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Zinc voltammetry: some problems
It is possible that the zinc plate is covered on oxide and should be polished? (from your pictures)
...
7-2-2023 at 11:28
by: RU_KLO
Purification of Cobalt solution (sulphate/Chloride)
Hi,

alter leaching from Li-Ion Bateries, Ive got a lot of Cobalt hydroxide (green precipitate tha ...
6-1-2023 at 09:08
by: RU_KLO
PbO2 purification
I want Pb02 as pure as posible starting from PbO2 from batteries.
30-12-2022 at 04:08
by: RU_KLO
PbO2 purification
Hi,
Im trying to purify PbO2 taken from batteries.
Did not find anything in Internet. And as it i ...
29-12-2022 at 07:26
by: RU_KLO
Permanganates
No, did not heat it.

here are some (bad) pics - taken from a video.

the first pic: trying to m ...
28-12-2022 at 04:49
by: RU_KLO
Making Chromium salts fron Chromates
[rquote=679717&tid=159171&author=sceptic][rquote=679715&tid=159171&author=blogfast25 ...
25-12-2022 at 11:14
by: RU_KLO
Making Chromium salts fron Chromates
[rquote=679702&tid=159171&author=sceptic][rquote=679684&tid=159171&author=RU_KLO]

...
23-12-2022 at 04:15
by: RU_KLO
Making Chromium salts fron Chromates
Hi,

I want to make different Chromium salts (Chlorides, Carbonates, Sulphates), starting from Pot ...
22-12-2022 at 10:16
by: RU_KLO
Portable DC source for electric arc-Ruby synthesis by the Henry Moissan method
1st: Im no Engineer, but do electronics as hobby from the last 30 years. mostly below 5 Amp circuits ...
22-12-2022 at 09:55
by: RU_KLO
TESTED MnSO4 + PbO2
the main Idea was:

2 MnSO4 + 5 PbO2 + 3 H2SO4 → 2 HMnO4 + 5 PbSO4 + 2 H2O

HMnO4 + KOH -> ...
19-12-2022 at 07:14
by: RU_KLO
Ammonium Persulfate to Ammonium sulfate
Hi,

I need ammonium sulfate and have an excess of Persulfate.

I know that ammonium sulfate is ...
6-12-2022 at 08:06
by: RU_KLO
Lead Nitrate to Lead Chloride
Hi,

I need Lead Chloride (not reagent grade, but with the less contamination as possible)

As t ...
3-12-2022 at 16:14
by: RU_KLO
Testing Ion Exchange Membrane
Im starting with electrolysis (as with Chemistry as well)

After checking several videos on YT, I ...
25-11-2022 at 11:39
by: RU_KLO
H2 trap
Currently a marmelade jar half full of iron? (probably not pure) nails. Did not weight it.

But i ...
20-11-2022 at 10:08
by: RU_KLO
H2 trap
Currently im dissolving some metals with HCl.

Im doing this inside (no fume hood) (-I know is not ...
20-11-2022 at 03:56
by: RU_KLO
Cobalt chloride making
From Wiki: Cobalt chloride heptahydrate can be synthesized by reacting two moles of hydrochloric aci ...
8-11-2022 at 12:33
by: RU_KLO
Can oxone oxidise MnSO4 to MnO2 ?
@DraconicAcid,

most leacheates from Li ion batteries have/could contain.
Mn, Ni, Co and Li.

I ...
4-11-2022 at 10:22
by: RU_KLO
Ammonium hydroxide titration
So, rounding up:

Ammonia in flask, diluted to 0.1M (roughly estimated) + methyl orange
HCl in Bu ...
2-11-2022 at 05:38
by: RU_KLO
Ammonium hydroxide titration
@ Bedlasky, roughly density 0,95 which corresponds to 15% (from an internet table. No analytical sca ...
2-11-2022 at 03:14
by: RU_KLO
Ammonium hydroxide titration
Thanks,

ordered Methyl Orange for standarization (read somewhere) of HCL. Did not know that also ...
1-11-2022 at 10:49
by: RU_KLO
Ammonium hydroxide titration
Made some Ammonium hydroxide, and want to titrate to know its concentration.

after reading, its s ...
1-11-2022 at 06:05
by: RU_KLO
Ammonium Persulfate decomposition
woelen thanks,

Tried and learned about ammonia suckback....

31-10-2022 at 06:03
by: RU_KLO
Ammonium Persulfate decomposition
Thanks, I know that buying new reagents is always a solution. but currently the only ammonium salt ...
30-10-2022 at 05:24
by: RU_KLO
Ammonium Persulfate decomposition
Hi,

regarding Wiki:

When heated to 120°C, ammonium persulfate decomposes releasing sulfur oxi ...
29-10-2022 at 17:24
by: RU_KLO
Glacial Acetic Acid from Sodium Bisulfate + Sodium Acetate - No Yield?
Is it possible to remove last traces of water in a dessicator bag (anhydrous NaOH, anhydrous CaSO4). ...
25-10-2022 at 10:15
by: RU_KLO
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