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Preparation of Al(HSO4)3
[quote]
So even if these papers are free of fraud and they correctly described the formula of the ... |
6-10-2021 at 18:06
by: EverythingAl2O3 |
Preparation of Al(HSO4)3
I found the procedure for Al(HSO4)3. It is the same.
A 50 mL suction flask was equipped with a cons ... |
1-10-2021 at 14:29
by: EverythingAl2O3 |
Preparation of Al(HSO4)3
Author directed me to this paper that mentions the preparation of Fe(HSO4)3 and might be the same fo ... |
29-9-2021 at 16:48
by: EverythingAl2O3 |
Preparation of Al(HSO4)3
Sorry to awaken an old thread no one cared about but I have come across a reaction that mentions usi ... |
18-8-2021 at 20:11
by: EverythingAl2O3 |
An attempt at making Phorone
Just an update on the phorone tests. One the left image we see acetone with NH4Cl with no solvent af ... |
17-7-2021 at 06:52
by: EverythingAl2O3 |
Protecting groups for tertiary amines
Is there anything stopping you from doing an acid catalyzed ether synthesis? So you could use H2SO4 ... |
17-7-2021 at 06:20
by: EverythingAl2O3 |
H2S reduction of ketones and aldehydes
[quote]
It's super easy to make H2S but god damn it stinks if you don't deal with it well. I went ... |
19-6-2021 at 06:43
by: EverythingAl2O3 |
H2S reduction of ketones and aldehydes
[quote]
Perfect timing just watched a video about making a hydrogen sulfide generator with candle ... |
16-6-2021 at 19:25
by: EverythingAl2O3 |
H2S reduction of ketones and aldehydes
I found an interesting reduction reaction using H2S/H2S sources like Na2S. It is a photocatalytic re ... |
16-6-2021 at 04:15
by: EverythingAl2O3 |
Acetaldehyde synthesis
Yes it is a bit much for it. Though it seems far more regenerable than using Chromate oxidizers ment ... |
6-6-2021 at 07:19
by: EverythingAl2O3 |
Acetaldehyde synthesis
Have we also considered the Corey-Kim oxidation? N-chlorosuccinimide with a unhindered thioether and ... |
28-4-2021 at 16:56
by: EverythingAl2O3 |
NH4Cl test
So for my initial NH4Cl test I started with 28g NH4Cl, and 100mL Acetone with 100mL water co-solvent ... |
8-3-2021 at 15:12
by: EverythingAl2O3 |
OTC Amine protection?
Are trying to protect a primary or secondary amine? What conditions will your reactant undergo? If i ... |
15-2-2021 at 17:51
by: EverythingAl2O3 |
An attempt at making Phorone
[quote]
If someone likes acetone way to phorone, I would suggest condensation by NaOH or KOH, ins ... |
15-2-2021 at 07:15
by: EverythingAl2O3 |
Have we been "overcooking" our acetals?
In orgo 2 they teach that acetal and imines are water sensitive in acid solutions and will be destro ... |
10-2-2021 at 10:06
by: EverythingAl2O3 |
K2CO3 / KOH from Wood ashes ?
[quote]
I tried to extract soluble salts from wood ash.
I filled one third bucket with ashes from ... |
9-2-2021 at 07:48
by: EverythingAl2O3 |
An attempt at making Phorone
I have finally gotten some NH4Cl and I will be testing the phorone synthesis next break I get from s ... |
9-2-2021 at 06:52
by: EverythingAl2O3 |
An attempt at making Phorone
[quote]
Regarding triacetonamine, you don't need such a complex apparatus if you're willing to to ... |
19-1-2021 at 11:44
by: EverythingAl2O3 |
Possible alternative pathway to phorone
I found this paper in the link that shows the synthesis of triacetoneamine, but the scheme shows pho ... |
17-1-2021 at 07:20
by: EverythingAl2O3 |
An attempt at making Phorone
Honestly did think it was too good to be true but thought it wouldn't hurt to try anyway |
16-1-2021 at 10:54
by: EverythingAl2O3 |
An attempt at making Phorone
[quote]
Hi EverythingAl2O3, I've been following your experimental endeavors with interest as I ha ... |
16-1-2021 at 10:00
by: EverythingAl2O3 |
Carbonate ester synthesis from urea?
[quote]
As discussed in other threads, simple carbonate esters can be made simply from the alcohol ... |
15-1-2021 at 09:08
by: EverythingAl2O3 |
Carbonate ester synthesis from urea?
I know that carbonate esters are typically made from the reaction of phosgene and alcohols. I don't ... |
15-1-2021 at 06:50
by: EverythingAl2O3 |
Phorone update 2 product after acetone addition
So...This did not go anything like it did previously. I added an additional 30mL of acetone after re ... |
14-1-2021 at 14:30
by: EverythingAl2O3 |
Attempt 2 update
I redid the reaction using 100mL of acetone and 100mL 33% HCl and left it overnight at 50C. After st ... |
14-1-2021 at 10:18
by: EverythingAl2O3 |
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