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Help with Acetylation of Catechol
Thank you Boffis!

I have been searching a lot for a procedure for catechol diacetate, and did not ...
2-1-2025 at 11:00
by: Maui3
Help with Acetylation of Catechol
Today, I attempted to acetylate catechol by first adding catechol to a NaOH solution at room tempera ...
2-1-2025 at 09:17
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
I smelled bromal too.
2-1-2025 at 01:26
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
Interesting, thanks!
1-1-2025 at 02:52
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
Well then you'd have to use H2SO4 too, to dry the HBr. I geuss sodium bromide and sodium bisulfate c ...
1-1-2025 at 01:43
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
Thank you jackchem2001! Those are great points!
Chloric1, I definitely agree with you.
1-1-2025 at 01:02
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
https://imgur.com/8G9yMwq
https://imgur.com/e4BsCw1
30-12-2024 at 11:01
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
Here are two pictures of the procedure:
[img]https://imgur.com/a/nHQumLT[/img]
[img]https://imgur. ...
30-12-2024 at 11:01
by: Maui3
2-Chemical Synthesis of Alkylbromides (Without The Use Of H2SO4)
Today, I succesfully synthesized ethyl bromide (Bromoethane) from just 2 chemicals: ethanol and brom ...
30-12-2024 at 11:00
by: Maui3
Total synthesis of muscimol + extraction and isolation from Amanita muscaria
I might actually replicate this procedure. Is nitrogen neccesary for those steps? I found this paper ...
30-12-2024 at 08:40
by: Maui3
How likely is HCl to cleave methylenedioxy groups?
For reference I am talking about doing a FC-alkylation with benzodioxole and ethyl chloride.
29-12-2024 at 12:43
by: Maui3
How likely is HCl to cleave methylenedioxy groups?
How likely is the HCl generated in friedels craft alkylation to cleave a methylenedioxy group?
29-12-2024 at 12:41
by: Maui3
FC-alkylation Positioning
Thank you for the clarification! But this still depends on temperature, right?
27-12-2024 at 03:11
by: Maui3
FC-alkylation Positioning
I am gonna do a FC-alkylation soon with ethyl bromide, 1,3-benzodioxole (1,2-methylenedioxybenzene) ...
26-12-2024 at 08:36
by: Maui3
Total synthesis of muscimol + extraction and isolation from Amanita muscaria
I have actually thought of extracting Muscimol from Amanita Muscaria before. Couldn't really (supris ...
23-12-2024 at 09:57
by: Maui3
(My) Total Synthesis of a Legal Quaaludes Analogue (Etaqualone)
[b]Important Note:[/b]
I know about Methaqualones uses as a recreational drug, but I am just making ...
21-12-2024 at 10:39
by: Maui3
How dry does HBr need to be for this reaction?
Thank you woelen for the tips! I will try it.
Teodor, I am pretty sure it works with bisulfate + br ...
19-12-2024 at 10:21
by: Maui3
How dry does HBr need to be for this reaction?
Hi! I am trying to make dibromomethane like this:

CH2Cl2 + HBr = CH2BrCl + HCl
CH2BrCl + HBr = C ...
18-12-2024 at 06:26
by: Maui3
Chemical Price Comparison Software in the making..
That's a lot of suppliers chempyre235!
Thank you - it definitely helps!
17-12-2024 at 10:24
by: Maui3
Chemical Price Comparison Software in the making..
Ah, didn't know that - will remove Elemental Scientific now then.. It was actually so difficult to a ...
15-12-2024 at 09:11
by: Maui3
Chemical Price Comparison Software in the making..
Right now I am working on adding suppliers in the U.S.

I am using this forums list of suppliers, ...
15-12-2024 at 03:25
by: Maui3
Phthalimide -> Anthranillic acid Reaction Not Working
Bnull, thank you for sending me the procedure :) I'll probably try that.
Pumukli, thank you too! Wo ...
8-12-2024 at 07:27
by: Maui3
Phthalimide -> Anthranillic acid Reaction Not Working
Thank you for the tips!

Pumukli, what procedure were you following for the isatoic anhydride?
7-12-2024 at 12:33
by: Maui3
Phthalimide -> Anthranillic acid Reaction Not Working
Thank you. I think my bleach might also contain impurities, since the mixture turned black. I am sup ...
7-12-2024 at 10:11
by: Maui3
Phthalimide -> Anthranillic acid Reaction Not Working
Hi!

I have tried to make anthranillic acid from phthalimide too many times now. It just does not ...
7-12-2024 at 06:59
by: Maui3
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