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Dioxane didn’t end well
Sounds like you skipped the second sulfuric acid wash after distillation
4-5-2021 at 03:07
by: XeonTheMGPony
Dioxane didn’t end well
[rquote=658666&tid=157330&author=clearly_not_atara]Sounds like it worked out. :D

The othe ...
22-4-2021 at 03:56
by: XeonTheMGPony
Synthesis checks for HMTD
If you are starting to do this now, take the advice others have given and treat this stuff like glow ...
18-4-2021 at 05:46
by: XeonTheMGPony
Making copper from copper sulfate and iron nails
I used citric acid and seemed to have reduced the copper sulphate back to metallic copper effectivel ...
16-4-2021 at 03:44
by: XeonTheMGPony
What is happening at Deschem?
[rquote=658002&tid=157284&author=zed]I've got a fair sized order, I want to place with Desch ...
13-4-2021 at 03:31
by: XeonTheMGPony
My Chloral Hydrate Synth
Ok so I re chlorinated it, Sp, Bp, are all in spec, I now have some over chlorinated heavy stuff sme ...
5-4-2021 at 03:47
by: XeonTheMGPony
Using enormous excess of solvents for extractions?
[rquote=657053&tid=157215&author=Fyndium]Not sure if this is part of the topic, but I consta ...
26-3-2021 at 03:28
by: XeonTheMGPony
Looking for a hotplate stirrer for around $100 CAD. What should I get?
[rquote=656652&tid=157183&author=itsallgoodjames][rquote=656651&tid=157183&author=Xe ...
19-3-2021 at 15:34
by: XeonTheMGPony
Looking for a hotplate stirrer for around $100 CAD. What should I get?
[rquote=656641&tid=157183&author=itsallgoodjames]I've been looking to get a proper hotplate ...
19-3-2021 at 03:18
by: XeonTheMGPony
latest glassware purchase
recent glass order from daschem,e excellently packed per usual.

vacuum trap and the rest you'll r ...
18-3-2021 at 17:17
by: XeonTheMGPony
The neurochemicals in nature
[rquote=652589&tid=81743&author=symboom]
Thank you that's great to hear.
akuamma is normal ...
11-3-2021 at 03:25
by: XeonTheMGPony
Where to get phosphorus pentoxide in Canada, and what's a reasonable price for it?
SCHEDULE VI(Sections 2, 6, 55 and 60)
PART 1
Class A PrecursorsFootnote 1

1 Acetic anhydride
1 ...
10-3-2021 at 16:55
by: XeonTheMGPony
erythritol tetranitrate recrystallization
When I make an ETN batch, I crash into ice water and mix, let stand for a couple hours (let all the ...
8-3-2021 at 03:54
by: XeonTheMGPony
Wrong/Bad Condensor with Soxhlet Extractor
[rquote=655992&tid=157119&author=electrokinetic]@Xeon thanks and good luck. I'd rather get ...
8-3-2021 at 03:42
by: XeonTheMGPony
Hydrazine sulfate and sodium sulfate separation
This is where spending more research time would have saved you a large head ach!

Do the fist Neut ...
7-3-2021 at 05:59
by: XeonTheMGPony
erythritol tetranitrate recrystallization
get urea, 3% by weight to co administer to the recrystallizing water, and to the solvant
5-3-2021 at 03:40
by: XeonTheMGPony
Wrong/Bad Condensor with Soxhlet Extractor
what I did, ordered an adapter to 24/40 and used my Allihn @ 300mm for it, Now I have a Dimroth I'll ...
5-3-2021 at 03:32
by: XeonTheMGPony
Glacial acetic acid in Canada?
I am finding google is becoming more and more useless now days, nearly as infuriating as amazon.ca s ...
3-3-2021 at 03:39
by: XeonTheMGPony
Hydrazine process here outdated?
here 35% is available in 4L jugs for peroxide.
2-3-2021 at 16:16
by: XeonTheMGPony
Making a lab stand/rack setup - what is a good design?
[rquote=655726&tid=157091&author=digga]I did the 1/2" black metal pipe uprights setting on a ...
2-3-2021 at 16:12
by: XeonTheMGPony
Glacial acetic acid in Canada?
Any one have a supplier that sells to individuals or selling a few liters?
2-3-2021 at 16:09
by: XeonTheMGPony
My Chloral Hydrate Synth
[rquote=655692&tid=157099&author=Metacelsus]Very nice writeup!

If you're going for DDT, I ...
2-3-2021 at 06:03
by: XeonTheMGPony
Mercury in Canada
Mercury is about 200 dollars a pound in Canada
1-3-2021 at 08:55
by: XeonTheMGPony
My Chloral Hydrate Synth
Hello, after reading up on all the threads here, and online I finally did a run for chloral hydrate ...
1-3-2021 at 08:35
by: XeonTheMGPony
Making a lab stand/rack setup - what is a good design?
[rquote=655564&tid=157091&author=zed]Clamps are expensive, compared to the bargain prices, c ...
27-2-2021 at 10:42
by: XeonTheMGPony
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