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Plutonium reactions - how'd they figure this stuff out? The use of iodine may be a case of the crystal bar process. |
18-3-2024 at 12:03 by: clearly_not_atara |
chloromethylene dibenzoate: stable formyl chloride equivalent Can't edit the last post anymore but the thesis above:
https://aura.american.edu/articles/thesis/Sy ... |
17-3-2024 at 07:36 by: clearly_not_atara |
Separating chloroacetic acid and an sulfuric acid Depending on how much sulfuric acid you used, it might be possible to absorb it onto anhydrous sodiu ... |
16-3-2024 at 20:39 by: clearly_not_atara |
chloromethylene dibenzoate: stable formyl chloride equivalent ^Thanks. The book is similarly circumspect. It also cites Descudé, but a different paper ([i]Compt. ... |
15-3-2024 at 21:45 by: clearly_not_atara |
Thioacetamide synthesis Acetone is probably fine. Some amount of condensation is probably possible. But it shouldn't affect ... |
15-3-2024 at 11:15 by: clearly_not_atara |
Ethylchloride preparation According to Raoult's law, the product is most likely a gas, since the rxn is sluggish at low temper ... |
15-3-2024 at 10:50 by: clearly_not_atara |
Thioacetamide synthesis Do not use ethanol to recrystallize.
[quote]when hydrogen ions exists, it can generate thiosulfate ... |
15-3-2024 at 09:07 by: clearly_not_atara |
chloromethylene dibenzoate: stable formyl chloride equivalent Wenzel in 1914 (attached) reported the reaction of chlorine with methylene dibenzoate, giving the ti ... |
14-3-2024 at 17:08 by: clearly_not_atara |
Calcium Silicate from concrete rubble? [rquote=691536&tid=160214&author=nikotyna1939]I don't just buy calcium silicate because in m ... |
14-3-2024 at 07:47 by: clearly_not_atara |
Hydrazinol (N-amino hydroxylamine) This is postulated as an intermediate in some oxidations of hydrazine. It is probably extremely unst ... |
13-3-2024 at 07:52 by: clearly_not_atara |
burnt through steel crucible? Zinc seems like a likely culprit. Often alloyed with copper and tin, low bp, potentially flammable v ... |
13-3-2024 at 07:33 by: clearly_not_atara |
Synthesis of fatty acids from expired soap Soap doesn't really expire. They just want you to buy more. Granted there will be some rancidity, bu ... |
13-3-2024 at 05:08 by: clearly_not_atara |
Calcium Silicate from concrete rubble? You can just buy wollastonite IIRC |
12-3-2024 at 18:39 by: clearly_not_atara |
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde I think that the solubility of HCl in BzCl is probably quite low. HCl is highly volatile and only di ... |
11-3-2024 at 20:07 by: clearly_not_atara |
Failed attempts at oxidation of alcohols with DMSO/P2O5 The Swern conditions are known to attack phenols as well:
https://cir.nii.ac.jp/crid/13902826791139 ... |
9-3-2024 at 07:15 by: clearly_not_atara |
Failed attempts at oxidation of alcohols with DMSO/P2O5 Have you tried any other substrates? It's plausible that cinnamyl alcohol just acts weird here. Not ... |
8-3-2024 at 14:04 by: clearly_not_atara |
Thioacetamide synthesis Even among thioamide preparations, this one sounds particularly dangerous. H2S at high pressure? Org ... |
8-3-2024 at 07:14 by: clearly_not_atara |
The Short Questions Thread (4) I didn't know Yakov Smirnov posted here |
6-3-2024 at 21:51 by: clearly_not_atara |
Metallic soaps If it forms an acetate, it should probably form a stearate. The reactivity of the carboxylate doesn' ... |
5-3-2024 at 15:17 by: clearly_not_atara |
Unexpected product in mucic acid dry distillation Recently my thoughts came back to this.
https://www.mdpi.com/2073-4344/13/7/1114
In the above ... |
5-3-2024 at 11:14 by: clearly_not_atara |
The Short Questions Thread (4) CAS 56138-70-6:
https://www.lookchem.com/ProductWholeProperty_LCPL1207016.htm
https://academic ... |
2-3-2024 at 08:46 by: clearly_not_atara |
pKa of an aldehydic hydrogen? Look up "acyl anion" |
2-3-2024 at 08:36 by: clearly_not_atara |
Solvents for Lithium Hydride There are no soluble saline hydrides in any solvents. LiH is always used heterogeneous. And yeah I d ... |
29-2-2024 at 21:38 by: clearly_not_atara |
What exactly is going on in this here molecule? It also appears that perchloryl amides were investigated by the US military:
https://apps.dtic.mi ... |
29-2-2024 at 11:11 by: clearly_not_atara |
What exactly is going on in this here molecule? There's a negative charge on the oxygens, a positive charge on the hydrogens, and the separation is ... |
28-2-2024 at 14:53 by: clearly_not_atara |
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