| Search |
| [Next Page] |
Successful 2 in 1 synthesis: Optimized home-synthesis of SOCl2. Phase II.
To my surprise, the colour in flask B from before had changed from a dark purple/brown to a very pal ... |
16-12-2021 at 14:50
by: Monoamine |
Successful 2 in 1 synthesis: Optimized home-synthesis of SOCl2. Phase I.
[b]It worked![/b] 
The previous attempt to make SOCl[sub]2[/sub] didn’t give a pure product, ... |
16-12-2021 at 14:43
by: Monoamine |
Nitric Acid and Silver Nitrate
Guess what happens when you spill silver nitrate on your hand?
This:
[file]91469[/file]
(A ... |
16-12-2021 at 03:13
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668737&tid=158187&author=Lionel Spanner]]
It mostly seems to be used for making chl ... |
16-12-2021 at 01:46
by: Monoamine |
Thionyl chloride synthesis (SOCl2) from sulfur trioxide (SO3) and sulfur dichloride (SCl2). Phase II.
Next, we stoppered flask B and set it up for distillation to try and fractionally distill off the SC ... |
16-12-2021 at 01:38
by: Monoamine |
Thionyl chloride synthesis (SOCl2) from sulfur trioxide (SO3) and sulfur dichloride (SCl2). Phase I.
To make SOCl[sub]2[/sub], we followed the synthesis of Georg Brauer on page 382 in “handbook of pr ... |
16-12-2021 at 01:30
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
Thank you clearly_not_atara for the tips about reactions of SCl2 with alcohols. Maybe a future proje ... |
15-12-2021 at 23:18
by: Monoamine |
Discussion: Sulfur dichloride
[file]91445[/file]
SCl[sub]2[/sub] slowly decomposes back into S[sub]2[/sub]Cl[sub]2[/sub] and Cl[ ... |
15-12-2021 at 10:18
by: Monoamine |
Synthesis of sulfur dichloride (SCl2)
This synthesis is adapted from a youtube video by Extraction&Ire (found [url=https://www.youtube ... |
15-12-2021 at 10:12
by: Monoamine |
Synthesis of sulfur trioxide (SO3)
This procedure is adapted from the procedure described by user “Garage Chemist”. His original no ... |
14-12-2021 at 13:10
by: Monoamine |
Project: Making thionyl chloride from easy-to-get precursors
[color=Red]Warning: SO[sub]2[/sub], HCl and Cl[sub]2[/sub] are toxic gasses. SO[sub]3[/sub], SCl[sub ... |
14-12-2021 at 12:28
by: Monoamine |
WARNING: Explosive reaction between pool chlorine chemicals
Thank you for the warning and self experiment. So I guess the "safe" way to make Cl[sub]2[/sub] is j ... |
6-12-2021 at 23:41
by: Monoamine |
Converting a separation funnel to a pressure equalizing addition funnel
Putting together bits of hoses and doing some very amateurish glass blowing from some glass drinking ... |
3-12-2021 at 13:45
by: Monoamine |
monoamide of terephtalic acid
To be fair though, I'm also not sure about the last step (purifying by fractional distillation, sinc ... |
29-11-2021 at 13:04
by: Monoamine |
Theoretical attempt
Ok here is how I might try it. No clue whether it would properly work though... Still, it's fun to t ... |
29-11-2021 at 12:44
by: Monoamine |
Separation of toluene and isobutanol
Isn't isobutanol much more water soluble than toluene? In that case couldn't you extract the isobuta ... |
28-11-2021 at 21:41
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
Thanks for the tip about glass cracking when it's tightened too much. Haven't had it happen yet, but ... |
28-11-2021 at 21:35
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
|
28-11-2021 at 09:42
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
[file]91201[/file] |
28-11-2021 at 09:40
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
|
28-11-2021 at 09:39
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
[file]91195[/file] |
28-11-2021 at 09:37
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
[file]91193[/file]
[Edited on 28-11-2021 by Monoamine] |
28-11-2021 at 09:36
by: Monoamine |
Sulfur trioxide (SO3) misshap (and fix)
[b]It was a cold and stormy day so I decided to go outside and make some oleum...[/b]
Scroll down ... |
28-11-2021 at 09:34
by: Monoamine |
Mercury-free Clemmensen reduction?
[rquote=462500&tid=69602&author=Melgar]This PDF seems to claim that mercury isn't necessary ... |
13-10-2021 at 18:14
by: Monoamine |
Stereochemistry of the ibogaloid catharanthine
Ah got it. Thanks. I guess what confused me is that in clearsynth picture the methyl bridge from the ... |
13-10-2021 at 15:28
by: Monoamine |
| [Next Page] |
