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Trinitrotoluene preparation
I don't have any copies of that site. But I think you are over-crediting that procedure of megaloman ...
21-5-2002 at 16:38
by: Coen
Perchloric acid preparation
You should see that this reaction is thermodynamically not right already.

You can also make HClO4 ...
20-5-2002 at 18:44
by: Coen
Sodium peroxide 8-hydrate
Nice, but not THAT interesting though.
If I remember I still have a bottle of that stuff somewhere. ...
20-5-2002 at 18:14
by: Coen
Acetic anhydride preparation
Although I agree with you that it's quite certain there is atleast some CH3CHO in your product. But ...
20-5-2002 at 18:10
by: Coen
Acetic anhydride preparation
Hmm. This is another one of those industrial processes which have been transformed to home experimen ...
20-5-2002 at 18:09
by: Coen
Acetic anhydride preparation
No, but only if there are no other alternatives. And there ARE in this case.
I will give some more ...
20-5-2002 at 18:07
by: Coen
Acetic anhydride preparation
I am sorry to dissapoint you, but it is not possible to dehydrate acetic acid to Ac2O.

Some time ...
20-5-2002 at 18:05
by: Coen
Hydrofluoric acid
Well, I guess that's possible. But I don't have very much of HF solution. It's maybe a little "clean ...
20-5-2002 at 18:00
by: Coen
Hydrofluoric acid
Yes, this is rather strange. The reaction between CaF2 en H2SO4 is even used commercially sometimes. ...
20-5-2002 at 17:42
by: Coen
Nitric acid stills
I must say I have quite some experience with destillations of nitric acid.

I distill one part of ...
20-5-2002 at 17:11
by: Coen

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