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Reusing leftover Zn from Zn/HCl reduction
Yes you can reuse it, I once even did it myself when low on zinc dust.
5-2-2011 at 19:03
by: Magic Muzzlet
Chemicals in NZ. Not industrial qunatites
Nitric acid, shipped legally or illegally, is one of THE last things I would want to ship overseas.
30-1-2011 at 14:34
by: Magic Muzzlet
Vacuum Filtration Woes...
It shouldn't be ripping, you need to lower the vacuum, or maybe the papers are just really shitty. I ...
30-1-2011 at 10:27
by: Magic Muzzlet
Distilling from a viscous mixture
It's already been covered and it's no problem to get out of the flask, distillation has always gone ...
30-1-2011 at 09:46
by: Magic Muzzlet
Alternative to cyclohexane for halogen extraction
Basically washing the DCM is having your solvent in the sep funnel, then you add water, shake etc an ...
25-1-2011 at 13:36
by: Magic Muzzlet
Alternative to cyclohexane for halogen extraction
The ks3 stripper from kleanstrip is my OTC source for DCM, all I do is fill up a flask with the past ...
25-1-2011 at 12:15
by: Magic Muzzlet
When naphthalene balls aren’t naphthalene balls(?)
The issue could have been avoided by reading the wrapper in the first place? It just seems obvious y ...
24-1-2011 at 14:30
by: Magic Muzzlet
Alternative to cyclohexane for halogen extraction
Chloroform should work just as well for your purpose I presume. For cyclohexane elemental scientific ...
21-1-2011 at 11:50
by: Magic Muzzlet
Alternative to cyclohexane for halogen extraction
Cyclohexane is very easy to obtain especially in the us, even as a hobbyist. But I would use DCM pro ...
21-1-2011 at 11:13
by: Magic Muzzlet
PREPERATION OF ACIDS FROM ALKALI SALTS
There is lots of info in many places look on this forum, google, lambdasyn possibly versuchschemie.d ...
17-1-2011 at 20:29
by: Magic Muzzlet
PREPERATION OF ACIDS FROM ALKALI SALTS
I think he wants to make formic acid from the sodium formate, but the question is quite unclear to m ...
17-1-2011 at 19:51
by: Magic Muzzlet
flask insulation?
You should just use a pan or something on top with sand/oil/water, don't rely on just putting a flas ...
12-1-2011 at 19:58
by: Magic Muzzlet
Sodium Ethoxide
http://www.orgsyn.org/orgsyn/orgsyn/prepcontent.asp?print=1&showprint=1&prep=cv1p0258
:)
10-1-2011 at 20:45
by: Magic Muzzlet
mental block need ideas
Then why don't you do exactly what you are wanting to do? Syntheses take time, during that time you ...
7-1-2011 at 09:13
by: Magic Muzzlet
Nitric acid production
There is a search function and also threads on this subject ;)
7-1-2011 at 08:47
by: Magic Muzzlet
mental block need ideas
You should find out beforehand however long it takes you which reactions you would like to do, then ...
7-1-2011 at 08:28
by: Magic Muzzlet
The short questions thread (3)
I lack the resources to do a column at this time, but I have been trying crystallization from ethano ...
6-1-2011 at 11:10
by: Magic Muzzlet
WTB Hydroxylamine hydrochloride
I do not see how the prep in Brauer is better than a simple reflux. The writeup on versuchschemie is ...
1-1-2011 at 12:16
by: Magic Muzzlet
WTB Hydroxylamine hydrochloride
The method with sulfuric acid will give the sulfate, I should have included that part of info.. Anyw ...
30-12-2010 at 19:00
by: Magic Muzzlet
WTB Hydroxylamine hydrochloride
You won't get very far in chemistry with that attitude.
You should check out photographic supplies ...
30-12-2010 at 16:38
by: Magic Muzzlet
Isoproyl Nitrite gasmask
Haha I really thought this was going to be about making a mask to breathe alkyl nitrites with, but y ...
30-12-2010 at 10:53
by: Magic Muzzlet
The short questions thread (3)
1-pentyl-3-(1-naphthoyl)indole, JWH-018.

I have made this compound on 3 occasions and after alkyl ...
28-12-2010 at 11:53
by: Magic Muzzlet
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
Well I am back reporting in this thread again, in short still no success at all with the sulfuric du ...
28-12-2010 at 11:26
by: Magic Muzzlet
The short questions thread (3)
Thanks for your input Vulture and I know it is meant to be freshly prepared, but the solid I got is ...
12-12-2010 at 15:08
by: Magic Muzzlet
Esters
There are a few good sites on the net but I'm sure many would be apprehensive about just posting the ...
26-11-2010 at 10:24
by: Magic Muzzlet
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