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Michael Addition and the Synthesis of Aminoglutethimide
Here's an experiment involving Michael addition for those who like me have an interest in this type ... |
22-8-2007 at 02:09
by: freachem |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
Hi
Garage chemist, please direct me your method of making PCl5 with red phosphor and chloroform. ... |
26-7-2007 at 04:22
by: freachem |
2,6-dinitrosobenzene-1,4-diol prep ?
Here's some more information but I don't see any mention of a dinitrosation,
Preparations of C-N ... |
23-7-2007 at 23:33
by: freachem |
2,6-dinitrosobenzene-1,4-diol prep ?
Thanks Sauron
These links are also useful
For nitration
http://www.orgsyn.org/orgsyn/chemname. ... |
23-7-2007 at 04:16
by: freachem |
2,6-dinitrosobenzene-1,4-diol prep ?
Hello again
Pleased to anounce that I still have fingers. Anyway more to the topic, I have made s ... |
21-7-2007 at 09:01
by: freachem |
Test for nitro compound on modified carbon
Hello
I recently went about attempting to modify the surface of graphite using a diazo reduction ... |
18-5-2007 at 03:56
by: freachem |
4,4-dinitrotriphenylamine conversion
Hi
After many a painstaking attempt I finally made a decent qty of 4,4-dinitrotriphenylamine. Jus ... |
11-4-2007 at 05:13
by: freachem |
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
Hi
Could Fe(SO3)3 be used for SO3 production |
30-3-2007 at 06:42
by: freachem |
Recovery of Cesium salts from Pollucite ore.
Thanks
Just for added info
The by products are cesium iodide, cesium bromide, and a tripheny ... |
30-3-2007 at 03:05
by: freachem |
re-use of cesium compounds
Hi, I used cesium carbonate in an organic reaction which included the use of halobenzenes etc. Do yo ... |
30-3-2007 at 01:28
by: freachem |
Acetic anhydride preparation
Momentary laps in concentration, I figure more acetic acid will form. |
7-12-2006 at 22:35
by: freachem |
Acetic anhydride preparation
Hi all
Just dabbling here but what would happen if you reacted peroxyacetic acid and acetaldehyde ... |
7-12-2006 at 11:28
by: freachem |
o-toluidine from o-nitrotoluene
Hi Kafka
Thanks for the reply
I started with 40g toluene, I nitrated it using HNO3/H2SO4(ratio ... |
6-12-2006 at 02:57
by: freachem |
o-toluidine from o-nitrotoluene
Hi
I recently attempted a reduction using HCl Sn and o-nitrotoluene, The problem I am having is ... |
5-12-2006 at 06:22
by: freachem |
