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Peroxide Concerns - Please Help
The plan is to attempt to recover at least half the ether through distillation using as low heat as ...
25-3-2021 at 13:38
by: gravityzero
Peroxide Concerns - Please Help
If an ether based mixture contained a desired product which will crystallize out, but the mixture al ...
25-3-2021 at 08:05
by: gravityzero
Nitroethane from ethylsulfate, Desseigne variation.
Curious in making the ethyl sulfate from ethanol and sodium sulfate. Tried this not long ago, but my ...
24-9-2020 at 09:26
by: gravityzero
Clarification
I want to clarify the statement I made earlier.
I have an offline backup of this material.

I do ...
29-4-2018 at 15:53
by: gravityzero
Clarification
I want to clarify the statement I made earlier.
I have an offline backup of this material.

I do ...
29-4-2018 at 15:51
by: gravityzero
Videos Archived
Community,

I often make archives of content I feel might disappear.
I have on hand 182 videos of ...
29-4-2018 at 15:22
by: gravityzero
Videos Archived
Community,

I often make archives of content I feel might disappear.
I have on hand 182 videos of ...
29-4-2018 at 15:18
by: gravityzero
Electrochemical Cells - Understanding Amperage or Current
Thanks so much for all the helpful advice everyone! I do appreciate this community and the willingn ...
30-3-2018 at 12:51
by: gravityzero
Electrochemical Cells - Understanding Amperage or Current
So I've ran across a number of different electrolysis projects that I would like to try.
One conc ...
28-3-2018 at 16:52
by: gravityzero
Diethylamine Hydrochloride Synthesis
This seems like a fairly cheap and easy procedure to attempt. It is odd that no one has reported mu ...
26-1-2018 at 17:59
by: gravityzero
Porous Pot for Voltaic Cell
Thanks for all the suggestions. It is appreciated. The width is 65mm x height of 190mm.
I agree w ...
18-10-2017 at 13:50
by: gravityzero
Porous Pot for Voltaic Cell
Would like to start looking into electrolysis cells a bit further.
Found a patent example that call ...
13-10-2017 at 10:04
by: gravityzero
Methylenation of catechol with dichloromethane
[rquote=490064&tid=76069&author=Crowfjord]Nice. I probably would have used even more DMSO, t ...
18-8-2017 at 09:43
by: gravityzero
Oxidation of styrene to phenylacetaldehyde
After reading the thread in full, it is still unclear if anyone is able to get to Styrene Oxide simp ...
2-11-2016 at 15:39
by: gravityzero
Glyoxylic acid by magnesium reduction
Thanks Waffles SS.

I actually got more out of those articles than some of the previous ones I've ...
10-8-2016 at 15:41
by: gravityzero
Glyoxylic acid by magnesium reduction
If anyone cares to shed a little more light on the separation technique.

Let's say one attempted ...
9-8-2016 at 15:52
by: gravityzero
Potassium Hydrogen Sulfate Preparation - KHSO4
Cool. I really appreciate the information and assistance. I think I will try this through a comple ...
20-7-2016 at 13:12
by: gravityzero
Potassium Hydrogen Sulfate Preparation - KHSO4
Well KOH + H2SO4 will do the trick. I would rather do this with potassium carbonate if it will work ...
20-7-2016 at 12:47
by: gravityzero
Potassium Hydrogen Sulfate Preparation - KHSO4
It amazes me sometimes what appears to be a simple chemical is often difficult to prepare or even pu ...
20-7-2016 at 12:05
by: gravityzero
Gradual addition of powdered KMnO4 to the reaction mixture
[rquote=322115&tid=29407&author=Mailinmypocket]A powder addition funnel with a worm screw to ...
12-3-2014 at 13:11
by: gravityzero
MeNO2 Distillation
Had some old nitro laying around and was thinking about purifying some this weekend.

Gonna work w ...
12-3-2014 at 11:20
by: gravityzero
Preparation of acetic acid?
When I see this type of post I have to ask, where do you live?
Acetic Acid is readily available in ...
21-2-2014 at 13:18
by: gravityzero
what do you use to store iodine/bromine
Thanks Mailinmypocket. I went with the teflon capped media bottles.
Picked up a few Hybex brand ...
21-2-2014 at 11:23
by: gravityzero
Iodine Containment
Around 6 months ago, I came across around 200g of iodine. Had a few plans at the moment, but had to ...
21-2-2014 at 08:49
by: gravityzero
Vacuum Distillation - Best Vacuum Pump? Will the glassware implode?
A nice pump can be had for under $200 new. Most name brand glassware is intended to support heavy v ...
14-2-2014 at 17:00
by: gravityzero
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