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5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends Wow, amazing work Niklas! This might be one of the nicest looking documentations of this synthesis. ...	7-2-2025 at 14:42 by: BAV Chem
Diethylether (sulfuric acid saving method) [rquote=694377&tid=160329&author=bnull] No. As explained in the second paper by Senderens ( ...	30-7-2024 at 01:06 by: BAV Chem
Extremely dangerous and inadvisable method for producing nitrite esters (Split from "Preparation of ionic nitrites") As far as I know the copper itself acts as the reducing agent in this reaction. The HCl liberated ...	26-7-2024 at 14:58 by: BAV Chem
Extremely dangerous and inadvisable method for producing nitrite esters (Split from "Preparation of ionic nitrites") [rquote=694243&tid=52&author=Master Triangle] Can't recall what their reference was, but I ...	21-7-2024 at 03:43 by: BAV Chem
Diethylether (sulfuric acid saving method) We might not even need to search for an alternative catalyst although admittedly that would be a ver ...	20-7-2024 at 15:03 by: BAV Chem
The simplest preparation of sulfuric acid?! This method of producing sulfuric acid might be quite laborious but it seems to scale up remarkably ...	20-7-2024 at 14:52 by: BAV Chem
A successful semi-automated ether preparation and an exercise in tar chemistry So apparently the process described by Diachrynic does not work for everyone so far. I've done the p ...	13-7-2024 at 05:53 by: BAV Chem
Diethylether (sulfuric acid saving method) [rquote=693134&tid=160329&author=Keras][rquote=693133&tid=160329&author=Jenks]Phosph ...	7-6-2024 at 01:09 by: BAV Chem
Glyoxal extraction from an OTC product Some time ago I came across an OTC product that apparently contains glyoxal. It's some sort of clean ...	1-11-2023 at 05:00 by: BAV Chem
Acetic anhydride preparation [rquote=653821&tid=9&author=dicyanin] GB299342 looks interesting as sodium metaphosphates ...	9-4-2023 at 15:44 by: BAV Chem
unconventional sodium Well that didn't work. Some traces of sodium are produced but it seems to quickly react with the for ...	25-7-2022 at 03:29 by: BAV Chem
Electrolysis of molten sodium formate Reading through this thread there was at one point the idea of electrolyzing molten carboxylic acid ...	15-7-2022 at 12:19 by: BAV Chem
Synthesis Sodium Ferrocyanide? @CharlesWood As boffis already said you might want to check this out: https://www.sciencemadness ...	13-7-2022 at 22:56 by: BAV Chem
Extremely dangerous and inadvisable method for producing nitrite esters (Split from "Preparation of ionic nitrites") [rquote=674393&tid=77186&author=Antiswat]i did a run where i used 100ish mL of HNO3 and mayb ...	20-6-2022 at 02:54 by: BAV Chem
Synthesis of sodium thiocyanate. Hello Boffis, I know I can actually order some thiocyanate on amazon rather easily but I'm still try ...	6-5-2022 at 16:00 by: BAV Chem
Thiocyanate from NaCN and sulfur I'm currently trying to make thiocyanate by refluxing a solution of NaCN over sulfur. My cyanide is ...	30-4-2022 at 13:41 by: BAV Chem
A particularly bad week (or two) So over the past two weeks I've somehow been very clumsy. For one I made some nitrotetrazole ove ...	26-3-2022 at 01:56 by: BAV Chem
Preparation of ionic nitrites It makes sense to run the reaction under alkaline conditions but doesn't that happen on its own with ...	18-3-2022 at 09:13 by: BAV Chem
Preparation of ionic nitrites [rquote=672065&tid=77186&author=Lionel Spanner]I may well be very late to the party, but has ...	18-3-2022 at 00:10 by: BAV Chem
Nitrate reduction via starch Over the past few weeks of playing around with this reaction I came up with the following procedure: ...	12-3-2022 at 08:22 by: BAV Chem
Reducing surface coating of CuO to metal A hot solution of glucose and sodium hydroxide works for reducing Cu(I) oxide to Cu metal and it sho ...	24-2-2022 at 05:37 by: BAV Chem
OMG some people can still buy sodium nitrite on the internet The stones of a lot of fruit release cyanide when metabolized. Enough to harm oneself. Are they gonn ...	23-2-2022 at 07:14 by: BAV Chem
How to make manganese dioxide electrodes [rquote=663517&tid=156747&author=mysteriusbhoice] thats what happens if you run at high o ...	7-8-2021 at 08:15 by: BAV Chem
How to make manganese dioxide electrodes That's exactly what I thought too but running any current through it with it as the anode only resul ...	1-8-2021 at 23:16 by: BAV Chem
Electrochemical etching of titanium using oxalic acid Normally Ti is etched using HCl before depositing the MnO[sub]2[/sub]. However this method does use ...	1-8-2021 at 15:18 by: BAV Chem
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