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Boronic acids
There's an ACS review on boron compounds that contains a section on boronic acids. That might be a g ...
2-2-2019 at 20:23
by: JnPS
bromobenzene
Do you have an estimate of the mass of iron you added? I'm running a similar reaction using AlBr3/Br ...
23-1-2019 at 10:40
by: JnPS
Starting from benzene...
Is this a school assignment or a synthetic scheme you wish to carry out? Cause I don't see why you w ...
27-6-2018 at 05:52
by: JnPS
Living the Chemistry Dream
I'm at an REU this summer at a university working under a post-doc and grad student. I had pretty mu ...
25-6-2018 at 15:10
by: JnPS
Modified Wolff-Kishner
Thanks for the replies!

@Metacelsus - The third to last step in that mechanism though, where the ...
19-5-2018 at 09:48
by: JnPS
Modified Wolff-Kishner
TL;DR: Will the first transformation in the attached picture work to remove the C=O?

Last semeste ...
18-5-2018 at 09:37
by: JnPS
OTC Oxalyl Chloride Challenge
Already looking up old patents and bugging professors for copies of ancient ACS articles, I'll be on ...
21-5-2017 at 14:38
by: JnPS
37% hydrochloric acid
If you have drain cleaner grade sulfuric acid and table salt you can make a simple HCl(g) generator ...
24-4-2017 at 11:26
by: JnPS
Selling a bunch of stuff
What do you have left? My semester will be over after this week so I would have time to drive down a ...
20-4-2017 at 05:26
by: JnPS
Report on Decarboxylation of Tryptophan in various solvents
[rquote=337520&tid=31306&author=mnick12]Okay this may be a silly question, but wouldn't the ...
17-4-2017 at 07:53
by: JnPS
How do you interpret NMR readings?
@Metacelsus Doh! *facepalm* Thanks for the correction, that's what I get for posting when I should h ...
17-4-2017 at 03:18
by: JnPS
Packet Desicants
Just curious if anyone has ever tried using those silica gel packets as a poor chemist's drying agen ...
16-4-2017 at 18:37
by: JnPS
How do you interpret NMR readings?
Just google how to read NMR spectra, It's not terribly difficult. They usually teach it to undergrad ...
16-4-2017 at 18:32
by: JnPS
Regarding the haloform reaction
The problem with using Ca(OCl)2 is the calcium salt that forms as a byproduct usually forms a slush ...
3-4-2017 at 11:06
by: JnPS
The Short Questions Thread (4)
Can somebody download/share this article?

α,β-Unsaturated Aminoketones. VIII.1 Reaction of Pri ...
9-3-2017 at 20:18
by: JnPS
Elementary Work on Schiff Bases
[u][b]Workup of Previous Procedures[/b][/u]

[b]N-Benzylideneaniline Recrystallization[/b]
Althou ...
9-3-2017 at 19:27
by: JnPS
amide group oxidation
Amides are not very reactive. I have never heard of it being possible to oxidize them to a nitro gro ...
4-3-2017 at 07:57
by: JnPS
5-Oxo-2-tetrahydrofurancarboxylic acid (butyrolacton-5-carboxylic acid) from glutamic acid
Beautiful writeup, neat experiment, I'll definitely add this to my ever growing to-do list.

Why ...
4-3-2017 at 07:24
by: JnPS
can i do make bromoethane using methylated spirits
Aren't methylated spirits a mixture of methanol/ethanol? You'd get bromoethane, but also methyl brom ...
3-3-2017 at 12:40
by: JnPS
The Short Questions Thread (4)
[rquote=476494&tid=25055&author=Geocachmaster]

The boiling point of ethyl acetoacetate is ...
3-3-2017 at 09:22
by: JnPS
Elementary Work on Schiff Bases
Further photos of Benzophenone Anil Prep
2-3-2017 at 21:09
by: JnPS
Elementary Work on Schiff Bases
Procedure above adapted form: J.H. Billman and K.M. Tai, [i]J. Org. Chem.[/i], [b]23[/b], 535 (1958) ...
2-3-2017 at 21:07
by: JnPS
Elementary Work on Schiff Bases
[b]Preparation of Benzophenone Anil[/b]
Unlike their aldimine counterparts, ketimines are much hard ...
2-3-2017 at 20:48
by: JnPS
Elementary Work on Schiff Bases
[b]Continued N-Benzylidenaniline Work-up:[/b]
After leaving the crystals to dry overnight the mass ...
2-3-2017 at 14:28
by: JnPS
Elementary Work on Schiff Bases
I finally got started working on schiff bases at the university so I wanted to keep tabs of all the ...
1-3-2017 at 14:43
by: JnPS
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