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Extraction and crude purification notes and procedure
Ok, so I finally got around to cracking some of these batteries open to try to get some SOCl[sub]2[/ ... |
7-8-2021 at 18:21
by: Monoamine |
Protection of the the indole nitrogen
I've been thinking about this a bit more lately, and I'm starting to suspect that the nitrogen in th ... |
7-8-2021 at 07:36
by: Monoamine |
Protecting groups for tertiary amines
[rquote=662983&tid=157678&author=EverythingAl2O3]Is there anything stopping you from doing a ... |
7-8-2021 at 07:20
by: Monoamine |
Protecting groups for tertiary amines
[rquote=663131&tid=157678&author=clearly_not_atara][rquote=662990&tid=157678&author= ... |
30-7-2021 at 18:13
by: Monoamine |
This seems like a pretty straight forward way to make acetal protected amines
This may be a bit late, but it seems pretty useful, so I'll post this here anyay:
[file]89605[/f ... |
30-7-2021 at 18:04
by: Monoamine |
Thionly chloride from batteries
Also, I came across a chemical vendor in India who sells SOCl2 and seems quite legit. In my experien ... |
30-7-2021 at 17:19
by: Monoamine |
Thionly chloride from batteries
Interesting! And yes, definitely want to be careful with the lithium, although considering that not ... |
30-7-2021 at 17:16
by: Monoamine |
Replacing halogen by hydrogen
Ah cool, Grignard may be the way to go then. Thanks for the tip!
Basically, I was hoping to make ... |
30-7-2021 at 17:05
by: Monoamine |
Replacing halogen by hydrogen
I've been looking far and wide for a method to perform the following reaction:
R-O-CH[sub]2[/sub] ... |
30-7-2021 at 13:55
by: Monoamine |
Quenching excess H2 in a reaction.
Following an earlier post for the catalytic preparation of NaH at room temperature.
The think is ... |
30-7-2021 at 04:38
by: Monoamine |
Electrophilic chlorination
[rquote=663132&tid=157734&author=clearly_not_atara]I'm not convinced that aldimino/ketimino ... |
21-7-2021 at 14:09
by: Monoamine |
FeBr3 from Fe
[rquote=108453&tid=9323&author=Klute]I decided on using the 37% just because it was closer a ... |
21-7-2021 at 13:42
by: Monoamine |
FeBr3 from Fe
Once you have some Br[sub]2[/sub], couldn't you just dry it by washing it with concentrated sulfuric ... |
21-7-2021 at 13:33
by: Monoamine |
Electrophilic chlorination
[rquote=663119&tid=157734&author=clearly_not_atara]Snap back to reality: [i]why[/i] are you ... |
20-7-2021 at 19:23
by: Monoamine |
Electrophilic chlorination
[rquote=663104&tid=157734&author=Monoamine]
PS:[b]An even more important question (and ma ... |
20-7-2021 at 15:41
by: Monoamine |
Possible recipe to do this:
Ok, so I thought about it a bit, and I think that it may be possible to do like this:
I tried to ... |
20-7-2021 at 15:22
by: Monoamine |
Electrophilic chlorination
So I'm starting to draw up all the prerequisites for a planned electrophilic chlorination off an aro ... |
20-7-2021 at 13:45
by: Monoamine |
Protecting groups for tertiary amines
[rquote=662985&tid=157678&author=njl]Or deprotonate and perform William ether synthesis[/rqu ... |
20-7-2021 at 09:51
by: Monoamine |
Protecting groups for tertiary amines
[rquote=662526&tid=157678&author=karlos³]Boil it in ethanolamine to dequaternise.[/rquote]
... |
20-7-2021 at 09:46
by: Monoamine |
Another possible way to for protection:
Just saw this: (https://www.organic-chemistry.org/protectivegroups/amino/toluenesulfonamides.htm).
... |
11-7-2021 at 20:21
by: Monoamine |
Protecting groups for tertiary amines
[rquote=662544&tid=157678&author=Jenks][rquote=662537&tid=157678&author=Monoamine][r ... |
11-7-2021 at 20:04
by: Monoamine |
Answer:
According to this product safety sheet
([url=https://ehslegacy.unr.edu/msdsfiles/23752.pdf]Zn-H ... |
11-7-2021 at 18:17
by: Monoamine |
Disposal of solvents
Usually the local dump will take organic solvents. After all, they also take gasoline etc... It also ... |
11-7-2021 at 11:39
by: Monoamine |
Zn-Hg amalgam safety
I've been looking into reducing a ketone to an alkane. Scouring the literature, the classical way to ... |
11-7-2021 at 11:31
by: Monoamine |
Protecting groups for tertiary amines
[rquote=662529&tid=157678&author=Jenks]A very similar structure is ibogaine. Here is a [url= ... |
6-7-2021 at 16:44
by: Monoamine |
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