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Gunpowder (Potassium Chlorate) from Bleach
Two things:
It would definitely be worth designing even a small electrolysis cell if you want to ... |
4-12-2020 at 10:59
by: greenlight |
Powder addition in reflux?
[rquote=650036&tid=156626&author=SHADYCHASE54]Dr. Bob helped me with this issue and sold me ... |
28-11-2020 at 13:57
by: greenlight |
Reaction kinetics - very long stirrings?
Basically put, stirring increases the chance of collisions between the reagents to produce the desir ... |
28-11-2020 at 13:53
by: greenlight |
Trinitrotoluene help
Hmmmm, I remember when I was a teenager about 16 or 17 I attempted TNT synthesis with azeotropic nit ... |
26-11-2020 at 12:39
by: greenlight |
Preparation of Di-(4-chloro-2-nitrophenyl)-disulphide
Beautiful write-up, love the pics and reaction scheme |
24-11-2020 at 08:01
by: greenlight |
Pretty Pictures (2)
Dirty old ice pack ammonium nitrate crystals.
[Edited on 24-11-2020 by greenlight] |
24-11-2020 at 07:55
by: greenlight |
Hydroxylamine via HCL, Nitromethane, and H2O?
Thought I would add to this instead of making a 200th hydroxylamine thread.
The acid-catalyzed hy ... |
24-11-2020 at 07:26
by: greenlight |
what happened to LL?
[rquote=647568&tid=156409&author=TriiodideFrog]I was wondering the same thing. Maybe he deci ... |
28-10-2020 at 08:32
by: greenlight |
lead azide trouble
Could there be some low density issue with the powder affecting DDT transformation (density》= VODã ... |
20-10-2020 at 09:30
by: greenlight |
lead azide trouble
What about the lead salt source? Was that pure? |
19-10-2020 at 09:30
by: greenlight |
lead azide trouble
That is not normal.
Lead azide should easily DDT transfer even in very small amounts. I have det ... |
18-10-2020 at 09:30
by: greenlight |
Det caps in air bags
I cut open an airbag several years ago and I found what's left of it after I retrieved the sodium az ... |
11-10-2020 at 09:32
by: greenlight |
1,3,5,7-tetranitro-1,3,5,7-tetrazoctane
For the final nitrolysis of DPT, this paper was used: http://www.energetic-materials.org.cn/publish_ ... |
3-10-2020 at 09:45
by: greenlight |
HMX via nitrolysis of DPT
I thought that 50C would start to decompose the acid as well as purge the nitrogen dioxide but 10 mi ... |
2-10-2020 at 10:44
by: greenlight |
High pressure reactors
Have you thought of just converting a fire extinguisher over as long as the reagents won't react wit ... |
25-9-2020 at 10:40
by: greenlight |
HMX via nitrolysis of DPT
Thanks underground
@Microtek, only 5 or 10 minutes? Wow, at what temperature was this done at a ... |
25-9-2020 at 10:27
by: greenlight |
HMX via nitrolysis of DPT
Atmospheric distillation of 70% nitric acid complete resulting in yellow fuming nitric acid.
Vacuum ... |
23-9-2020 at 09:40
by: greenlight |
Reaction vessel choosing?
Beakers: Most reactions that require mixing and heating or cooling.
Conicals: Titrations and making ... |
23-9-2020 at 09:31
by: greenlight |
HMX via nitrolysis of DPT
Thanks
Yes, I might run another batch as I was thinking it would be interesting to detonate som ... |
7-9-2020 at 09:33
by: greenlight |
Dinitro pentamethylene tetramine
Well here it is:
[b]Materials:[/b]
* Nitrourea (7.25 grams)
* Formaldehyde solution 37% (45 ... |
6-9-2020 at 22:35
by: greenlight |
Unconventional Shaped Charges
I did have one that I always used to use but the battery went dead that day so I was forced to try a ... |
6-9-2020 at 21:56
by: greenlight |
HMX via nitrolysis of DPT
Yes, I'm using this one that's actually quite old:
https://www.google.com/url?sa=t&source=web&a ... |
4-9-2020 at 10:40
by: greenlight |
Nitrourea
[b]reagents[/b]:
* 19g urea nitrate
* 70ml 98% sulfuric acid
[b]method[/b]
70 ml of 98% ... |
4-9-2020 at 06:57
by: greenlight |
Urea nitrate
Not much to see here really. 22 grams of hardware store urea was dissolved in 55ml of distilled w ... |
4-9-2020 at 06:45
by: greenlight |
HMX via nitrolysis of DPT
Yes I have nitrourea but I did the steps on a small scale and only have 8 grams of it. I also suffe ... |
4-9-2020 at 06:39
by: greenlight |
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