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Gringard Question
I've always seen gringard reactions done with using bromine as the halogen with the magnesium. Can t ...
22-11-2016 at 19:17
by: Meltonium
Separation of Xylenes using Formic Acid Azeotrope
[rquote=463552&tid=69528&author=Maroboduus]So any idea what that first fraction was?
[Edit ...
21-11-2016 at 09:38
by: Meltonium
Makeshift Pt Catalyst?
So... in other words it would be unusable for a catalyst? I just have some lying around and was look ...
20-11-2016 at 18:05
by: Meltonium
Free Radical Alcohol?
The last time I titrated the peroxide it came out to be about 17% give or take. However, that was a ...
20-11-2016 at 14:40
by: Meltonium
Free Radical Alcohol?
I attempted an experiment to create hexanol from n-hexane and hydrogen peroxide. I became curious af ...
20-11-2016 at 14:18
by: Meltonium
Makeshift Pt Catalyst?
[rquote=467070&tid=70915&author=MeshPL]
But again, are you sure this is a coating of pure p ...
20-11-2016 at 12:00
by: Meltonium
Makeshift Pt Catalyst?
Opening up an old computer hard drive will reveal several shiny discs. These discs are plated in a s ...
20-11-2016 at 06:02
by: Meltonium
Free Radical Chlorination of p-Xylene
First, I was going to substitute one of the bromines with propionic acid in the secondary position, ...
12-11-2016 at 05:20
by: Meltonium
Free Radical Chlorination of p-Xylene
[rquote=466527&tid=70779&author=Metacelsus] If you just need a xylyl halide (and don't care ...
11-11-2016 at 18:20
by: Meltonium
Free Radical Chlorination of p-Xylene
My plan is to chlorinate the methyl groups of the p-xylene using chlorine gas and uv light. Could th ...
11-11-2016 at 12:53
by: Meltonium
2-chloropropionic acid
Quick question: If I preform a free radical chlorination on propionic acid, will the chlorine radica ...
9-11-2016 at 12:51
by: Meltonium
Trying to synthesize 1-iodobutane
You just need a proton donator. Strong acids are usually the easiest to use.
3-11-2016 at 06:34
by: Meltonium
Production of Potassium Chlorate
Alternatively, you can make KClO3 by boiling bleach down until the NaCl starts to crash out, isolate ...
3-11-2016 at 05:54
by: Meltonium
Fluoroantimonic + Hydrogen Peroxide Reaction?
Two words: Bad things.

Fluoroantimonic acid is much to acidic to study intensely, so I can say wi ...
2-11-2016 at 17:47
by: Meltonium
M-toluic Acid Chlorination
I've wanted to make DEET for a while now to explore the chemistry of it; I know it's not cost effect ...
2-11-2016 at 11:57
by: Meltonium
Will MeOH in DCM retain H2O?
[rquote=465637&tid=70577&author=Acuyo]

So is MgSO4 normally ok for drying DCM?[/rquote]
...
1-11-2016 at 07:06
by: Meltonium
2-Chloropropane Strange Distillation
The procedure I followed was my own using an excess of isopropanol, 165mL of 12M HCl, and 20mL of a ...
1-11-2016 at 03:53
by: Meltonium
2-Chloropropane Strange Distillation
Today, I attempted to make 2-chloropropane from isopropanol and concentrated hydrochloric acid with ...
31-10-2016 at 19:57
by: Meltonium
Increasing oxidation rate by bubbling air into water - pressurize system?
For many gasses, if you increase the pressure and drop the temperature, they stay in solution better ...
29-10-2016 at 04:15
by: Meltonium
Platinum Catalyst Mount
Recently I obtained some platinum wire to use as a catalyst. My planned reaction is making NO2 from ...
28-10-2016 at 08:24
by: Meltonium
Transition Metal Bisulfates
Do you have any specific transition metal bisulfate you need? Also what are you using it to catalyze ...
28-10-2016 at 08:17
by: Meltonium
Zinc Chloride Tetrahydrate Decomp.
So finally it's gotten down from 400ml to about 120 mL. As the concentration increased, a straw yell ...
28-10-2016 at 04:21
by: Meltonium
DCM Reactions
Is it possible to use DCM to add a methyl chloride group onto a molecule and continue the process to ...
24-10-2016 at 11:55
by: Meltonium
Zinc Chloride Tetrahydrate Decomp.
I have made a solution of ZnCl2 from dissolving zinc metal in hydrochloric acid. While researching a ...
22-10-2016 at 18:34
by: Meltonium
Zinc Chloride Strange Floaters
[rquote=464637&tid=70246&author=Metacelsus]How did you electrolyze your ZnO? I assume you di ...
22-10-2016 at 09:32
by: Meltonium
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