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uv for tlc
black lights are usually low wattage and won't illuminate spots that well. Also it's good to have a ...
22-4-2016 at 08:50
by: chemrox
Reagents for sale
oxalyl chloride
phosphorous oxychloride
22-4-2016 at 08:30
by: chemrox
Help with debenzylation of N-Benzyl
Li/NH4
21-4-2016 at 11:56
by: chemrox
dimethylation procedures & reagent choice
It looks like I could N-alkylate trytpamine with Ch3I in acetonitrile with 1.5 eq of Hunig's base

...
20-4-2016 at 11:59
by: chemrox
Where do you experiment ?
I converted a kitchen in the space I rented for offices. I built a sort of fume evacuation system by ...
20-4-2016 at 10:52
by: chemrox
Selling my glassware
Can't you wash it?
20-4-2016 at 10:39
by: chemrox
questions regarding formation and reductive alkylation of an imine
The ochem4free links are out of date with a warning page popping up
19-4-2016 at 11:26
by: chemrox
dimethylation procedures & reagent choice
what about using Hunig's base and MeI?
19-4-2016 at 10:31
by: chemrox
US-based chemists: has Laboy Glass shipped to you successfully?
I have never had a problem receiving glassware or reagents. I can't imagine why glassware would be d ...
18-4-2016 at 17:25
by: chemrox
dimethylation procedures & reagent choice
Thanks-that is consistent with the diagram too..
18-4-2016 at 15:49
by: chemrox
Sodium Ethyl Sulfate
Two comments: 1) it's a worthwhile venture as sodium ethyl sulfate goes for $134/25g. 2) this isn't ...
18-4-2016 at 13:59
by: chemrox
dimethylation procedures & reagent choice
@Pummukli-any chance you could post those refs in refs?
I found the attached. I don't understand th ...
18-4-2016 at 12:55
by: chemrox
dimethylation procedures & reagent choice
I want to dimethylate an amine. The compound is an aromatic ethyl amine. The Ar group is probably ir ...
17-4-2016 at 22:17
by: chemrox
How to test if H2SO4 or HBr
[rquote=445442&tid=65943&author=ParadoxChem126]MrHomeScientist's sulfate test is probably th ...
15-4-2016 at 12:18
by: chemrox
lipless beakers
I have a 200 ml lipless glass beaker I got in a lot years ago and I would like to find a source for ...
15-4-2016 at 11:29
by: chemrox
DIY/Cheap Tube Reactor
I have a tube furnace and 1 inch od X 12" tube. I don't use these. They could be had for a price. I ...
15-4-2016 at 10:44
by: chemrox
Bad Habits In The Lab
[rquote=444236&tid=62030&author=100PercentChemistry]Not washing my glassware after an experi ...
15-4-2016 at 10:26
by: chemrox
Potassium Iodide
[rquote=445094&tid=65899&author=JJay]There are a number of sellers on everyone's favorite au ...
15-4-2016 at 10:09
by: chemrox
DIY recirculating aspirator issues
I bought Cole-Palmer aspirator pump for $40 and it's been honking along for ten years. It has dual a ...
13-4-2016 at 11:51
by: chemrox
DIY bunsen
As above and you really need a needle valve for the gas inlet and an adjuster for the air. These par ...
12-4-2016 at 16:15
by: chemrox
government restrictions why bother
[rquote=444373&tid=65819&author=Alkoxide]Many politicians are a special kind of special. The ...
12-4-2016 at 16:07
by: chemrox
preparation of cinnamic acid from benzaldehyde
[quote]99.3% benzaldehyde, 0.5% benzoic acid, 0.1% benzyl alcohol, and a trace of cinnamaldehyde. [/ ...
12-4-2016 at 14:17
by: chemrox
OpenBabel - Informative Thread
aga's profile confirms my sanity
11-4-2016 at 21:51
by: chemrox
preparation of cinnamic acid from benzaldehyde
[rquote=444850&tid=65876&author=Loptr]I was going to recommend purifying the adduct, but I w ...
11-4-2016 at 21:46
by: chemrox
Chloral from Chloroacetaldehyde
[rquote=444978&tid=65895&author=gdflp][rquote=444976&tid=65895&author=aga]
Does MnO ...
11-4-2016 at 12:35
by: chemrox
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