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Large scale plastic waste PBT plastic hydrolysis experiment
@ Hexabromobenzene; these were interesting experiments! I have carried out a fair amount of work on ... |
23-2-2023 at 02:18
by: Boffis |
Mysterious DEET insect-repellent formulation
Hi SplendidAcylation; Were you using a flat bottom flask (conical or otherwise) on a flat hotplate? ... |
22-2-2023 at 13:59
by: Boffis |
Calcium pyruvate to sodium pyruvate or pyruvic acid
As pointed out above by several posters calcium pyruvate is now a fairly readily available food supp ... |
15-2-2023 at 14:22
by: Boffis |
Replacement for acetonitrile in oxone oxidation
Does anyone have any idea if this method would work on conjugate dienes like sorbic acid and piperin ... |
22-1-2023 at 02:41
by: Boffis |
Synthesis of malonic acid
Hi kmno4. I haven’t replied to this thread earlier as when at home over the Christmas period I was ... |
19-1-2023 at 13:05
by: Boffis |
Can DCM act as a Lewis Acid?
If you have washed the reaction mixture with water then the AlCl3 will have hydrolysed and perform n ... |
20-12-2022 at 01:15
by: Boffis |
DNP synthesis
Firstly EvlRenne; from where did this procedure come? Phenol nitrates easily to the mononitro compou ... |
20-12-2022 at 01:08
by: Boffis |
Nitroguanidine reduction product
Is the stuff floating in the red liquor actually red or just the solution? I checked out Richter vol ... |
16-12-2022 at 09:53
by: Boffis |
Nitroguanidine reduction product
Under rather specific conditions with conventional reducing agents it is possible to reduce some nit ... |
16-12-2022 at 05:50
by: Boffis |
Analogs of haloform reaction?
@Falvin, if you want to get useful responses to a post you need to put a bit more effort into your p ... |
14-12-2022 at 05:11
by: Boffis |
Caffeine: reducing the keto-groups to alkanes
If you check out libgen there are a series of books on heterocyclic compounds and there are at least ... |
14-12-2022 at 00:30
by: Boffis |
Preparation of chlorosulfonic acid derived protecting groups
I have a real hard-copy book on naphthalene chemistry. Throughout the book it describes the preparat ... |
3-12-2022 at 13:45
by: Boffis |
Hydrazine Hydrate turning yellow
You need to be more specific with you details! How does IPA (= isopropyl alcohol I presume) free bas ... |
3-12-2022 at 04:03
by: Boffis |
allyl alcohol
Has anyone thought about trying this reaction with higher poly-hydroxyalkanes and sugar alcohols suc ... |
30-11-2022 at 03:32
by: Boffis |
Bromination of 1,3 benzodioxole to 5-Bromo-1,3-benzodioxole?
Hi Pumikli, I think the difference in the numbering is due to the fact it is regarded as a benzo-het ... |
29-11-2022 at 06:30
by: Boffis |
haloform reaction - cinnamic acid from benzylideneacetone
Hi Fery et al. While I haven't tried this reaction on benzalacetone type substrates I have recently ... |
27-11-2022 at 12:10
by: Boffis |
1,2,3,4-tetrahydrocarbazole
[rquote=678466&tid=159074&author=Fery]Hi Boffis, the experiment was for the beauty of chemis ... |
21-11-2022 at 11:57
by: Boffis |
2,2'-Bipyridine synthesis
Hi Diachrymnic, nice write up once again and I like your make-shift retort from copper pipe and fitt ... |
21-11-2022 at 11:48
by: Boffis |
Pyrazine Synthesis?
Diachrynic; nice write-up; its a pity about the yield. I may have a go at this synthesis myself when ... |
21-11-2022 at 11:02
by: Boffis |
Formic Acid Dehydration
Hi Chemist1357; I had this problem once and did some research into upgrading my formic acid and I fo ... |
21-11-2022 at 09:50
by: Boffis |
Interesting route to 4-methoxyphenol
@ tyro; nice work and an excellent write-up. There are echoes of this method in benignium's write-up ... |
13-11-2022 at 13:39
by: Boffis |
1,2,3,4-tetrahydrocarbazole
@ Fery; nice write-up once again. Any particular reason why you chose tetrahydrocarbazole as your ta ... |
13-11-2022 at 13:38
by: Boffis |
Synthesis of malonic acid
I agree with you kmno4 about the mp of the diacetic acid and I find this route rather implausible to ... |
12-11-2022 at 07:46
by: Boffis |
Synthesis of malonic acid
Hi kmno4, thankyou for the paper, I haven't seen this one before but I have looked at, and indeed tr ... |
11-11-2022 at 12:15
by: Boffis |
Removing graphite from glass frit filter
Have you tried reversing the flow of water through the frit. If this and Piranha solution don't move ... |
11-11-2022 at 09:36
by: Boffis |
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