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KOH/NaOH azeotropic dehydration
My guess is that this won't work due to the high affinity of KOH and NaOH for water. This is typical ...
4-3-2019 at 03:48
by: 12thealchemist
Is it possible to synthesise Pd/C from home?
Here's a very recent youtube video on preparing Pd/C. YouTube isn't always the best source of inform ...
1-3-2019 at 01:46
by: 12thealchemist
Methane synthesis
If we're considering all possibilities, one could generate methane via protonation of a methyl Grign ...
27-2-2019 at 07:24
by: 12thealchemist
Where can I buy distilled water in the UK?
[rquote=603477&tid=145543&author=fff]Hi all,
I need some distilled water. I've searched loc ...
25-2-2019 at 06:10
by: 12thealchemist
Synthesis of longer chain tertiary alcohols
Rubidium has recently been synthesised by Pok over on the potassium thread and the "new" German chem ...
22-2-2019 at 07:48
by: 12thealchemist
The Wump Incident
This reminds me a similar incident many many years ago in a polystyrene (unexpanded) container that ...
20-2-2019 at 07:42
by: 12thealchemist
Preparation of alkali metals via the catalysed magnesium reduction process
This is the final version, including the latest updates from NurdRage. He is set to release one more ...
19-2-2019 at 06:12
by: 12thealchemist
Legality discourse split from "4-Allylcatechol Methylenation"
[rquote=601918&tid=144615&author=DavidJR]Errrrrrrrrr.... this looks a bit dodgy. It's only a ...
14-2-2019 at 07:36
by: 12thealchemist
Preparation of Nickel (ii) acetate
Why would the salts be more dangerous as solid than in solution? Surely solution is just as dangerou ...
14-2-2019 at 02:41
by: 12thealchemist
Cryogenic Chemistry (Cryochem)
This paper might be of use, with regards to the liquid SO[sub]2[/sub]
1-2-2019 at 01:30
by: 12thealchemist
Cryogenic Chemistry (Cryochem)
Almost any reaction involving BuLi uses a dry ice/acetone bath, including making LDA (lithium diisop ...
28-1-2019 at 04:38
by: 12thealchemist
Preparation of alkali metals via the catalysed magnesium reduction process
I have been updating the write-up as the videos come out, but figured I would only update this post ...
30-12-2018 at 02:11
by: 12thealchemist
Alright looking for insight
I think the "5" electron clouds are supposed to be three sp[sup]2[/sup] hybridised orbitals, and one ...
24-12-2018 at 04:03
by: 12thealchemist
Choice of metal for thermite
I think that depends on how easy it is to obtain, store, and use the finely divided metal. It sounds ...
23-12-2018 at 01:27
by: 12thealchemist
Removing BrCl from Bromine
Tried to make bromine from BCDMH? (1-Bromo-3-chloro-5,5-dimethylhydantoin, a water sanitation chemic ...
20-12-2018 at 12:50
by: 12thealchemist
Tired of reporting spam
I've noticed a significant increase in the quantity of spam slipping through the net. It seems the m ...
20-12-2018 at 12:22
by: 12thealchemist
Removing fishy smell from air - possible?
The amount of amine required to give a smell is absolutely minuscule. With a home lab set up, the qu ...
18-12-2018 at 09:40
by: 12thealchemist
Tin from Solder
Lead chloride is noticeably more soluble in solutions where there is already a high chloride concent ...
17-12-2018 at 01:38
by: 12thealchemist
Gradual disintegration of metal thermite balls
I've noticed this many times with the metallic nodules obtained from thermites and thermite-type rea ...
16-12-2018 at 01:49
by: 12thealchemist
Astatine probable vapor colour
There is this diagram on Wikipedia on the Tennessine page:

[file]72419[/file]
15-12-2018 at 02:00
by: 12thealchemist
Astatine probable vapor colour
To me, bromine vapour is reddish brown, more red than nitrogen dioxide but less red than chromyl chl ...
14-12-2018 at 11:20
by: 12thealchemist
Uranium ore tests
Uranates and vanadates both have the capability of forming complex anionic structures; the main grou ...
14-12-2018 at 05:45
by: 12thealchemist
Astatine probable vapor colour
Would it be possible to calculate the approximate colour by working from the molecular orbitals? The ...
14-12-2018 at 02:21
by: 12thealchemist
Uranium ore tests
Which vanadium species you get is very pH dependent. Vanadates are notorious for forming aggregatory ...
13-12-2018 at 09:32
by: 12thealchemist
Uranium ore tests
The old-school analytical tests (now hobby chem) from my analysis table book for uranium are:
[list ...
13-12-2018 at 09:16
by: 12thealchemist
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