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Dinitrourea
Can anyone explain why they use trifluoroacetic acid (5x5ml) to wash the dinitrourea?
It's pretty e ... |
12-8-2010 at 06:13
by: maxidastier |
Nitration Calculations
Me, tooo  |
12-8-2010 at 01:14
by: maxidastier |
How well erythritol nitrates in HNO3/H2SO4?
Ok, sry, I had some other facts in my mind. You're right. Basic stuff. I should have known better.
... |
12-8-2010 at 01:02
by: maxidastier |
How well erythritol nitrates in HNO3/H2SO4?
I tried nitration of Erythritol with self distilled HNO3 98%.
And I suggest not to le temperatures ... |
11-8-2010 at 05:38
by: maxidastier |
Calcium cyanamide and aminoguanidine from urea and calcium oxide
Next step is the making of guanidine compounds?
There is another thread existing about preparati ... |
11-8-2010 at 05:24
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
I'm only interested in the step of producing Guaninidinitrate and further Nitroguanidin.
Is there a ... |
11-8-2010 at 00:11
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
Well, actually I tried both aging times with the same amounts and got better results when agin more ... |
30-7-2010 at 02:34
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
Well, actually, there are a few more things, that need to be updated, nice work anyway Engager, but: ... |
29-7-2010 at 07:30
by: maxidastier |
Rhodiums loss of GABA to GHB
[rquote=75747&tid=3159&author=jimmyboy]just oxidize THF -- far easier to come by[/rquote]
... |
11-7-2010 at 05:32
by: maxidastier |
ETN synthesis problem
Well, thank you, but as I see, this programm as a little bit overseized.
I really just need a equot ... |
9-7-2010 at 09:46
by: maxidastier |
ETN synthesis problem
Can someone help me with the equotation?
I'd like to use my distilled 98% HNO3 instead of KNO3..
... |
3-7-2010 at 09:57
by: maxidastier |
ETN synthesis problem
....if you don't use it immediately or dissolve it in NG or whatever. |
16-6-2010 at 09:49
by: maxidastier |
ETN synthesis problem
That's not the point. I always made it small scale. My question is only how much of every ingredient ... |
19-5-2010 at 07:10
by: maxidastier |
ETN synthesis problem
And how much KNO3? |
17-5-2010 at 10:19
by: maxidastier |
ETN synthesis problem
Would you be so kind and tell me: What is so dangerous about adding too much H2SO4 IN THIS PARTICULA ... |
16-5-2010 at 05:43
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
I did it the same way, but: 1. They send out (NOx)gases in my room, so that the room becomes dusty : ... |
15-5-2010 at 09:51
by: maxidastier |
ETN synthesis problem
when the task is 100g H2SO4/60gNitrate/15gErythritol, then 100ml of 95% H2SO4 are way enough, becaus ... |
15-5-2010 at 02:18
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
I've some Nitroguanidin now, but it dries very slowly. Can I put it in the oven, or is it not normal ... |
15-5-2010 at 01:22
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
I tried it with: 170 g Ammonium Nitrate, 100+60g Urea and 40 g Silical Gel.
Yield should have been ... |
10-5-2010 at 10:28
by: maxidastier |
ETN synthesis problem
So I'll try to find out how many milliliters of 95% H2SO4 are the same as 100 g of 100% H2SO4, right ... |
5-5-2010 at 06:10
by: maxidastier |
ETN synthesis problem
@noise: maybe you just stop making noise |
5-5-2010 at 03:12
by: maxidastier |
ETN synthesis problem
I have 95% H2SO4...so do I need 100 g or 100 ml?? |
4-5-2010 at 07:17
by: maxidastier |
ETN synthesis problem
nitration time is 20-30 mins, but it doesn't hurt if you make it 45 mins; stirring, at least every 5 ... |
2-5-2010 at 01:58
by: maxidastier |
ETN synthesis problem
so I add 60 g of nitrate salt to 100 g of H2SO4 95%?
I tried, but it's impossible to stirr... |
1-5-2010 at 05:52
by: maxidastier |
ETN synthesis problem
it fu**ing didn't work with dissolving Erythritol in H2SO4 and then adding nitrate salt ammonium nit ... |
1-5-2010 at 04:36
by: maxidastier |
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