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Oops
Well, that didn't go [i]too[/i] well...
I decided to opt for the calcium chloride washing method. ... |
5-3-2025 at 11:22
by: SplendidAcylation |
Removing dissolved ammonia from acetonitrile?
Thanks for the replies!
[rquote=699509&tid=160919&author=unionised]Wash the nitrile with ... |
5-3-2025 at 04:55
by: SplendidAcylation |
Problems with magnesium nitrate hexahydrate dehydratation
I would go out on a limb and say that your mistake is heating/melting magnesium nitrate in a stainle ... |
5-3-2025 at 04:50
by: SplendidAcylation |
Removing dissolved ammonia from acetonitrile?
Hi,
After a (too long) unplanned break from chemistry, I have recently attempted the preparation ... |
4-3-2025 at 05:01
by: SplendidAcylation |
Why is the nitrating power of nitrites and nitrates so different?
Unfortunately I don't really have any idea about your question, but I was wondering, have you consid ... |
3-3-2025 at 14:34
by: SplendidAcylation |
Chlorinating Carboxylic Acids
Have you considered benzoyl chloride? It can be used to convert carboxylic acids into acid chlorides ... |
17-2-2025 at 14:29
by: SplendidAcylation |
Ammonia from ammonium bicarbonate ?
Perhaps you could make a solution of ammonium bicarbonate and add calcium chloride, precipitating ca ... |
2-9-2024 at 13:24
by: SplendidAcylation |
Tin formate
Hiya.
I have tried making formaldehyde this way, and it doesn't work... At least, I couldn't get ... |
24-8-2024 at 13:25
by: SplendidAcylation |
Drying calcium chloride
[rquote=694640&tid=61108&author=Precipitates]I produced 100 g or so of some [i]mostly[/i] an ... |
21-8-2024 at 13:23
by: SplendidAcylation |
Does the temperature drop when a molecule splits in half?
[rquote=693613&tid=160334&author=j_sum1]I have not read all of this. Just enough to give yo ... |
7-7-2024 at 03:05
by: SplendidAcylation |
Does the temperature drop when a molecule splits in half?
Thanks for the replies everyone!
I must apologize profusely for the appallingly late response, un ... |
16-6-2024 at 03:38
by: SplendidAcylation |
Does the temperature drop when a molecule splits in half?
Hi,
I have recently been trying to get a better understanding of thermodynamics and kinetics, as ... |
18-5-2024 at 09:18
by: SplendidAcylation |
Success!
[rquote=692194&tid=160260&author=Texium]I would advocate for converting to acetic anhydride. ... |
6-4-2024 at 06:05
by: SplendidAcylation |
Acetic anhydride or acetyl chloride, that is the question...
[rquote=692154&tid=160260&author=clearly_not_atara]The ketene formation is not a huge proble ... |
3-4-2024 at 03:34
by: SplendidAcylation |
Acetic anhydride or acetyl chloride, that is the question...
Thanks for the replies everyone 
[rquote=692071&tid=160260&author=Texium]Generally, a ... |
2-4-2024 at 04:08
by: SplendidAcylation |
Acetic anhydride or acetyl chloride, that is the question...
Hi,
I have some fairly simple questions about acetyl chloride and acetic anhydride...
I apolog ... |
30-3-2024 at 06:29
by: SplendidAcylation |
Is triethylamine hygroscopic?
Thanks!
I dried it over NaOH overnight, decanted it off, and then distilled it over some more NaO ... |
28-3-2024 at 02:29
by: SplendidAcylation |
Is triethylamine hygroscopic?
Oops! I said my alcohol was a Mannich base, but of course, that is nonsense; It is an amino-alcohol ... |
26-3-2024 at 06:48
by: SplendidAcylation |
Definition of "melting point"
Off the top of my head, it is the temperature where the Gibbs free energy for the phase transition i ... |
25-3-2024 at 14:27
by: SplendidAcylation |
Two possible methods
Hi,
The oxidation of benzyl alcohol using nitric acid is very effective, there is a photo essay o ... |
25-3-2024 at 14:24
by: SplendidAcylation |
Is triethylamine hygroscopic?
Thanks for the replies! 
I feel quite silly for not having thought about using a different solv ... |
25-3-2024 at 04:27
by: SplendidAcylation |
Is triethylamine hygroscopic?
Hi,
Just a quick question...
I have a very old bottle of triethylamine, probably at least 60 y ... |
24-3-2024 at 06:40
by: SplendidAcylation |
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
[rquote=691509&tid=156115&author=clearly_not_atara]I think that the solubility of HCl in BzC ... |
22-3-2024 at 04:34
by: SplendidAcylation |
How problematic is dissolved HCl in acyl halides?
Hi,
I have since attempted the chlorination of benzaldehyde to make benzoyl chloride, and it was ... |
11-3-2024 at 06:13
by: SplendidAcylation |
Weight - Molarity of di/ter/quart-atomic elements
RU_KLO raises an interesting point... I too would appreciate clarification on this topic.
Halogen ... |
20-2-2024 at 06:39
by: SplendidAcylation |
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