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ETN synthesis problem
@quicksilver:
100gr H2SO4
60gr KNO3
15gr Erythritol
according to other descriptions, it has t ... |
1-5-2010 at 02:29
by: maxidastier |
ETN synthesis problem
@Dough: Well, it sounds interesting but:
I've read that at a certain temperature (little above 35° ... |
1-5-2010 at 02:07
by: maxidastier |
Synthetic route to tetrazoles from urea & ammonium nitrate
Can you help me with synthesis of Guanidinitrate?
I don't understand the last part of your descript ... |
22-4-2010 at 10:11
by: maxidastier |
ETN synthesis problem
Well, I used different ratios and different nitrates (KNO3 and NH4NO3)
My last synthesis was from ... |
22-4-2010 at 10:02
by: maxidastier |
ETN synthesis problem
No, i don'T think this goes for ETN. When I once let it get over 30C it got very yellow (maybe the N ... |
15-4-2010 at 05:56
by: maxidastier |
ETN synthesis problem
A nitration time of only 20 mins seems not to lower the yield... |
14-4-2010 at 07:46
by: maxidastier |
ETN synthesis problem
oh my god...One hour earlier I prepared a new synthesis and followed your tips with only 20 mins of ... |
14-4-2010 at 06:29
by: maxidastier |
ETN synthesis problem
You only had an nitration time about 20 mins?
Won't that result in a low yield?
Because I realized ... |
14-4-2010 at 02:50
by: maxidastier |
ETN synthesis problem
Well, thankfully I kept that stuff that didn't dissolve in the methanol.
Although I couldn't believ ... |
13-4-2010 at 07:51
by: maxidastier |
ETN synthesis problem
Recrystallization seems to be one key issue.
The nitration shouldn't even be so short.
One might ... |
12-4-2010 at 10:06
by: maxidastier |
ETN synthesis problem
It's really annoying now.
My forth synthesis with the same result:
5 g of Erythritol didn't give m ... |
12-4-2010 at 08:55
by: maxidastier |
ETN synthesis problem
I'm wondering how many solvable non-ETN material is in the mix.
I prepared some ETN with 20 g Amm ... |
11-4-2010 at 04:51
by: maxidastier |
ETN synthesis problem
Really? Why do so many get high yields with the commerical Ethanol?
I have distilled my own METHANO ... |
3-4-2010 at 12:02
by: maxidastier |
ETN synthesis problem
But do you think those 50 g packages are enough? |
3-4-2010 at 09:15
by: maxidastier |
ETN synthesis problem
hello,
I'm just having one only question: Can I use Soda instead of Baking Soda? |
3-4-2010 at 08:26
by: maxidastier |
