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nitroaldol not dehydrating to nitrostyrene or something else? More often than not melting points can vary by a few degrees depending on impurities in the product, ... |
22-7-2014 at 14:49 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! [rquote=339232&tid=31878&author=Magpie]I think I was wrong here. I have never actually work ... |
22-7-2014 at 13:56 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? So I made an interesting discovery today that explains a lot! In the process I found a very effectiv ... |
22-7-2014 at 09:55 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! [rquote=339202&tid=31878&author=Magpie][rquote=339186&tid=31878&author=FireLion3]
H ... |
21-7-2014 at 21:01 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! I've got plenty of reagents laying around. I've got some R-Napthylethylamine laying around that I'm ... |
21-7-2014 at 20:23 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! Good point..... but this is urgent and I cannot afford to be waiting a week for a response by postin ... |
21-7-2014 at 20:11 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! The odor seems to have mostly cleared up. Benzyl Bromide must be a strong lachrymator at very low co ... |
21-7-2014 at 19:52 by: FireLion3 |
Accidentally made benzyl bromide! Ouch My eyes! What happen? Need advice! [b]I have a small fume-tent set up with a 500cfm fan running attached to a carbon scrubber. I walked ... |
21-7-2014 at 19:16 by: FireLion3 |
NaOH + Drying agent as an alternative to using a strong base? Removing water with drying agents to push equilibrium further to the right is a tried and true synth ... |
21-7-2014 at 14:35 by: FireLion3 |
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA? Good point.
I actually managed to find some DBDMH online. Sold under chlorine free "Brilliance S ... |
21-7-2014 at 02:07 by: FireLion3 |
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA? That's interesting, thank you, though, if I could get the bromine then I could skip the need for thi ... |
20-7-2014 at 22:00 by: FireLion3 |
DBDMH / 1,3-Dibromo-5,5-dimethylhydantoin - OTC USA? I recently learned about this as an exciting alternative to NBS. I remember glimpsing a similar comp ... |
20-7-2014 at 21:29 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? [rquote=339111&tid=31843&author=mnick12]Well conversion is different than yield, as you seem ... |
20-7-2014 at 20:23 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? Thanks for the reply. I wasn't attempting to take my frustration out on the community, just became r ... |
20-7-2014 at 17:38 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? Are you intentionally going out of your way to twist my words and make fallacious statements? Please ... |
20-7-2014 at 16:00 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? While that sort of reasoning is true in many reactions, it should be close to negligible in a reacti ... |
20-7-2014 at 15:21 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? How can there be excess bromine? When I stop stirring, the bromine sinks to the bottom, when I start ... |
20-7-2014 at 14:49 by: FireLion3 |
Oxone Aromatic Halogenation in Water - Is this write-up a lie? I know, the title sounds stupid, but I don't really have much of an explanation here. This is my 4th ... |
20-7-2014 at 13:38 by: FireLion3 |
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex If Nickel II Chloride is soluble in both alcohol and water, I didn't think excess water would be an ... |
20-7-2014 at 11:12 by: FireLion3 |
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex I didn't see that concentration there. I do know I can get some pretty high purity acetone at anothe ... |
19-7-2014 at 20:11 by: FireLion3 |
Issue forming Bis(triphenylphosphine)nickel chloride coordination complex This is the complex:
https://en.wikipedia.org/wiki/Bis%28triphenylphosphine%29nickel_chloride
I ... |
19-7-2014 at 19:59 by: FireLion3 |
Benzene from Sodium Benzoate - Dry distillation required? Why? That makes sense. I was hoping to make reasonable quantities of Benzene from Benzoate without having ... |
14-7-2014 at 09:17 by: FireLion3 |
Benzene from Sodium Benzoate - Dry distillation required? Why? I was looking at these preps and they all talk about dry distilling benzene from Sodium Benzoate and ... |
14-7-2014 at 08:41 by: FireLion3 |
Thermoelectric Cooling Mantle? I was thinking recently about endothermic and exothermic reactions. It's generally use to just turn ... |
10-7-2014 at 10:02 by: FireLion3 |
Is there a general rule about stirring rate & reaction speed like there is for temperature? [rquote=337740&tid=31483&author=ziqquratu][rquote=337734&tid=31483&author=FireLion3] ... |
9-7-2014 at 18:35 by: FireLion3 |
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