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Easy OTC oxidative cleavage of alkenes - Real or more BS?
I completely agree with everything you've said Nicodem.

I've ordered in some cinnamic acid and i' ...		 31-3-2014 at 09:53
by: forsh
Easy OTC oxidative cleavage of alkenes - Real or more BS?

[img]http://i62.tinypic.com/iem1ba.gif[/img]

Thats the reaction I think I have here.


Tru ...		 31-3-2014 at 06:32
by: forsh
Easy OTC oxidative cleavage of alkenes - Real or more BS?
I've completed the reaction and i've just got the GCMS back. I did the reaction exactly as describe ...		 31-3-2014 at 04:50
by: forsh
Uses for polyethylene glycol
Missile fuel? http://www.google.co.uk/patents/US6632378 		25-3-2014 at 12:41
by: forsh
Easy OTC oxidative cleavage of alkenes - Real or more BS?
[rquote=324230&tid=29702&author=Dr.Bob]It looks perfectly reasonable. Oxone is a useful ox ...		 25-3-2014 at 06:43
by: forsh
Easy OTC oxidative cleavage of alkenes - Real or more BS?
Yeah. I'm getting everything together and i'm going to do the reaction tomorrow with styrene - just ...		 25-3-2014 at 06:33
by: forsh
Easy OTC oxidative cleavage of alkenes - Real or more BS?
Hi,
While doing a lit search on oxidative cleavage I stumbled on this new paper in tetrahedron [url ...		 25-3-2014 at 05:08
by: forsh
Synthesis of the nonbenzodiazepine Pagoclone
"I don't see how the 5-methylhexan-2-one can be obtained easily unless one can order from a big chem ...		 4-3-2014 at 12:12
by: forsh
Any creative use for kavalactones?
Not very OTC, but throwing it out there ...

How about an oxidative cleavage to aldehyde or carbox ...		 4-3-2014 at 10:27
by: forsh
THP protection of amines?
Hi,
I've had some success with this Claisen method now. I heated 1.5g of my aromatic allyl ether i ...		 15-1-2014 at 14:23
by: forsh
THP protection of amines?
Hi,

Just a short update. I am now getting excellent yields in the earlier steps in my synthesis u ...		 7-1-2014 at 03:57
by: forsh
THP protection of amines?
Thank you for your suggestions.
The paper I read that told me that zinc would catalyst a Claisen re ...		 2-12-2013 at 01:57
by: forsh
THP protection of amines?
Hi all. I've moved onto the next few steps of this synthesis, but i've hit a bit of a wall now.
...		 28-11-2013 at 10:00
by: forsh
THP protection of amines?
Tried both DFJ and Nicodem's methods today, both worked superbly with similar yields. Thank you ver ...		 14-11-2013 at 05:36
by: forsh
THP protection of amines?
Well I can definitely see the difference between the long experienced chemists and the young researc ...		 13-11-2013 at 01:51
by: forsh
THP protection of amines?
[rquote=307036&tid=27231&author=Nicodem][rquote=307031&tid=27231&author=forsh]My pla ...		 12-11-2013 at 11:56
by: forsh
THP protection of amines?
[rquote=307029&tid=27231&author=Nicodem]
Yes, anilines can be alkylated by dihydropyran und ...		 12-11-2013 at 10:20
by: forsh
THP protection of amines?
Hi there,
Apologies for the long post,I hope you will bear with me. I'm trying to protect the phen ...		 12-11-2013 at 03:25
by: forsh

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