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Large scale plastic waste PBT plastic hydrolysis experiment @ Hexabromobenzene; these were interesting experiments! I have carried out a fair amount of work on ... |
23-2-2023 at 02:18 by: Boffis |
Mysterious DEET insect-repellent formulation Hi SplendidAcylation; Were you using a flat bottom flask (conical or otherwise) on a flat hotplate? ... |
22-2-2023 at 13:59 by: Boffis |
Calcium pyruvate to sodium pyruvate or pyruvic acid As pointed out above by several posters calcium pyruvate is now a fairly readily available food supp ... |
15-2-2023 at 14:22 by: Boffis |
Replacement for acetonitrile in oxone oxidation Does anyone have any idea if this method would work on conjugate dienes like sorbic acid and piperin ... |
22-1-2023 at 02:41 by: Boffis |
Synthesis of malonic acid Hi kmno4. I haven’t replied to this thread earlier as when at home over the Christmas period I was ... |
19-1-2023 at 13:05 by: Boffis |
Can DCM act as a Lewis Acid? If you have washed the reaction mixture with water then the AlCl3 will have hydrolysed and perform n ... |
20-12-2022 at 01:15 by: Boffis |
DNP synthesis Firstly EvlRenne; from where did this procedure come? Phenol nitrates easily to the mononitro compou ... |
20-12-2022 at 01:08 by: Boffis |
Nitroguanidine reduction product Is the stuff floating in the red liquor actually red or just the solution? I checked out Richter vol ... |
16-12-2022 at 09:53 by: Boffis |
Nitroguanidine reduction product Under rather specific conditions with conventional reducing agents it is possible to reduce some nit ... |
16-12-2022 at 05:50 by: Boffis |
Analogs of haloform reaction? @Falvin, if you want to get useful responses to a post you need to put a bit more effort into your p ... |
14-12-2022 at 05:11 by: Boffis |
Caffeine: reducing the keto-groups to alkanes If you check out libgen there are a series of books on heterocyclic compounds and there are at least ... |
14-12-2022 at 00:30 by: Boffis |
Preparation of chlorosulfonic acid derived protecting groups I have a real hard-copy book on naphthalene chemistry. Throughout the book it describes the preparat ... |
3-12-2022 at 13:45 by: Boffis |
Hydrazine Hydrate turning yellow You need to be more specific with you details! How does IPA (= isopropyl alcohol I presume) free bas ... |
3-12-2022 at 04:03 by: Boffis |
allyl alcohol Has anyone thought about trying this reaction with higher poly-hydroxyalkanes and sugar alcohols suc ... |
30-11-2022 at 03:32 by: Boffis |
Bromination of 1,3 benzodioxole to 5-Bromo-1,3-benzodioxole? Hi Pumikli, I think the difference in the numbering is due to the fact it is regarded as a benzo-het ... |
29-11-2022 at 06:30 by: Boffis |
haloform reaction - cinnamic acid from benzylideneacetone Hi Fery et al. While I haven't tried this reaction on benzalacetone type substrates I have recently ... |
27-11-2022 at 12:10 by: Boffis |
1,2,3,4-tetrahydrocarbazole [rquote=678466&tid=159074&author=Fery]Hi Boffis, the experiment was for the beauty of chemis ... |
21-11-2022 at 11:57 by: Boffis |
2,2'-Bipyridine synthesis Hi Diachrymnic, nice write up once again and I like your make-shift retort from copper pipe and fitt ... |
21-11-2022 at 11:48 by: Boffis |
Pyrazine Synthesis? Diachrynic; nice write-up; its a pity about the yield. I may have a go at this synthesis myself when ... |
21-11-2022 at 11:02 by: Boffis |
Formic Acid Dehydration Hi Chemist1357; I had this problem once and did some research into upgrading my formic acid and I fo ... |
21-11-2022 at 09:50 by: Boffis |
Interesting route to 4-methoxyphenol @ tyro; nice work and an excellent write-up. There are echoes of this method in benignium's write-up ... |
13-11-2022 at 13:39 by: Boffis |
1,2,3,4-tetrahydrocarbazole @ Fery; nice write-up once again. Any particular reason why you chose tetrahydrocarbazole as your ta ... |
13-11-2022 at 13:38 by: Boffis |
Synthesis of malonic acid I agree with you kmno4 about the mp of the diacetic acid and I find this route rather implausible to ... |
12-11-2022 at 07:46 by: Boffis |
Synthesis of malonic acid Hi kmno4, thankyou for the paper, I haven't seen this one before but I have looked at, and indeed tr ... |
11-11-2022 at 12:15 by: Boffis |
Removing graphite from glass frit filter Have you tried reversing the flow of water through the frit. If this and Piranha solution don't move ... |
11-11-2022 at 09:36 by: Boffis |
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