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What's the most expensive substance you've bought?
Gaboxadol is quite an expensive compound, but not nearly as others out there. It is just one I order ...
4-5-2021 at 20:27
by: ChemichaelRXN
I want to hear your favorite chemistry demonstrations
Oil and vinegar

No just kidding...

I liked the video by ChemicalForce where he mixed carbon di ...
9-4-2021 at 10:24
by: ChemichaelRXN
Got a new RotoVap!
Very nice, I need a nice shiny new one too one of these days...and an HPLC.

I managed to get this ...
2-4-2021 at 07:45
by: ChemichaelRXN
Decarboxylation of L-tryptophan in DMSO
Sorry for the error, for some reason thinking melatonin had that carboxylic acid. You would need 5-M ...
20-3-2021 at 09:49
by: ChemichaelRXN
Decarboxylation of L-tryptophan in DMSO
I was thinking of this same reaction out of a list i want to do.
I have the DMSO, Acetophenone, ace ...
19-3-2021 at 16:26
by: ChemichaelRXN
Rare and hard to obtain chemicals for sale
Great supplier, thank you for the order! Received well in Canada.

Highly recommend and will order ...
1-3-2021 at 12:51
by: ChemichaelRXN
Acid mixtures that dissolve gold
I believe HCl/FeCl3 or FeCl3 alone works too, but never tried it.
23-2-2021 at 14:30
by: ChemichaelRXN
Benzoyl chloride + 4-Aminoadamantan-1-ol
That sounds like a good idea. Any example of this reaction/procedure?
That is a pretty useful comp ...
15-2-2021 at 13:20
by: ChemichaelRXN
Benzoyl chloride + 4-Aminoadamantan-1-ol
I guess the sodium ethoxide pathway would work. I cant find too much on this one though. I will make ...
14-2-2021 at 15:17
by: ChemichaelRXN
Benzoyl chloride + 4-Aminoadamantan-1-ol
Ok, interesting. Overlooked that, thanks. Maybe I can oxidize the amine to a nitro and reduce after ...
14-2-2021 at 15:13
by: ChemichaelRXN
Removing acetone from chloroform
You can add water to separate the chloroform from the solution of acetone, but chloroform is slightl ...
14-2-2021 at 11:37
by: ChemichaelRXN
Benzoyl chloride + 4-Aminoadamantan-1-ol
Hello,

I am going to be producing an esterification product with Benzoyl chloride + 4-Aminoadaman ...
14-2-2021 at 04:48
by: ChemichaelRXN
Acetic Anhydride from Zinc Acetate?
I dont need acetic anhydride, but I was thinking, do you think reacting 2 moles of acetic acid with ...
10-2-2021 at 02:13
by: ChemichaelRXN
Do not buy from laboyglass.com
I have always ordered from Deschem and the quality seems great to be honest.
10-1-2021 at 07:03
by: ChemichaelRXN
Reductions of Nitro groups with Zn and acid
If the reaction works ok, you can extract it with chloroform 1.49g/ml instead of toluene 0.865g/ml, ...
3-1-2021 at 23:09
by: ChemichaelRXN
New organic chemistry youtube video: Making isobutyl bromide
No problem, I messaged you.

Also I tried the sulfurol and HBr reaction in the past, but what I go ...
25-12-2020 at 12:33
by: ChemichaelRXN
New organic chemistry youtube video: Making isobutyl bromide
Nice work! If you want some sulfurol for free to halogenate, let me know. You can convert it to “b ...
25-12-2020 at 05:49
by: ChemichaelRXN
Organometallic liquid gold luster
Different subject a bit, but have you ever melted copper and silver together and make a ring. I made ...
23-12-2020 at 15:46
by: ChemichaelRXN
Formaldehyde bisulfite adduct preparation
Yea maybe rotovap half of the solution not crystallizing or add NaCl to make a brine to reduce the s ...
20-12-2020 at 06:59
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Thanks for talking about it for me to get one. Not too familiar with titanium hydride, maybe sodium ...
15-12-2020 at 15:49
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Mine are 0.6Mpa or 87psi. I guess a hot water bath would be safe enough.

I just bought one too; H ...
14-12-2020 at 16:35
by: ChemichaelRXN
AlCl3 is an alternative to SOCl2
Here is some more info. on TCCA reactions; https://www.organic-chemistry.org/chemicals/oxidations/tr ...
14-12-2020 at 14:49
by: ChemichaelRXN
2,2,7,7-tetramethyloxepane
Yea, it might just work. I recall hearing anything less than the 1,4-dibromobutane would just break ...
13-12-2020 at 09:43
by: ChemichaelRXN
2,2,7,7-tetramethyloxepane
Hello,

Has anyone ever performed a Grignard reaction where you are reacting two halogen groups wi ...
13-12-2020 at 06:59
by: ChemichaelRXN
Benzoyl chloride from benzoic acid
Ok, great, thank you for the info., I appreciate it!
9-12-2020 at 13:04
by: ChemichaelRXN
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