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Electrolysis of Sodium Bisulfate to form Sodium Persulfate
[rquote=692306&tid=160276&author=mysteriusbhoice]you dont need persulfate to make perchlorat ...
10-4-2024 at 23:06
by: LardmanAttack
Electrolysis of Sodium Bisulfate to form Sodium Persulfate
I've been attempting perchlorates once again, and one of the things needed for electrolysis that I'v ...
6-4-2024 at 02:14
by: LardmanAttack
Unsuccessful Aminoguanidine Bicarbonate synthesis
I'm just mainly trying to figure out what problems other people have had and how they've overcome th ...
23-4-2020 at 01:43
by: LardmanAttack
Unsuccessful Aminoguanidine Bicarbonate synthesis
[rquote=633939&tid=155162&author=Boffis]LardmanA; If you want us (SM) to help you we will ne ...
23-4-2020 at 01:39
by: LardmanAttack
Unsuccessful Aminoguanidine Bicarbonate synthesis
[rquote=633921&tid=155162&author=B(a)P]Have you read Engagers posts on this synthesis?[/rquo ...
11-4-2020 at 21:01
by: LardmanAttack
Unsuccessful Aminoguanidine Bicarbonate synthesis
I've been trying to work my way up the ladder of syntheses to get to tetrazole compounds and I'm cur ...
11-4-2020 at 15:31
by: LardmanAttack
NHN synthesis not working
[rquote=629596&tid=154712&author=ShotBored]My experience working with Nickel catalysts was t ...
18-1-2020 at 13:35
by: LardmanAttack
Concentrating nitric acid using sulfuric acid
Alright, thanks for the advice. I suppose I could try getting a vacuum distillation setup ready usin ...
18-1-2020 at 13:31
by: LardmanAttack
Concentrating nitric acid using sulfuric acid
Preferably, I'd want to concentrate the nitric acid to over 99% so it can perform well in the nitrat ...
16-1-2020 at 01:59
by: LardmanAttack
Concentrating nitric acid using sulfuric acid
I eventually need WFNA for the nitration of hexamine, and have been wondering about the logistics of ...
16-1-2020 at 01:50
by: LardmanAttack
NHN synthesis not working
So I was successfully able to make NHN by adding the concentrated nickel solution to the hydrazine s ...
16-1-2020 at 01:37
by: LardmanAttack
Awful ETN yields
In the end, I think my biggest issues were 1. not enough time letting it react, 2. too much water an ...
16-1-2020 at 01:35
by: LardmanAttack
Awful ETN yields
[rquote=629530&tid=154677&author=Tsjerk]Not exactly, you form nitrate groups, not nitro grou ...
16-1-2020 at 01:31
by: LardmanAttack
Sensitivity of chlorate explosives/cheddite.
I've been working with chlorate based explosives for around 8-9 months now, Their sensitivity isn't ...
14-1-2020 at 18:42
by: LardmanAttack
Awful ETN yields
[rquote=629427&tid=154677&author=XeonTheMGPony]Spend more time learning about the reaction, ...
14-1-2020 at 18:32
by: LardmanAttack
Awful ETN yields
So in summary: you want as little water as possible, use an excess of nitrate/nitric, start cold, th ...
12-1-2020 at 13:49
by: LardmanAttack
NHN synthesis not working
[rquote=629334&tid=154712&author=wessonsmith]Here is the NHN synthesis video.

https://you ...
12-1-2020 at 13:41
by: LardmanAttack
NHN synthesis not working
Interesting, I wonder if it didn't work due to leftover acid from the nickel nitrate synthesis? or t ...
12-1-2020 at 13:38
by: LardmanAttack
NHN synthesis not working
I've been wanting to make and experiment with NHN for a while now and I finally was able to get nick ...
10-1-2020 at 21:53
by: LardmanAttack
Awful ETN yields
I've always wondered if the ETN is slightly soluble in an acidic solution and if fully neutralizing ...
9-1-2020 at 23:49
by: LardmanAttack
Awful ETN yields
So I tried the ammonium nitrate/sulfuric method, and it was marginally better than normal, seeing ho ...
6-1-2020 at 23:42
by: LardmanAttack
Awful ETN yields
[rquote=629038&tid=154677&author=XeonTheMGPony][rquote=629026&tid=154677&author=cate ...
6-1-2020 at 03:18
by: LardmanAttack
Awful ETN yields
[rquote=629003&tid=154677&author=Tsjerk]Do you actually use sulfuric acid? And if so, what c ...
5-1-2020 at 02:30
by: LardmanAttack
Awful ETN yields
[rquote=628998&tid=154677&author=XeonTheMGPony]Some actual information would be nice, like h ...
5-1-2020 at 02:28
by: LardmanAttack
Awful ETN yields
Also to clarify before anyone asks, yes my erythritol is pure, that was a big problem for me in the ...
3-1-2020 at 22:01
by: LardmanAttack
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