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Some arsenic chemistry
Another great article woelen! And those mineral samples are gorgeous! |
23-12-2020 at 01:56
by: Heptylene |
Need help finding a non flammable low temp boiling liquid
To make an ice/salt bath, the CaCl2 has to be hexahydrate, not the dihydrate usually sold for dehumi ... |
20-12-2020 at 09:13
by: Heptylene |
Violuric acid salts (fantastic colors and variety)
Incredible colors! I'm adding this compound to my todo list
Rubidium would be cool to see as well ... |
17-12-2020 at 02:23
by: Heptylene |
Feasibility of creating a nuclear reactor with the aim of transmutation?
[rquote=651053&tid=156677&author=itsallgoodjames]My goal is to end up with detectable amount ... |
12-12-2020 at 03:17
by: Heptylene |
The insanity that is OHS
Wtf I would just explode if someone told me dissolving magnesium in vinegar is a problem. Is there a ... |
11-12-2020 at 10:37
by: Heptylene |
How do you draw benzene rings?
I do it as below. I don't know if it's a common way or not, but it's the fastest way to produce a re ... |
10-12-2020 at 11:28
by: Heptylene |
How to build a cheap and durable electrolytic cell
It really depends on what you want to do. When I started in the hobby, I used plastic containers, co ... |
3-12-2020 at 02:16
by: Heptylene |
What can cause garlic-like smell ?
Could it be a phosphorus or arsenic impurity in chromium metal? Dissolving metals are a well establi ... |
3-12-2020 at 01:56
by: Heptylene |
What are most dangerous toxic chemicals you are comfortable handling in your home lab?
These are some things I don't want to handle in my lab:
- Anything explosive is out of the question ... |
29-11-2020 at 01:49
by: Heptylene |
Powder addition in reflux?
Perhaps addition of the powder as a slurry in the reaction solvent is possible? |
28-11-2020 at 07:10
by: Heptylene |
Best Way to Prevent Crystals from being Stuck to Glass?
Have you tried boiling down the water while using magnetic stirring? In my experience this makes slu ... |
26-11-2020 at 14:24
by: Heptylene |
Crystallisation - truly a dark art
That was a great read, thanks monolithic! |
21-11-2020 at 04:28
by: Heptylene |
Crystallisation - truly a dark art
I've had non-reproducible crystallisations with 4-nitrobromobenzene. First time, the crude product p ... |
20-11-2020 at 09:13
by: Heptylene |
Just arrived API 365 Triple Quadrupole Mass Spectrometer
+1 for pictures, vacuum equipment is always delightful to see!
You orignially bought it for its p ... |
19-11-2020 at 05:41
by: Heptylene |
Anschütz-Thiele receiver/fraction cutter
I just got an Anschütz-Thiele receiver, which is the german version of the Perkin triangle. I've be ... |
18-11-2020 at 09:23
by: Heptylene |
Removal of vapor duct Büchi R-114
If you can sacrifice the metal part, I would dissolve it in HCl to avoid breaking the glass. |
16-11-2020 at 06:55
by: Heptylene |
Everyday Chemistry
Oh Arkoma I feel for you, pepper extract is a bitch to work up. I've done it 3 or 4 times and everyt ... |
14-11-2020 at 09:59
by: Heptylene |
Everyday Chemistry
I distilled some fuming nitric acid this afternoon! I decided to go with a relatively small scale: 2 ... |
14-11-2020 at 07:18
by: Heptylene |
How to cut 1oz silver bar into pieces that will fit in a test tube
A chisel will work for a 1oz bar for sure. Be sure to choose the right kind of chisel (for metal). O ... |
31-10-2020 at 09:20
by: Heptylene |
Oil lock up of rotary vane vacuum pumps
Glad to know oil-filled machinery is not an issue  For me it was a first.
I don't use the pump ... |
20-10-2020 at 00:20
by: Heptylene |
Oil lock up of rotary vane vacuum pumps
Hmm, I wish I had known about this issue a few months ago.
I recently acquired a Leybold D10E rot ... |
19-10-2020 at 12:55
by: Heptylene |
Cheap solvent pump that will not dissolve itself?
A syringe pump maybe? Though I must admit your exact requirements aren't clear to me. What exactly a ... |
19-10-2020 at 12:29
by: Heptylene |
Chemical containers?
I use a lot of 1000 ml GL45 bottles for liquids. They are great and don't leak much. I store all my ... |
15-10-2020 at 00:46
by: Heptylene |
PTFE / Teflon labware inclusions - normal or not?
Maybe you can sand the inside and dissolve whatever the inclusions are? Though you would need very t ... |
6-10-2020 at 13:23
by: Heptylene |
For those distilling at home, how do you feed water into your condenser?
At first I used water from the tap, but it's pretty wasteful. Then I moved to using a 10 liter bucke ... |
5-10-2020 at 03:02
by: Heptylene |
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