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successful method for purifying anthranilic acid(quick report)
[rquote=658627&tid=155744&author=draculic acid69]Last question:. Is this recrystallisation p ... |
21-4-2021 at 08:47
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
[rquote=658567&tid=155744&author=draculic acid69]Just a quick question; was tap or distilled ... |
20-4-2021 at 10:49
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658558&tid=157068&author=karlos³][rquote=658553&tid=157068&author=SuperOxid ... |
19-4-2021 at 16:45
by: SuperOxide |
Large scale anthranilic acid prep
[file]88063[/file] |
19-4-2021 at 13:27
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658507&tid=157068&author=mr_bovinejony]@oxide I just don't like the reaction, titrat ... |
19-4-2021 at 13:00
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
[rquote=658519&tid=155744&author=draculic acid69]Water seems to be a no go for this substanc ... |
19-4-2021 at 08:01
by: SuperOxide |
successful method for purifying anthranilic acid(quick report)
Just an update - I gave this a go again yesterday, and while it technically works, it takes a looooo ... |
18-4-2021 at 18:16
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658453&tid=157068&author=mr_bovinejony]The hoffman reaction is bullshit for any chem ... |
18-4-2021 at 15:23
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658442&tid=157068&author=mr_bovinejony]I definitely think so, even with the brown di ... |
18-4-2021 at 08:16
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658425&tid=157068&author=mr_bovinejony]From what I've seen, the hoffman route usuall ... |
18-4-2021 at 07:07
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658387&tid=157068&author=mr_bovinejony]Eh that's what happens when its left out in t ... |
17-4-2021 at 20:42
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658385&tid=157068&author=RustyShackleford]Wow. Your anthranilic acid looks awful con ... |
17-4-2021 at 16:19
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=658377&tid=157068&author=mr_bovinejony]https://imgur.com/ujQ4mhy
https://imgur.co ... |
17-4-2021 at 13:44
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=657349&tid=157162&author=Fery]I found helpful video here:
https://www.youtube.com/w ... |
1-4-2021 at 10:19
by: SuperOxide |
Methaqualone
[rquote=651155&tid=156723&author=karlos³][...]
Also, a personal opinion, I consider the pr ... |
28-3-2021 at 17:00
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=657197&tid=157162&author=Benignium]Awesome! There is indeed going to be some DCM as ... |
28-3-2021 at 15:37
by: SuperOxide |
Large scale anthranilic acid prep
[rquote=657073&tid=157068&author=mr_bovinejony]I recently did a run of 150 grams of the grap ... |
26-3-2021 at 10:04
by: SuperOxide |
Large scale anthranilic acid prep
Very interesting... I have 500g of phthalimide that I will probably never use, which I could make th ... |
26-3-2021 at 08:43
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
FYI - finally got this synth/workup finished (mostly).
Here's the result:
[file]87604[/file]
... |
24-3-2021 at 18:44
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656481&tid=157162&author=Benignium]Somewhat unrelated, but I was left with a few gra ... |
16-3-2021 at 08:13
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656474&tid=157162&author=S.C. Wack]PS the pH and amount of NaOH to add does not need ... |
15-3-2021 at 16:16
by: SuperOxide |
Anyone else in the US having issues finding OTC sodium bromide?
[rquote=656404&tid=157140&author=zed][...]
Funny World. My Pyrotechnics guy say yer lim ... |
15-3-2021 at 11:30
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656423&tid=157162&author=Fery]This advice is too late, but why did you use Sn instea ... |
15-3-2021 at 08:08
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656400&tid=157162&author=zed]Um. You are going to steam distill it. Most of the br ... |
14-3-2021 at 15:41
by: SuperOxide |
First o-toluidine synthesis - running into some issues with the reaction mixture
[rquote=656387&tid=157162&author=Benignium]Seems reasonable on paper. Add all of the NaOH so ... |
14-3-2021 at 13:38
by: SuperOxide |
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