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Amination of tertiary alkyl halide
Since the mechanism is supposedly SN1, using a more polar solvent might help in reaction. |
20-3-2013 at 16:55
by: bananaman |
Difficult contaminant
1) My personal experience was to test the solubility of your compound with various solvents, e.g. CH ... |
20-3-2013 at 16:52
by: bananaman |
Hydrogen chloride gas balloon
[rquote=278319&tid=23749&author=wireshark]I know hydrogen balloons are a regular thing used ... |
19-3-2013 at 22:24
by: bananaman |
Boric Acid Catalysis of Amide
I am not too sure about the catalysis by boric acid, though there is a journal article about the rea ... |
19-3-2013 at 22:22
by: bananaman |
Amino acid chemistry
Try reading Mannich reaction. |
18-3-2013 at 17:37
by: bananaman |
Boric Acid Catalysis of Amide
Amine + Carboxylic acid --> Amide + Water
Xylene/toluene/benzene are able to form azeotropes w ... |
18-3-2013 at 17:35
by: bananaman |
microscale column chromatography
[rquote=278125&tid=23681&author=jamit]How practical is column chromotography for home lab an ... |
17-3-2013 at 20:25
by: bananaman |
Dimethylation of tryptamine via formaldehyde/STAB
Amines are known to be rather polar, and would often stick to polar silica gel. Usually, there is a ... |
15-3-2013 at 00:50
by: bananaman |
microscale column chromatography
According to the Van Deemter equation, size of particles would affect the resolution of peaks. The s ... |
14-3-2013 at 17:06
by: bananaman |
microscale column chromatography
In addition to the use of Pasteur pipettes, you might want to simply run it on a TLC plate, and subs ... |
13-3-2013 at 20:12
by: bananaman |
Copper catalyzed cyanations of benzyl chlorides with potassium ferrocyanide
[rquote=276192&tid=23499&author=Lambda-Eyde]As in the [url=http://en.wikipedia.org/wiki/Sand ... |
27-2-2013 at 16:47
by: bananaman |
Acetamide Synthesis
Sorry for the mistakes previously. Attached is a relevant paper regarding the preparation of acetami ... |
26-2-2013 at 17:33
by: bananaman |
Copper catalyzed cyanations of benzyl chlorides with potassium ferrocyanide
[rquote=276091&tid=23499&author=no_dream]
Anyway this reaction is a novel method, using non ... |
26-2-2013 at 17:09
by: bananaman |
Acetamide Synthesis
Acetic acid is one of the products from the reaction between ethyl acetate and ammonia.
CH3COOC2H ... |
25-2-2013 at 18:34
by: bananaman |
Hydrogenation
[rquote=275549&tid=23415&author=luckybot]What about propane?[/rquote]
What do you mean by ... |
20-2-2013 at 21:50
by: bananaman |
Cleaning Chromatographic Silica Media
Since silica is considered to be a polar medium, why not try flushing the silica column with solvent ... |
19-2-2013 at 16:52
by: bananaman |
Does This Reaction Actually Occur?
Why not simply try using those cation exchange resin?
Start off with the potassium form, and pass ... |
18-2-2013 at 23:44
by: bananaman |
Hydrogenation
Why not simply attach your vessel to a vacuum pump, and have it evacuate the entire vessel before in ... |
18-2-2013 at 23:39
by: bananaman |
Synthesis of N-(4-Hydroxyphenyl)glycine (or related photography processing chemicals)
I tend to believe that there is a need for some protection chemistry to be performed on glycine and ... |
17-2-2013 at 22:44
by: bananaman |
