=hexabio] NaH is a pretty brutal reagent just for depronating ... |
14-11-2017 at 10:47
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
[rquote=497430&tid=78225&author=hexabio] I have never seen NaH used in BOC protections, can ... |
14-11-2017 at 09:24
by: DJF90 |
Protecting weak secondary amines - driving me crazy!
What you're referring to is not a secondary amine, but an indole. Two quite separate things.
I'd ... |
13-11-2017 at 12:36
by: DJF90 |
[UK] TLC plates needed
I think you will have a hard time sourcing any that are 60 cm long, considering the standard "full-s ... |
6-11-2017 at 12:01
by: DJF90 |
Preparation of S2Cl2
Nice work Magpie. Good to see you're still busy in the lab
What was the rational for using conc su ... |
4-11-2017 at 15:25
by: DJF90 |
Vigreux and reflux column combo. Custom piece
I can't think of any possible use for this. From my perspective, it is nonsensical and certainly can ... |
4-11-2017 at 09:30
by: DJF90 |
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