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Copper(II) Aspirinate Synthesis
Synthetic updates!

The green cobalt complex:
Sodium Tris-carbonatocobaltate (III) Trihydrate
( ...
27-6-2013 at 19:16
by: sargent1015
Bad days in the lab or with glassware?
[rquote=289581&tid=13214&author=sargent1015]Did not happen to me, but my co-worker shoved a ...
27-6-2013 at 17:00
by: sargent1015
Copper(II) Aspirinate Synthesis
[rquote=289728&tid=24730&author=Acidum] Call me grammar/iupac/nerdy nazi, but I just can not ...
27-6-2013 at 15:43
by: sargent1015
The short questions thread (3)
[rquote=289597&tid=14239&author=DubaiAmateurRocketry]

Nah i want lithium hydride.[/rquote ...
27-6-2013 at 10:32
by: sargent1015
Copper(II) Aspirinate Synthesis
[rquote=289586&tid=24730&author=DraconicAcid]
Thanks for posting that. Now I'm wondering i ...
27-6-2013 at 05:05
by: sargent1015
Copper(II) Aspirinate Synthesis
Here's that paper.

[file]23938[/file]

I think I will attempt the Tris-carbonatocobaltate(III ...
26-6-2013 at 10:06
by: sargent1015
Bad days in the lab or with glassware?
Did not happen to me, but my co-worker shoved a stir rod through an evacuated dewar flask. Needless ...
26-6-2013 at 10:01
by: sargent1015
Storage Questions
[rquote=289568&tid=24800&author=mud]electrical tape would leave a residue mess.[/rquote]

...
26-6-2013 at 08:42
by: sargent1015
Storage Questions
[rquote=289560&tid=24800&author=mud]What about shipping said containers? What is the tape co ...
26-6-2013 at 07:47
by: sargent1015
Science equipment looking for a home
[rquote=289489&tid=15667&author=Magpie] It should solder OK then I would think. [/rquote]
E ...
25-6-2013 at 17:49
by: sargent1015
The Sciencemadness Book Project, Revived
Actually, if you wanted to write up a nice procedure for that, I am thinking of including a section ...
25-6-2013 at 17:37
by: sargent1015
Science equipment looking for a home
Hmmm I guess I could make one of those.... Just a simple adapter and an aerator?
25-6-2013 at 16:29
by: sargent1015
Science equipment looking for a home
Hey Dr. Bob, I am assuming the last list is fairly up to date. Do you have any vacuum aspirators or ...
25-6-2013 at 10:28
by: sargent1015
The Sciencemadness Book Project, Revived
Old school is quite relative for this 21 year old chemist :P
25-6-2013 at 08:22
by: sargent1015
Copper(II) Aspirinate Synthesis
Talk about lucky snag. That amine makes it an excellent ligand. And if it is the free acid version, ...
25-6-2013 at 08:21
by: sargent1015
The Sciencemadness Book Project, Revived
Alright, so it's summer and I have freetime again away from the classroom. I am in need of your guys ...
25-6-2013 at 05:39
by: sargent1015
A project everyone can pitch in on! Writing the book on chemistry.
Well, crap, how did I miss chromatography! Probably because that's all I do all day everyday and it ...
25-6-2013 at 05:30
by: sargent1015
A project everyone can pitch in on! Writing the book on chemistry.
I like to think that the target audience is someone with maybe a high school class or two in chemist ...
24-6-2013 at 20:46
by: sargent1015
Vacuum Protection
There will always be some vapor, but the two trap idea is best. If I may ask, what typical solvents ...
24-6-2013 at 20:30
by: sargent1015
Vacuum Protection
I am hoping that you cool your trap with ice, dry ice, running water, etc. Otherwise, most solvents ...
24-6-2013 at 19:31
by: sargent1015
Copper(II) Aspirinate Synthesis
Oooo do that! If I may ask, where did you get the anthranilate?
24-6-2013 at 19:02
by: sargent1015
Copper(II) Aspirinate Synthesis
Just took an NMR of the aspirin that I isolated over the weekend and it is beautifully pure. I will ...
24-6-2013 at 11:50
by: sargent1015
1,1,2,2-tetrabromoethane Synthesis & Impurities
Not too ridiculous, a dry ice and acetone bath gets you to -78C (with dry ice being available from s ...
24-6-2013 at 11:42
by: sargent1015
lots of reagents for sale
[rquote=288225&tid=24657&author=Antiswat]not to break apart the business of this.. thats som ...
23-6-2013 at 21:20
by: sargent1015
Poor Yields of Elemental Sulfur extraction with Xylene from Encap™ Fast Acting™ Sulfur Plus AST™
God these are a delight to read :D Keep on doing science, I love reading your posts!
23-6-2013 at 21:10
by: sargent1015
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