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Ceramic chemistry ware.
Sedit, Can you make large pieces? maybe 1-2 cubic feet? I'd love to have what would be basically ...
13-1-2011 at 15:46
by: Eclectic
SO2 Production
I was thinking of the same basic arrangement as at the top of the post as primary sulfur evaporator ...
13-1-2011 at 15:34
by: Eclectic
flask insulation?
Standard fiberglass insulation with the facing material removed works.
The aluminum foil faced mate ...
12-1-2011 at 20:21
by: Eclectic
Make Potassium (from versuchschemie.de)
Maybe useful solvents in this application:

http://www.novolyte.com/documents/brochures/glymes-and ...
12-1-2011 at 20:17
by: Eclectic
Make Potassium (from versuchschemie.de)
!!DANGER!!, DANGER, Will Robinson!

[rquote=58293&tid=5112&author=Axt]The Explosion of Chl ...
11-1-2011 at 06:35
by: Eclectic
Synthesis of longer chain tertiary alcohols
OK. Has anyone here ever heard anything about Barbier-Gringnard reactions? Alkyl halide, zinc dus ...
3-1-2011 at 20:01
by: Eclectic
Make Potassium (from versuchschemie.de)
I got the Ritchie Compass filling fluid URLed in my last post above, and it is in fact Isopar L, and ...
31-12-2010 at 12:35
by: Eclectic
Make Potassium (from versuchschemie.de)
1-ethylcyclohexanol from ethyl bromide and cyclohexanone might be interesting to try.
29-12-2010 at 17:58
by: Eclectic
Make Potassium (from versuchschemie.de)
Exxon Isopar L seems to be fairly close to Shellsol D70:

http://exxonmobilchemical.ides.com/en-US ...
28-12-2010 at 17:04
by: Eclectic
Make Potassium (from versuchschemie.de)
Baby oil is fairly high viscosity? It looks like "white mineral oil", ISO VG 10-15, viscosity 70 wo ...
26-12-2010 at 10:09
by: Eclectic
Make Potassium (from versuchschemie.de)
Even better!
25-12-2010 at 18:17
by: Eclectic
Make Potassium (from versuchschemie.de)
Take a look at AW 32 hydraulic oil, it's available as high purity food grade also.
25-12-2010 at 13:45
by: Eclectic
catching H2S
How about some kind of burner, followed by SO2 scrubber? It would also get rid of acetylene,CS2, an ...
24-12-2010 at 08:23
by: Eclectic
Make Potassium (from versuchschemie.de)
K-1 water white kerosine made for unvented heaters and lamps should be fully hydrogenated. Aromatic ...
23-12-2010 at 10:04
by: Eclectic
Make Potassium (from versuchschemie.de)
I still think the commonly available glycol ethers may work. (Brake Fluid)
Has anyone tried Barb ...
22-12-2010 at 11:20
by: Eclectic
Calcium metal by chemical means
It's lump CaH, kinda looks like grey chalk, made by Metal Hydrides, inc from late WWII through Viet ...
16-12-2010 at 12:08
by: Eclectic
Calcium metal by chemical means
The hydrogen generators from Fair Radio Sales each contain about 2kg of CaH.
16-12-2010 at 11:09
by: Eclectic
Make Potassium (from versuchschemie.de)
K-1 kerosene or low sulfur diesel fuel with the volatiles fractionated off would be the most availab ...
16-12-2010 at 10:09
by: Eclectic
Calcium metal by chemical means
Does metallic calcium from calcium hydride count? :P

(Surplus military hydrogen generators from ...
16-12-2010 at 09:57
by: Eclectic
Make Potassium (from versuchschemie.de)
CH3CH2CH2CH2OCH2CH2OH

http://en.wikipedia.org/wiki/2-Butoxyethanol


8-12-2010 at 17:29
by: Eclectic
Make Potassium (from versuchschemie.de)
Did we decide that k-1 kerosene with the volatiles distilled off and butoxyethanol as the alcohol we ...
8-12-2010 at 06:58
by: Eclectic
Preparation of elemental phosphorus
You may be getting phosphorus chlorides and oxychlorides using NaCl as flux. Heating P2O5 and NaCl ...
29-10-2010 at 13:57
by: Eclectic
Trioxane depolymerization
Just saying, for first step isolation and purification from fuel tablets, no need to powder, just us ...
28-10-2010 at 21:12
by: Eclectic
Preparation of elemental phosphorus
The advantage of phosphoric acid and activated carbon heated by microwaves and contained in borosili ...
26-10-2010 at 04:58
by: Eclectic
Trioxane depolymerization
Easy way to purify trioxane is sublimation....I've done 50lbs in 3, 5 gallon plastic buckets with li ...
26-10-2010 at 04:42
by: Eclectic
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