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Drying pseudonitrosites
Thank you. I've always found it a very elegant reaction. And I'm more interested in the chemistry mu ...
14-5-2021 at 03:01
by: dicyanin
Drying pseudonitrosites
This is the sample of isodillapiole pseudonitrosite I kept in a capped container. It is now 2 days a ...
13-5-2021 at 06:17
by: dicyanin
Drying pseudonitrosites
[b][u]Preparation of beta-nitroisodillapiole[/u][/b]

The above pseudonitrosite was added in small ...
13-5-2021 at 06:15
by: dicyanin
Drying pseudonitrosites
Pondering over the stability of pseudonitrosites, I remembered I still had a sample of isodillapiole ...
13-5-2021 at 06:08
by: dicyanin
Can you only dry 3A Molecular Sieves in the Microwave? (OTC)
Here's a pic of the 3A molecular sieves (still wet with methanol) I've been using and re-using for y ...
11-5-2021 at 04:19
by: dicyanin
Drying pseudonitrosites
It never was an issue for me as the pseudonitrosite is washed a few times with alcohol and finally w ...
10-5-2021 at 08:14
by: dicyanin
synthesis of methyl iodide from methanol, HCl and sodium iodide?
My apologies for waking up the dead, but I thought I might as well share my own notes here using a v ...
9-5-2021 at 08:53
by: dicyanin
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
[rquote=658154&tid=157292&author=zed]

Making Anhydrous Sodium Methoxide solutions, withou ...
20-4-2021 at 09:41
by: dicyanin
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
Benignium: for syringaldehyde the reaction runs much better under autogenous pressure as described b ...
20-4-2021 at 09:26
by: dicyanin
Acetic anhydride preparation
[rquote=639066&tid=9&author=monolithic][rquote=638561&tid=9&author=Waffles SS]Or why ...
27-1-2021 at 04:39
by: dicyanin
Acetic anhydride preparation
Working with ketene is madness in a home lab.

GB299342 looks interesting as sodium metaphosphates ...
27-1-2021 at 03:44
by: dicyanin
Does methanol smell like anything to you?
[rquote=649131&tid=156525&author=karlosĀ³]Haha very good! I actually thought about that too, ...
27-1-2021 at 03:04
by: dicyanin
Does methanol smell like anything to you?
[rquote=649102&tid=156525&author=Fery]Tsjerk grape brandy is quite OK. Other fruit brandies ...
27-1-2021 at 02:59
by: dicyanin
Does methanol smell like anything to you?
You're not going to absorb a toxic dose of methanol transdermally from an accidental spill on your h ...
27-1-2021 at 02:51
by: dicyanin
Does methanol smell like anything to you?
[rquote=653807&tid=156525&author=Fyndium]How much precautions do you take when handling meth ...
27-1-2021 at 02:48
by: dicyanin
Does methanol smell like anything to you?
[rquote=648978&tid=156525&author=karlosĀ³]
But how is it for you guys with pure DMF or DMSO ...
27-1-2021 at 02:42
by: dicyanin
Does methanol smell like anything to you?
[rquote=648940&tid=156525&author=Fery]there is very big variability in smelling compounds am ...
27-1-2021 at 02:28
by: dicyanin
Does methanol smell like anything to you?
[rquote=648934&tid=156525&author=p4rtridg3]
Thinking back to the many times I've used it in ...
27-1-2021 at 02:06
by: dicyanin
Propionyl chloride with cyanuric chloride and anger
[rquote=653525&tid=156935&author=clearly_not_atara] rP is not always available. Of course, i ...
27-1-2021 at 01:53
by: dicyanin
Propionyl chloride with cyanuric chloride and anger
I remember Sauron's time here, I agree it was mostly arm-chair chemist masturbation :D.
27-1-2021 at 01:48
by: dicyanin
Acetonedicarboxylic acid from ferric ammonium citrate
sorry for resurrecting the dead, but I was searching for the same info and in the search enginge I f ...
1-11-2020 at 05:15
by: dicyanin
acidifying pyrosulfate with sulfuric acid in an attempted oleum substitute?
Hi,

It is posssible to obtain sodium or potassium pyrosulfate in varying amounts of purity, eithe ...
30-10-2020 at 05:32
by: dicyanin
Ammonium Nitrate Source
[rquote=633470&tid=154996&author=RogueRose][rquote=633469&tid=154996&author=Lion850] ...
24-9-2020 at 23:09
by: dicyanin
LET THIS SIGNAL THE END OF THE FRIDGE PUMP QUESTIONS!
Water cooling is overkill, I used a ventilator on my fridge compressor, continuously blowing air on ...
2-4-2020 at 17:55
by: dicyanin
Ammonium Nitrate Source
I usually buy ethanol denatured with 5% diethyl ether through the pharmacy. 20 euros for a gallon.
2-4-2020 at 17:32
by: dicyanin
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