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A process to produce silvery thallium ampoules
Many of the low-melting metals require customized equipment to give satisfactory purification result ...
15-10-2018 at 17:49
by: Dan Vizine
The trials & tribulations of Thorium production
Obviously, with Th in a powdered form, inhalation danger is a primary issue.

An interesting calcu ...
3-10-2018 at 19:08
by: Dan Vizine
barium hydroxide [Ba(OH)2]
Hi Magpie,

Are you in the US?

I have maybe 75 or 100 g of BaO. You can have whatever you need ...
18-9-2018 at 07:14
by: Dan Vizine
benzyl chloride
You're correct, Loptr. The bp of the bromo analog is almost 50 C higher.

The more labile bromines ...
8-9-2018 at 09:00
by: Dan Vizine
Brown liquid in KOH drain cleaner
Funkyman99

OK, I realize that we don't want to stifle amateur experimentalism, but is that what t ...
7-9-2018 at 08:09
by: Dan Vizine
benzyl chloride
Hi Loptr,

Well, CMCS is certainly far safer than HCl/HCOH mixtures. Thanks for the reference.

...
7-9-2018 at 07:25
by: Dan Vizine
benzyl chloride
Loptr,

The chemical is bis(chloromethyl) ether.

It is volatile, dangerous in almost any amount ...
6-9-2018 at 12:59
by: Dan Vizine
benzyl chloride
I've done this photochemically catalyzed chlorination reaction numerous times with m-xylene. Toluene ...
6-9-2018 at 12:35
by: Dan Vizine
Doable synthesis of F2 in amateur setting?
[rquote=532029&tid=80282&author=metalresearcher][rquote=531874&tid=80282&author=symb ...
28-8-2018 at 13:54
by: Dan Vizine
Nickel II Nitrate
When you think of drying as a mass transfer issue, you realize that almost nothing is faster than az ...
27-8-2018 at 13:15
by: Dan Vizine
Nickel II Nitrate
What year was the nickel? Only pre-1982 Canadian nickels were nickel

According to someone...
"Ca ...
27-8-2018 at 11:25
by: Dan Vizine
Calculating the energy of thermite
Vertox,

I know this reference has been posted earlier, but you probably haven't seen it. This exp ...
27-8-2018 at 11:15
by: Dan Vizine
Calculating the energy of thermite
[rquote=531339&tid=88884&author=MrHomeScientist]Also you should take into account the state ...
24-8-2018 at 11:51
by: Dan Vizine
can a diamond dissolve in acid ?
[rquote=530969&tid=88900&author=Keras][rquote=530964&tid=88900&author=zhonglanindust ...
24-8-2018 at 09:31
by: Dan Vizine
Calculating the energy of thermite
It isn't, really. It just looks imposing because of the symbols.


The balanced equation for the ...
24-8-2018 at 08:55
by: Dan Vizine
Calculating the energy of thermite
I needed to prepare a document that concerned the redox reaction of Fe2O3 with sodium. Here's an exc ...
22-8-2018 at 13:01
by: Dan Vizine
The trouble with neodymium...
[rquote=513804&tid=14145&author=Lab Rat]

And that's basically my question. I've literall ...
19-8-2018 at 14:55
by: Dan Vizine
Handling toxic gasses in glassware
If you're using glassware with well-greased ground glass joints and you have a reliable connection t ...
10-8-2018 at 10:43
by: Dan Vizine
The trials & tribulations of Thorium production
[rquote=527209&tid=29927&author=neptunium]I know this is a little off topic but still..I hav ...
8-8-2018 at 06:22
by: Dan Vizine
Doable synthesis of F2 in amateur setting?
I looked at a number of routes to F2. I settled on the attached as this method relies on easy-to-obt ...
7-8-2018 at 15:20
by: Dan Vizine
The trials & tribulations of Thorium production
[rquote=527322&tid=29927&author=MJ101]@Dan Vizine: I read this thread from stem to stern. Aw ...
7-8-2018 at 15:05
by: Dan Vizine
Problems with Lithium Batteries
https://www.ebay.com/itm/10g-High-Purity-99-9-Pure-Lithium-Li-Metal-Element-Sealed-Argon/16268123174 ...
30-7-2018 at 09:31
by: Dan Vizine
Bromine Trifluoride small scale production
" a small explosive charge to forcefully direct high-pressure jets of highly corrosive material in a ...
30-7-2018 at 09:20
by: Dan Vizine
Thorium metal in coherent form
I thought Rd is a very hard metal? Why do you think Os was challenging?

Anyway, it's IMPERATIVE ...
9-9-2017 at 18:17
by: Dan Vizine
Thorium metal in coherent form
[rquote=491035&tid=75775&author=Fleaker]
Dan, I have some experience with powder metallurgy ...
8-9-2017 at 16:39
by: Dan Vizine
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