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Anhydrous AlCl3 attempt
My setup will be hcl/h2so4 for HCL generation w/ nitrogen or He carrier gas. If will also use the c ... |
2-9-2010 at 06:10
by: greenimp |
Anhydrous AlCl3 attempt
I have built the set up last night waiting for the weekend to run. Using 1/2 inch stainless, the tu ... |
1-9-2010 at 11:12
by: greenimp |
Anhydrous AlCl3 attempt
jacketing the tube as it leaves the BBQ and pumping warm air or hot motor oil through the jacket cou ... |
30-8-2010 at 15:23
by: greenimp |
Anhydrous AlCl3 attempt
i always like the HCL into H2SO4 w/good stirring for gas generation. Something about liquid-liquid ... |
30-8-2010 at 09:50
by: greenimp |
Anhydrous AlCl3 attempt
Yes, so things to do. Design rock solid gas generator. It must have stirring and probably two reacti ... |
30-8-2010 at 06:25
by: greenimp |
Anhydrous AlCl3 attempt
Very nice. I should have tried this method, but got so fed up with the DCM method I moved on to othe ... |
29-8-2010 at 09:57
by: greenimp |
Need Waters HPLC software
Hi, I have a waters PCI Bus/Lace card, and older version of millenium 32. We need to reinstall the ... |
26-9-2009 at 15:05
by: greenimp |
Easy anhydrous AlCl3 production
No I don't think it is anhydrous yet, I think all I did was remove some more un-complexed DMSO that ... |
23-7-2009 at 20:46
by: greenimp |
Easy anhydrous AlCl3 production
Well gave this a try today.
7g AlCl3-6H20 was dissolved in 50 ml 95% EtOH. To this was added sl ... |
23-7-2009 at 19:52
by: greenimp |
Any Polymer-Protein Hybrids?
check out poly-gamma-glutamic acid. It gamma linked glutamic acid residues. Made from bacillus sp. ... |
23-7-2009 at 11:44
by: greenimp |
Easy anhydrous AlCl3 production
Good point. I encountered that with my previous experiments. Actually, you might be able to use the ... |
21-7-2009 at 19:26
by: greenimp |
Easy anhydrous AlCl3 production
My local health food store stocks the 250ml and 500ml bottles of 99% DMSO. I asked the manager if t ... |
21-7-2009 at 16:30
by: greenimp |
Easy anhydrous AlCl3 production
To be true it was not me that found the patent. It was bought to my attention by another.
I have ... |
21-7-2009 at 12:04
by: greenimp |
Easy anhydrous AlCl3 production
I wanted to post something I have been thinking about recently. I have spent alot of tie trying t ... |
21-7-2009 at 11:13
by: greenimp |
Leuckart reaction
TD- On your accelerated Leuckart. I wanted to gauge the feeling here if it was only the concentratio ... |
17-7-2009 at 07:11
by: greenimp |
Is there an error in this porcess? I think so..
oh shit.  
Its this one: Cl2 + 2 NaOH -> NaClO + NaCl + H20
That's what I get for no ... |
20-5-2009 at 12:38
by: greenimp |
Is there an error in this porcess? I think so..
3 Cl2 + 6 NaOH → 5 NaCl + NaClO3 + 3H2O
I thought this was the formula for Sodium hypoc ... |
20-5-2009 at 12:21
by: greenimp |
Is there an error in this porcess? I think so..
From Organic Syntheses [url=http://www.orgsyn.org/orgsyn/prep.asp?prep=cv2p0044]link[/url]
The pa ... |
20-5-2009 at 10:10
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
Well, I was trying out a new method for converting eugenol to 4AC. Needless to say it wasn't workin ... |
5-5-2009 at 06:54
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
I wanted to try to bring this thread to a happy ending. After a lot of work and trouble shooting, t ... |
1-5-2009 at 21:20
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
Well she proved me wrong. Here is a paper documenting the actual methylenation of 4-ally-C. It ca ... |
13-2-2009 at 19:55
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
[quote][i]Originally posted by Nicodem[/i]
That your putative 4-allylcatechol is a liquid is not ... |
10-2-2009 at 02:55
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
[quote]
I don't get it. Above you describe that the methylenation of your substrate worked and now ... |
9-2-2009 at 08:52
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
Actually, there has been an argument. I keep saying the reaction won't work on 4-ally-C, based on m ... |
9-2-2009 at 02:20
by: greenimp |
Methylenation of catechol derivetives (Base cataylized)
Thanks, I was going to try the nitrogen atmosphere on my next run. I have a argon welding tank that ... |
8-2-2009 at 22:59
by: greenimp |
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