| Search |
| [Next Page] |
Boiling HNO3 plus even hotter cooking oil ?
How about using some form of aluminium media (pellets/beads) for a heating bath? Its unreactive with ... |
22-1-2019 at 08:56
by: DJF90 |
Looking for [2,2'-bithiophen]-5-yltrimethyl-stannane
Searching on eMolecules gives only the bis-stannylated compound as commercially available. You might ... |
13-11-2018 at 04:12
by: DJF90 |
Trying out a stille coupling reaction
It looks like you've neglected to adjust your stoichiometry to account for your change in stannane. ... |
13-11-2018 at 00:01
by: DJF90 |
Trying out a stille coupling reaction
Try these conditions: https://www.organic-chemistry.org/abstracts/literature/681.shtm
...but using ... |
11-11-2018 at 02:27
by: DJF90 |
3D printing Fluropolymer Lab Equipment
This might be useful/interesting in terms of print parameters:
https://www.plastic2print.com/175mm- ... |
1-11-2018 at 02:07
by: DJF90 |
Cobalt (II) Chloride catalysis of ester formation
Nice work AvB. Its not unusual to see methodology such as this in the literature where the claims ar ... |
8-10-2018 at 13:14
by: DJF90 |
Acidic Radicals Based Synthesis
I think you need to run some control experiments in parallel. I would suggest identical mixtures but ... |
25-9-2018 at 09:40
by: DJF90 |
Wanted: 14/23 female to 24/29 male adapter
I sent you a U2U and an email Sulaiman |
24-9-2018 at 23:20
by: DJF90 |
Demethylation of Vanillin and Eugenol
Nice to see you working on a sensible scale. You say the reaction was complete but provide no detail ... |
18-9-2018 at 05:03
by: DJF90 |
TLC help - which solvent system - benzalacetone derivate
Assuming your technique is right (quite difficult to ascertain without a picture), perhaps 9:1 DCM:E ... |
8-9-2018 at 13:57
by: DJF90 |
TLC help - which solvent system - benzalacetone derivate
Thats an equieluotropic table, so it allows you to find different systems of similar solvent strengt ... |
7-9-2018 at 00:38
by: DJF90 |
Diethyl ether on pulic transport
How much, what type of transport, and what region? I'd say a train/tube in London would be quite dif ... |
6-9-2018 at 00:20
by: DJF90 |
Catechol preparation
I too am glad to see you're back in the lab Magpie. I have several queries/suggestions to make, and ... |
1-9-2018 at 04:50
by: DJF90 |
Dissolving unknown metal that may have PGM's
It would be advantageous to take a small sample of each platter, dissolve in whatever affords a homo ... |
29-8-2018 at 02:49
by: DJF90 |
Missing persons
Is anyone in touch with Panache? I sent him a parcel a month ago and it has just been "returned to s ... |
24-8-2018 at 09:15
by: DJF90 |
anhydrous calcium iodide for making calcium
Have you looked in Brauer? |
20-8-2018 at 02:59
by: DJF90 |
Melting sulfur in mineral oil
Sulfur reacts with mineral oil at high temperatures to generate alkenes and hydrogen sulfide. Stick ... |
15-8-2018 at 12:32
by: DJF90 |
Preparing Grignard Reagents from 3-Bromopropylamine hydrobromide and other Compounds
Assuming the C60 reacts with the grignard but is stable to the subsequent manipulations (fullerene c ... |
13-8-2018 at 11:23
by: DJF90 |
58% EtOH + NaOH = .....
I'm more surprised by the phase separation... I was under the impression that this would form a homo ... |
2-8-2018 at 09:06
by: DJF90 |
IKA ETS-D5 Error 5
Have you set the plate temperature higher than 100 C (by turning the knob). Error 5 in my experience ... |
23-7-2018 at 00:29
by: DJF90 |
IKA ETS-D5 Error 5
I have this error pop up occassionally, but its usually when I've turned heating off on the hotplate ... |
21-7-2018 at 06:40
by: DJF90 |
Does anyone have solubility data of HCl in various solvents (Methanol, Ethanol, Ether)?
100g of methanol has a larger volume than 100g of water due to differences in density. Essentially y ... |
16-7-2018 at 09:18
by: DJF90 |
Does anyone have solubility data of HCl in various solvents (Methanol, Ethanol, Ether)?
This is given on p. 50 of "Purification of Laboratory Chemicals" by Armarego and Perrin (6th Ed.): |
16-7-2018 at 00:19
by: DJF90 |
2,3-dichloropropene synthesis?
http://www.orgsyn.org/demo.aspx?prep=CV1P0209
If the bromide is not suitable, then I suspect the ... |
17-6-2018 at 09:02
by: DJF90 |
Small scale preparation of Stannic Chloride (SnCl4)
You don't need to heat the tin to get it to react. See Brauer in the forum library, p729, for a deta ... |
26-4-2018 at 07:25
by: DJF90 |
| [Next Page] |
