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NaClO from TCCA
NaOCl solutions always contain NaCl, they are always made frome chlorine and NaOH.
21-9-2023 at 05:26
by: Bedlasky
HEY GUYS whats a chemical like this?
Holy shit, I didn't know that DCM can be that dangerous!

Once I accidentaly spilled some DCM on t ...
21-9-2023 at 05:25
by: Bedlasky
NaClO from TCCA
Make chlorine generator from TCCA and HCl, than bubble Cl2 in to the cold NaOH solution.
14-9-2023 at 10:44
by: Bedlasky
Dissolving Molybdenum in hypochlorite bleach
Reaction with sulfuric acid give you solution of molybdic acid. Solubility of molybdic acid is accor ...
1-9-2023 at 14:54
by: Bedlasky
Dissolving Molybdenum in hypochlorite bleach
Oh, I didn't know that it was used as analytical method! Do you have some of these papers?
1-9-2023 at 10:30
by: Bedlasky
Dissolving Molybdenum in hypochlorite bleach
It could possibly containt water of crystallization. I didn't found anything about it, but precipita ...
30-8-2023 at 16:03
by: Bedlasky
Dissolving Molybdenum in hypochlorite bleach
Interesting result! I once tried reaction between molybdenum powder and 4% NaOCl in the test tube, b ...
29-8-2023 at 13:46
by: Bedlasky
Introducing myself - new member
Welcome to the forum Ergo Storm!
26-8-2023 at 18:13
by: Bedlasky
Chemical Testing Questions
[rquote=686667&tid=159798&author=Sulaiman]This could be a great adventure and extremely educ ...
16-8-2023 at 08:06
by: Bedlasky
Chemical Testing Questions
Determination of sodium:

1. Gravimetric determination as NaZn(UO2)2(CH3COO)9.6H2O

[url]https:/ ...
14-8-2023 at 13:10
by: Bedlasky
Help with crystallising monopotassium glutamate
I don't know, NaOH with less water would be probably better.
5-8-2023 at 10:05
by: Bedlasky
Help with crystallising monopotassium glutamate
[rquote=686294&tid=159765&author=SplendidAcylation]

Sodium hydroxide granules are also a ...
4-8-2023 at 10:39
by: Bedlasky
Preparation of Ammonium iron (III) sulphate (ferric alum)
Jamit: The colour change is due to loss of water, not due to oxidation. Ammonium ferric sulfate is v ...
29-7-2023 at 12:01
by: Bedlasky
Selenium chemistry in HCl
If I needed pure HBr, I would heat H3PO4 with KBr. I just needed something quick and simple, so I us ...
23-7-2023 at 03:59
by: Bedlasky
Selenium chemistry in HCl
Today I tried reaction between sodium selenate and 48% HBr. This produce orange solution of SeOBr2.H ...
23-7-2023 at 02:46
by: Bedlasky
ethanol self-condensation
I repeated experiment today, this time using more soluble KOH and 4 h reaction time. I dissolved sam ...
23-7-2023 at 00:42
by: Bedlasky
ethanol self-condensation
I decided to check if EtOH is truly oxidized by O2 in alkaline environment to acetaldehyde. I used S ...
21-7-2023 at 23:14
by: Bedlasky
Lead compounds to Lead chloride, desulfurization and more
Do you have equipment to do titration or gravimetry to analyse your product?
21-7-2023 at 18:42
by: Bedlasky
Introducing Myself
Welcome to the forum, Pentaborane! I am looking forward to you projects!
20-7-2023 at 14:24
by: Bedlasky
ethanol self-condensation
I have some ketone free EtOH (denaturated with heptane, Et3N and denatonium benzoate, so this should ...
19-7-2023 at 07:56
by: Bedlasky
Selenium polycations
Selenite reacts with thiosulfate to form selenopentathionate:

[url]https://cdnsciencepub.com/doi/ ...
18-7-2023 at 06:24
by: Bedlasky
Selenium polycations
It's possible, I didn't check if oxidation proceed to IV or VI oxidation state.
16-7-2023 at 15:02
by: Bedlasky
Selenium chemistry in HCl
[rquote=685774&tid=159731&author=j_sum1]I don't have much to say except that you should watc ...
15-7-2023 at 18:55
by: Bedlasky
Selenium polycations
Here is another set of experiments.

Dissolve small amount of NaNO3, K2S2O8 and NaClO3 in 96% sulf ...
15-7-2023 at 18:47
by: Bedlasky
Selenium chemistry in HCl
Hi.

I played today with selenium chemistry in HCl. I followed these two papers:

[url]https://s ...
15-7-2023 at 10:38
by: Bedlasky
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