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Can benzaldehyde be saturated with HCl? Can the aldehyde be saturated with HCl? Will it cause any reaction, like self condensation or someth ...	20-11-2015 at 01:43 by: Crypto
Can water/alcohol azeotrope carry compounds during distillation like steam does? Steam can carry some compounds with it. That's steam distillation... What if I distill alcohol from ...	16-1-2015 at 07:44 by: Crypto
N-methylhydroxylamine preparation The procedure is taken from the ,,Laboratory methods of organic chemistry" by L. Gattermann. An a ...	6-1-2015 at 09:17 by: Crypto
Hydrolysis and decarboxylation of nitriles with Phosphoric acid. Can't find any experimental data. [quote] Long time ago I made such an experiment with ketonitrile (mentioned earlier in OS procedure ...	11-12-2014 at 15:36 by: Crypto
Hydrolysis and decarboxylation of nitriles with Phosphoric acid. Can't find any experimental data. [quote] My apology Crypto.[/quote] I didn't feel offended but you're welcome. [quote] ...	11-12-2014 at 12:49 by: Crypto
Hydrolysis and decarboxylation of nitriles with Phosphoric acid. Can't find any experimental data. Well if you would read "Phosphoric Acid: Purification, Uses, Technology, and Economics" by Rodney Gi ...	11-12-2014 at 08:20 by: Crypto
Hydrolysis and decarboxylation of nitriles with Phosphoric acid. Can't find any experimental data. I can't find any experimental data on the hydrolysis and subsequent decarboxylation of nitriles with ...	9-12-2014 at 06:34 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Cu I'm curious how would the system work with imines. I was planning to give it a try but I haven't got ...	12-9-2014 at 22:17 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Cu Apperently Copperman tried it without GAA and got worse results. Maybe just a little is needed. Unfo ...	25-8-2014 at 01:09 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Cu I can confirm that it works. I haven't had luck when I tried to reduce nitromethane but I did reduce ...	24-8-2014 at 13:40 by: Crypto
Some questions about the Al/Hg reduction system. Sorry for such a delay but I was cut off the internet. Here are the references: [url=https://w ...	24-8-2014 at 12:31 by: Crypto
Some questions about the Al/Hg reduction system. The thing with Al is that lots of it does not react. That lead me to think that actually not that mu ...	22-7-2014 at 14:24 by: Crypto
Some questions about the Al/Hg reduction system. Hi. I know there is a lot information about this system here on the forum as well as on other sites. ...	17-7-2014 at 01:47 by: Crypto
Can Marcury(l) Nitrate activate aluminium? I tried to use it and couldn't get it going. Instead of distilling nitric acid I procured some HgCl2 ...	17-7-2014 at 01:26 by: Crypto
Can Marcury(l) Nitrate activate aluminium? Is Hg2(NO3)2 suitable to prepare an Al/Hg amalgam? I know the chloride is best, and that Hg(NO3)2 w ...	6-7-2014 at 01:34 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Ga Any success recovering Ga? I have 10 grams of it just waiting to play with it. Would be nice to recy ...	29-6-2014 at 14:49 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Ga 10g of aluminum per 10g of substrate, but how much amalgam? Let's say someone wants to run the react ...	29-6-2014 at 14:17 by: Crypto
Experimental: Alternative to Al/Hg - the Al/Cu I tried to reduce nitromethane with Al/Cu today. I mixed 20ml of nitromethane with 50ml of IPA and 5 ...	27-6-2014 at 11:36 by: Crypto
Epoxidation of propiophenone Thank you all. I still need to learn a lot... I thought I'll finaly use the propiophenone for someth ...	3-6-2014 at 00:32 by: Crypto
Epoxidation of propiophenone Hi! I stumbled on a nice method for the preparation of styrene oxide posted by Nicodem some time ...	1-6-2014 at 23:57 by: Crypto
Acetaldehyde synthesis After reading the whole thread I must say that the above procedure seems to be the most practical fo ...	17-4-2014 at 12:07 by: Crypto
Acetaldehyde synthesis DoctorZET can you elaborate a bit on your method? What setup have you used and how have you prepared ...	15-4-2014 at 12:47 by: Crypto
Manganese (II) Acetate oxidation to Manganese (III) Acetate Thanks for some ideas Organikum. Can you elaborate a bit on the ammonium nitrate. What procedure wou ...	5-2-2014 at 14:39 by: Crypto
Manganese (II) Acetate oxidation to Manganese (III) Acetate I know Mn(OAc)2 can be oxidized to Mn(OAc)3 with KMnO4. Can other oxidizing agents be used? I saw so ...	4-2-2014 at 16:18 by: Crypto
Solubility of Manganese Acetate salts Hey! My chemistry books haven't got any info about the solubility of Manganese (II) and Manganese ...	26-1-2014 at 03:36 by: Crypto
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