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Protecting groups for tertiary amines
Amazing! Thank you for all the helpful replies!
Time to hit the books  |
6-7-2021 at 16:24
by: Monoamine |
Protecting groups for tertiary amines
Greetings!
I was wondering if any of you have some input about a problem for a synthesis I'm fac ... |
6-7-2021 at 11:13
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662204&tid=157640&author=S.C. Wack]Read the literature, room temp in this case US361 ... |
27-6-2021 at 09:51
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662130&tid=157640&author=Keras]There’s a chapter about that in the book [i]Small S ... |
26-6-2021 at 12:45
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662147&tid=157640&author=Bedlasky][rquote=662128&tid=157640&author=Monoamine ... |
26-6-2021 at 12:35
by: Monoamine |
16 oz of nitroethane. Buy or nah?
[rquote=661276&tid=157565&author=chemist1243]I found 16oz of nearly pure nitroethane in the ... |
25-6-2021 at 12:26
by: Monoamine |
Thionly chloride from batteries
[color=Red]Warning: Thionyl chloride produces toxic SO2 gas and HCl gas. User discretion is advised. ... |
25-6-2021 at 10:14
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662125&tid=157640&author=rockyit98]Sodium react with hydrogen to produce sodium hydr ... |
24-6-2021 at 19:57
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662119&tid=157640&author=njl]I was more familiar with sodium hydride's deprotonation ... |
24-6-2021 at 16:18
by: Monoamine |
Preparation of NaH from sodium metal.
[rquote=662116&tid=157640&author=karlos³][rquote=662115&tid=157640&author=Monoamine ... |
24-6-2021 at 15:57
by: Monoamine |
Preparation of NaH from sodium metal.
[color=Red](Disclaimer: Elemental Na as well as NaH are highly reactive in air and can spontaneously ... |
24-6-2021 at 10:39
by: Monoamine |
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors
[rquote=661717&tid=157590&author=Opylation]If you’re looking for a phenolic dealkylation p ... |
22-6-2021 at 08:57
by: Monoamine |
Maybe vitamin C is better for reducing Br2 than sodium thiosulfate after all...
On the other hand sodium thiosulfate (Na[sub]2[/sub]S[sub]2[/sub]O[sub]3[/sub]) may not be the best ... |
21-6-2021 at 19:51
by: Monoamine |
Avoiding over nitration (or generally over-electrophilic substitution)
[rquote=661954&tid=157621&author=DraconicAcid]I suspect that plenty of para will dissolve in ... |
21-6-2021 at 12:20
by: Monoamine |
Purification procedure.
Ok, after some research I think that the best way to separate the ortho and the meta product is by f ... |
20-6-2021 at 16:39
by: Monoamine |
Avoiding over nitration (or generally over-electrophilic substitution)
[rquote=661948&tid=157621&author=Boffis]Use only a small molar excess of nitric acid that sh ... |
20-6-2021 at 15:25
by: Monoamine |
Avoiding over nitration (or generally over-electrophilic substitution)
I'm interested in making the para nitro benzoic acid. The generally accepted reaction is below, but ... |
20-6-2021 at 12:26
by: Monoamine |
What does "drying over" some desiccant mean?
[rquote=661906&tid=157617&author=Texium]Drying over means putting the desiccant into the sol ... |
20-6-2021 at 12:18
by: Monoamine |
How to get Hydrobromic acid (HBr) from Br2
[rquote=504187&tid=79859&author=hardik22] I want to get HBr 48% w/w from Br2 ...
what is th ... |
20-6-2021 at 12:05
by: Monoamine |
How to get Hydrobromic acid (HBr) from Br2
[rquote=661915&tid=79859&author=draculic acid69][rquote=504319&tid=79859&author=Melg ... |
20-6-2021 at 11:56
by: Monoamine |
Any thoughts on whether the following might work?
Generate Br2 by dripping H2SO4 into NaBr (or KBr) (not in solution, just the dry salt).
If you are ... |
19-6-2021 at 17:55
by: Monoamine |
Interesting method!
[rquote=504648&tid=79859&author=Dope Amine]To get HBr/acetic acid I just add NaBr and phosph ... |
19-6-2021 at 17:19
by: Monoamine |
What does "drying over" some desiccant mean?
First let me apologize for this noob question, but I haven't been able to find a clear answer anywhe ... |
19-6-2021 at 16:40
by: Monoamine |
Errata
So for some reason, the system won't let me correct the original post, so consider this the errata t ... |
13-6-2021 at 08:48
by: Monoamine |
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors
[rquote=661625&tid=157590&author=Amos]I mean, I can appreciate that you worked hard on this, ... |
12-6-2021 at 14:17
by: Monoamine |
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