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Does this seem a safe and effective way to alkylate ammonia?
True, I forgot to consider the Na2CO3 would likely push out most of the NH3 from the aqeous. That do ... |
23-6-2017 at 15:02
by: alking |
magnetic stirrer problem
How hot are we talking? Mine will sometimes generate electricity with prolongued stirring but never ... |
23-6-2017 at 07:01
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I just realized the smell in this case may be from HBr, I did not wash the resulting product with a ... |
22-6-2017 at 17:28
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I just came across [url=https://www.youtube.com/watch?v=RV7F9u8B2DI]this[/url] too. No real need to ... |
22-6-2017 at 15:31
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I'm working up the 2-BrPr I made yesterday to finish this and it smells very strange, def not what I ... |
22-6-2017 at 14:16
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
[rquote=486124&tid=74874&author=Melgar][rquote=486114&tid=74874&author=alking]Are yo ... |
22-6-2017 at 13:52
by: alking |
Dimethylamine identification help
What he said. 150C is pretty close imo under the circumstances, it's highly unlikely you have anythi ... |
22-6-2017 at 08:20
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
Are you referring to the 2-BrPr synthesis or the amine alykation? I was talking about the later, but ... |
21-6-2017 at 09:59
by: alking |
Hg/Al Reductive Amination w/Ammonia - Not Viable?
What is cyclohexamine sold as in autoparts stores? That's one I'd like to add to my list.
Cyclohe ... |
21-6-2017 at 07:27
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I wasn't aware of that, but it makes sense. No sulfur on hand for now though and plenty of old drain ... |
21-6-2017 at 07:21
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
The vessel was held in a water bath between 60-64C for 4 hours after which heating was stopped and i ... |
20-6-2017 at 22:43
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I came across this while doing some more research.
https://www.thevespiary.org/rhodium/Rhodium/h ... |
20-6-2017 at 15:51
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
Well I'm giving it a shot right now, wish me luck. I've got it heating in a water bath inside a seal ... |
20-6-2017 at 14:56
by: alking |
What kind of pressure unit is "p mm."?
Thanks! I feel kind of dumb, it is mentioned right there in the first paragraph preceding the data, ... |
20-6-2017 at 10:08
by: alking |
What kind of pressure unit is "p mm."?
I'm looking at this pdf:
https://www.ideals.illinois.edu/bitstream/handle/2142/4535/engineeringex ... |
20-6-2017 at 08:58
by: alking |
Vacuum filtration pump?
I would suggest a water aspirator. If all you're ever going to do is filtrations then the 12V would ... |
19-6-2017 at 09:50
by: alking |
How do you powderise substances?
I toss it in the air, roundhouse kick it to dust, and then catch it all in a storage container befor ... |
19-6-2017 at 09:08
by: alking |
Mysterious chinese glassware sellers
That's my guess. I've used nashin before without issue, but I have received some flasks that were we ... |
19-6-2017 at 09:04
by: alking |
Removing acetone from ethers and other non polars
Water washing is the easiest way unless you have a lot of acetone in it as mentioned. If there's too ... |
19-6-2017 at 08:57
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I came across that earlier, I know that's a feasible route, but I'm wondering if this would specific ... |
18-6-2017 at 20:45
by: alking |
Does this seem a safe and effective way to alkylate ammonia?
I'd like to make n,n-diisopropylamine by alkylating ammonia in methanol by reacting it with 2-bromop ... |
18-6-2017 at 18:01
by: alking |
Is there any way I can determine my acid/base concentrations from what is on hand?
I actually just ran out of sodium carbonate yesterday! I'll probably wait until I get more rather th ... |
17-6-2017 at 09:07
by: alking |
Is there any way I can determine my acid/base concentrations from what is on hand?
I currently have no known concentrations in which to titrate with to determine that of another acid ... |
17-6-2017 at 06:21
by: alking |
Nitrated Biodiesel?
How well was everything mixed up before adding it? Is it possible an 'acidic pocket' formed some eth ... |
16-6-2017 at 12:02
by: alking |
Identify This?
Looking at that picture it does seem they attached the condenser directly on top. That just seems ve ... |
16-6-2017 at 08:39
by: alking |
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