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Purification of drain-cleaner acid
Hey Folks,

My local store sells "Liquid Lighting Virgin Sulfuric Acid Drain Cleaner", which is 93 ...
25-1-2022 at 17:56
by: JacobM
Handling of Aniline
Ah, I think I have one I can wear somewhere. If I can find it I'll use it.
18-1-2022 at 05:44
by: JacobM
The Preparation of Benzotriazole
I didn't bother a second recryst because it was getting late and I tried seeding it, but that didn't ...
18-1-2022 at 05:27
by: JacobM
Handling of Aniline
Thanks, I'll make sure that I do that.
17-1-2022 at 14:50
by: JacobM
Handling of Aniline
I'm going to wait for the ABEK cartridges I ordered to arrive before I do it. That should probably h ...
17-1-2022 at 14:49
by: JacobM
Handling of Aniline
B(a)P: Thanks. I'm only working with about 2-5ml aniline at one time, and I do believe that my venti ...
17-1-2022 at 14:33
by: JacobM
Toxicity of Aniline

Hi All,

I am considering an experiment that involves handling freebase aniline. I'm concerned a ...
17-1-2022 at 14:05
by: JacobM
Handling of Aniline
Hi All,

I am considering an experiment that involves handling freebase aniline. I'm concerned abo ...
17-1-2022 at 13:16
by: JacobM
The Preparation of Benzotriazole
I didn't read the orgsyn method thoroughly enough apparently. Thanks, Fery.

[Edited on 17-1-2022 by ...
17-1-2022 at 04:29
by: JacobM
The Preparation of Benzotriazole
I just finished a synthesis of benzotriazole, which doesn't appear to have any preparations here. I ...
16-1-2022 at 07:41
by: JacobM
S-Isopropylisothiouronium bromide
This is definitely an interesting piece of work here.
15-1-2022 at 05:58
by: JacobM
Methyl salicylate and wintergreen oil
I bought wintergreen essential oil, Gaultheria procumbens, and GC/MS reports from various sources gi ...
14-1-2022 at 07:49
by: JacobM
Easy-to-synthesize odor compounds
Fery: Piperonal has been on my list for a while...ozonolysis of piperine.

clearly_not_atara: That ...
14-1-2022 at 04:46
by: JacobM
Methyl salicylate and wintergreen oil
I'm wondering if wintergreen oil can be used to substitute methyl salicylate in a protocol that call ...
14-1-2022 at 03:33
by: JacobM
Easy-to-synthesize odor compounds
I've read the same reference - but who has CF3CO2H? I don't, and I really don't want to work with it ...
9-1-2022 at 14:56
by: JacobM
Easy-to-synthesize odor compounds
Yeah, I'll get that.

One more thing: can dilute (50-80%) H2SO4 be used to form butyl bromide from ...
8-1-2022 at 18:54
by: JacobM
Easy-to-synthesize odor compounds
Thanks, that might help.
8-1-2022 at 18:08
by: JacobM
Easy-to-synthesize odor compounds
Terpineol is also an option, however I haven't had the best luck with it. I've purchased 1/2 litre o ...
8-1-2022 at 14:46
by: JacobM
Procurement of Phenol
Like whom?
8-1-2022 at 13:41
by: JacobM
Procurement of Phenol
I've thought of doing this. However I can only find liquid phenol on Ebay of a decent purity. Liquid ...
8-1-2022 at 12:51
by: JacobM
Easy-to-synthesize odor compounds
Texium,

Well shows how much I know about US drug law. I thought it would be controlled because it ...
8-1-2022 at 12:28
by: JacobM
Procurement of Phenol
I need a fair bit of phenol (25g) for an upcoming experiment on the Bargellini reaction. I have made ...
8-1-2022 at 12:24
by: JacobM
Easy-to-synthesize odor compounds
Tsjerk, that's what I did. I guess it was the distillation after all?

Thanks for all of the sugge ...
8-1-2022 at 09:55
by: JacobM
Easy-to-synthesize odor compounds
Okay. I might have to try it.

To be honest I have had some success with aryl esters. I made methy ...
8-1-2022 at 05:33
by: JacobM
Easy-to-synthesize odor compounds
That looks interesting, but I find that alternative catalysts don't work well for me.
I think the r ...
8-1-2022 at 04:58
by: JacobM
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