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Chemistry behind RDX
OK, please be safe with the handling of the ketene. I couldn't find an LC50 value, but the IDLH (imm ... |
26-7-2024 at 07:43
by: Microtek |
Chemistry behind RDX
Ah, OK. But have you experimented with ketene production? A ketene lamp seems to be an easy route to ... |
25-7-2024 at 09:19
by: Microtek |
Why do explosive jelly degrade?
I agree with all of the above. As the jelly slowly sets and becomes more homogenous, it probably bec ... |
25-7-2024 at 09:15
by: Microtek |
methyl nitrate
We've talked about excessively cold nitrations before. A mixed acid that is too cold can lead to run ... |
25-7-2024 at 09:11
by: Microtek |
methyl nitrate
I agree that well neutralized, washed and dried methyl nitrate could probably be stored for a long t ... |
23-7-2024 at 08:23
by: Microtek |
Chemistry behind RDX
Is that observations from an experiment, or from research? I have never experimented with ketene, bu ... |
23-7-2024 at 08:14
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
One possibility would be to oxidize it to the N-oxide, and maybe form the ammonium or guanidine salt ... |
7-7-2024 at 00:25
by: Microtek |
Liquid primaries
As dettoo says, the lack of voids in a liquid energetic, makes ddt very inefficient. That means that ... |
26-6-2024 at 23:43
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
No, I haven't tried that. The reason I used the amino substituted triazole specifically, is that I h ... |
26-6-2024 at 23:35
by: Microtek |
Det cap questions: e-match nichrome, selecting a primary
Firearms primer mixture is much more sensitive than a quality primary such as many of the metal amin ... |
18-6-2024 at 23:11
by: Microtek |
PETN recrystallisation procedure for LOW density
@Etanol: My PETN does not contain the impurities you mention, possibly because I synthesize it from ... |
13-6-2024 at 01:37
by: Microtek |
PETN recrystallisation procedure for LOW density
You could do both. First a slow crystallization for obtaining a pure product, then redissolve in fre ... |
9-6-2024 at 01:41
by: Microtek |
PETN recrystallisation procedure for LOW density
The function of urea in this context is not to act as a base, but as a NOx scavenger. The same react ... |
7-6-2024 at 07:53
by: Microtek |
Nickel aminoguanidine diperchlorate
During the usual synthesis of NAP, the solution is boiled for about 5 minnutes. This would drive off ... |
3-6-2024 at 00:04
by: Microtek |
NHN synthesis not working
@ManyInterests: I encourage you to find a copy of the book "Small scale synthesis of Laboratory Reag ... |
11-5-2024 at 07:46
by: Microtek |
Exotic Primaries - Complex Salts
I tried copper, cobalt, zink, iron(III), nickel, aluminum and magnesium as the central ion in 4-amin ... |
2-5-2024 at 22:54
by: Microtek |
Exotic Primaries - Complex Salts
As I commented in another thread, there definitely is a Ni complex with aminoTRIazole, so I find it ... |
1-5-2024 at 12:33
by: Microtek |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I have recently experimented with 4-amino-1,2,4-triazole as a ligand for nickel perchlorate. I think ... |
21-4-2024 at 09:38
by: Microtek |
Nickel aminoguanidine diperchlorate
[quote]
Chrystal long needle’s sensitivity[/quote]
If you stir it continually during precipi ... |
14-4-2024 at 22:34
by: Microtek |
Nickel aminoguanidine diperchlorate
I would be wary of using ammonia for adjusting pH. I think you risk substituting some of the aminogu ... |
13-4-2024 at 14:00
by: Microtek |
Exotic Primaries - Complex Salts
I don't know how labile the hydrazine ligands are, but I would expect at least some of them to be re ... |
2-4-2024 at 23:43
by: Microtek |
Det Cap Strategies
Yes, I was talking about experiments with caps or similar sizes. The thing with HEs is that they als ... |
1-3-2024 at 00:30
by: Microtek |
Det Cap Strategies
Indeed, the sawdust bucket is an excellent way to iron out any problems with the caps before using t ... |
29-2-2024 at 08:54
by: Microtek |
Det Cap Strategies
I think you should abandon the idea of melt casting the base charge for now. It is possible that it ... |
29-2-2024 at 02:09
by: Microtek |
Det Cap Strategies
I suggest that you do a simple non-experimental cap first. Something like 1 g of pressed ETN or RDX, ... |
26-2-2024 at 23:30
by: Microtek |
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