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nitroaldol not dehydrating to nitrostyrene or something else?
More often than not melting points can vary by a few degrees depending on impurities in the product, ...
22-7-2014 at 14:49
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
[rquote=339232&tid=31878&author=Magpie]I think I was wrong here. I have never actually work ...
22-7-2014 at 13:56
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
So I made an interesting discovery today that explains a lot! In the process I found a very effectiv ...
22-7-2014 at 09:55
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
[rquote=339202&tid=31878&author=Magpie][rquote=339186&tid=31878&author=FireLion3]
H ...
21-7-2014 at 21:01
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
I've got plenty of reagents laying around. I've got some R-Napthylethylamine laying around that I'm ...
21-7-2014 at 20:23
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
Good point..... but this is urgent and I cannot afford to be waiting a week for a response by postin ...
21-7-2014 at 20:11
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
The odor seems to have mostly cleared up. Benzyl Bromide must be a strong lachrymator at very low co ...
21-7-2014 at 19:52
by: FireLion3
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice!
[b]I have a small fume-tent set up with a 500cfm fan running attached to a carbon scrubber. I walked ...
21-7-2014 at 19:16
by: FireLion3
NaOH + Drying agent as an alternative to using a strong base?
Removing water with drying agents to push equilibrium further to the right is a tried and true synth ...
21-7-2014 at 14:35
by: FireLion3
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA?
Good point.

I actually managed to find some DBDMH online. Sold under chlorine free "Brilliance S ...
21-7-2014 at 02:07
by: FireLion3
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA?
That's interesting, thank you, though, if I could get the bromine then I could skip the need for thi ...
20-7-2014 at 22:00
by: FireLion3
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA?
I recently learned about this as an exciting alternative to NBS. I remember glimpsing a similar comp ...
20-7-2014 at 21:29
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
[rquote=339111&tid=31843&author=mnick12]Well conversion is different than yield, as you seem ...
20-7-2014 at 20:23
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
Thanks for the reply. I wasn't attempting to take my frustration out on the community, just became r ...
20-7-2014 at 17:38
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
Are you intentionally going out of your way to twist my words and make fallacious statements? Please ...
20-7-2014 at 16:00
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
While that sort of reasoning is true in many reactions, it should be close to negligible in a reacti ...
20-7-2014 at 15:21
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
How can there be excess bromine? When I stop stirring, the bromine sinks to the bottom, when I start ...
20-7-2014 at 14:49
by: FireLion3
Oxone Aromatic Halogenation in Water - Is this write-up a lie?
I know, the title sounds stupid, but I don't really have much of an explanation here. This is my 4th ...
20-7-2014 at 13:38
by: FireLion3
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex
If Nickel II Chloride is soluble in both alcohol and water, I didn't think excess water would be an ...
20-7-2014 at 11:12
by: FireLion3
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex
I didn't see that concentration there. I do know I can get some pretty high purity acetone at anothe ...
19-7-2014 at 20:11
by: FireLion3
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex
This is the complex:
https://en.wikipedia.org/wiki/Bis%28triphenylphosphine%29nickel_chloride

I ...
19-7-2014 at 19:59
by: FireLion3
Benzene from Sodium Benzoate - Dry distillation required? Why?
That makes sense. I was hoping to make reasonable quantities of Benzene from Benzoate without having ...
14-7-2014 at 09:17
by: FireLion3
Benzene from Sodium Benzoate - Dry distillation required? Why?
I was looking at these preps and they all talk about dry distilling benzene from Sodium Benzoate and ...
14-7-2014 at 08:41
by: FireLion3
Thermoelectric Cooling Mantle?
I was thinking recently about endothermic and exothermic reactions. It's generally use to just turn ...
10-7-2014 at 10:02
by: FireLion3
Is there a general rule about stirring rate & reaction speed like there is for temperature?
[rquote=337740&tid=31483&author=ziqquratu][rquote=337734&tid=31483&author=FireLion3] ...
9-7-2014 at 18:35
by: FireLion3
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