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Looking for Heidolph rotovap G6 glass set adapter
Hi Dr. Bob,

I had a similar thing I sent in a U2U to you. Please let me know if you received it.
12-5-2022 at 19:03
by: Triflic Acid
Cleaning Nitric Acid Stains from Skin
Honestly, it doesn't hurt and doesn't have any negative health effects, so I don't see why you would ...
5-5-2022 at 10:55
by: Triflic Acid
Reduction of 4-Chloro-3-nitrotoluene failure
Using Mg metal in methanol has worked well for me in the past, when I was making dizaotoluene, from ...
3-5-2022 at 06:28
by: Triflic Acid
Catalyst for Amide hydrolysis
I’m actually trying to produce vanillin from capsaicin. So that doesn’t work for me sadly.
1-5-2022 at 12:06
by: Triflic Acid
Catalyst for Amide hydrolysis
AvB, thanks, that look pretty intersting. I might give that a try once I can synthesize some ethyldi ...
29-4-2022 at 21:23
by: Triflic Acid
Magnesium Powder
I can personally attest to united nuclears:https://www.amazon.com/gp/product/B08ZGBBG82/ref=ppx_yo_d ...
29-4-2022 at 08:25
by: Triflic Acid
Catalyst for Amide hydrolysis
Around 7 months ago I tried to produce vanillyl amine from capsaicin. That ended badly because I had ...
29-4-2022 at 08:19
by: Triflic Acid
Acetic anhydride preparation
Well, there is this really annoying chemist who works 3 hoods away from me at work :P
29-4-2022 at 08:03
by: Triflic Acid
Acetic anhydride preparation
Acetaldehyde with tert-butyl hypochlorite should create acetyl chloride:
"tert-Butyl hypochlorite i ...
27-4-2022 at 13:40
by: Triflic Acid
Hydrazine to Hydrazone question... please and thank you
Another option for you might be to reduce your hydrazine to an amine, then diazotize to make the alc ...
24-4-2022 at 07:59
by: Triflic Acid
DCM shortages
Has anyone here heard about a dcm supply chain shortage for next year? I've been hearing rumours, bu ...
13-4-2022 at 14:00
by: Triflic Acid
very viscous styrene
Polymerized styrene can form hard clear chunks that might look like crystals, sending photos would h ...
8-4-2022 at 19:48
by: Triflic Acid
Allene from acetone and P₂O₅
It might: https://patents.google.com/patent/US4301319A/en
20-2-2022 at 19:24
by: Triflic Acid
Reagent exchange Any interested parties??
what do you mean "crystals"?
4-1-2022 at 08:39
by: Triflic Acid
Questions about piranha solution.
Manganese oxides also react with hydrochloric acid but produce Cl2 gas, so this must be done outdoor ...
4-1-2022 at 08:38
by: Triflic Acid
Apparatus for making anhydrous aluminium chloride
You should probably use some acidic dehydrating agent since any suspended NaOH or Na2O from the sodi ...
2-1-2022 at 07:55
by: Triflic Acid
Deploying an Impractical HE By In Situ Preparation, Pros and Cons
I believe they do this same thing when dropping VX nerve agents. The BLU-80 Missle mixes the precurs ...
30-12-2021 at 20:26
by: Triflic Acid
Separation of toluene and isobutanol
A cheap, albeit not greatly effective method, would be to get the reflux a large amount of this mixt ...
27-12-2021 at 08:36
by: Triflic Acid
The 2021 Christmas greeting thread
Merry Christmas from the western US deserts!
25-12-2021 at 16:31
by: Triflic Acid
Synthesis of dichloromethane- question mark.
@Texium, I also should have been more clear. When I said on-tap, I was referring to an easy to set u ...
25-12-2021 at 16:26
by: Triflic Acid
Help with FT-IR spectra
Have you run it through AIST. that can help you get a rough match to another spectrum
17-12-2021 at 08:16
by: Triflic Acid
Synthesis of dichloromethane- question mark.
and what is so bad about it?
16-12-2021 at 08:35
by: Triflic Acid
Cleaning buchner funnel after NHN synthesis
A bit of advice, do the reaction on a day that it snows. If you somehow run out of ice during the pr ...
15-12-2021 at 11:52
by: Triflic Acid
Shooting oxygen tank shows fire and no fuel ??
they should have packed the cylinders with magnesium shavings, then ran far far away. The explosion ...
15-12-2021 at 11:51
by: Triflic Acid
Cleaning buchner funnel after NHN synthesis
As a side note, when making explosives, I always keep a filter paper between the glass frit and the ...
15-12-2021 at 07:53
by: Triflic Acid
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