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Problems with wet chemical sodium synthesis
For anyone else trying this reaction, I would not recommend magnesium powder/dust unless you have ve ...
24-5-2020 at 13:42
by: monolithic
Latest chemical order?
[rquote=636733&tid=9890&author=j_sum1]A couple of kg of zinc ordered off ebay which I intend ...
23-5-2020 at 20:47
by: monolithic
Synthesising 1,4 Dioxane
As a follow up to my last post, I tried fractionally distilling the ethylene glycol + H2SO4. This br ...
23-5-2020 at 20:22
by: monolithic
Synthesising 1,4 Dioxane
I filled a 1000 ml round bottom flask, set up for simple distillation, with 350 ml of purified ethyl ...
22-5-2020 at 17:00
by: monolithic
sassafras extraction from roots - anyone have experience or know yeilds?
Seems like a lot of work but I imagine it smells amazing once separated and purified. I have a few t ...
22-5-2020 at 15:22
by: monolithic
Latest chemical order?
I just bought 64 oz of Liquid Lightning at WalMart. https://www.walmart.com/ip/Liquid-Lightning-Virg ...
22-5-2020 at 10:03
by: monolithic
Looking for Sudan III (Sudan Red) or substitutes...
[rquote=635567&tid=155341&author=nimgoldman]I am looking for Sudan III dye to use it as indi ...
22-5-2020 at 04:26
by: monolithic
Newe YouTube Video: Methyl Iodide Synthesis with Aluminum Foil
Nice video. If you have the time, I'm sure many of us would also appreciate a video on just your des ...
21-5-2020 at 04:43
by: monolithic
Advice on buying a GC/MS
I've always wanted to buy HPLC or GC/MS but the learning curve seems absurdly steep. So much to go w ...
20-5-2020 at 07:31
by: monolithic
Problems with wet chemical sodium synthesis
[rquote=636370&tid=155408&author=G-Coupled]Can the dirty Magnesium shavings/turnings not be ...
18-5-2020 at 16:44
by: monolithic
Problems with wet chemical sodium synthesis
In the USA you can buy small quantities of relatively pure magnesium turning/powders on eBay. Maybe ...
18-5-2020 at 04:33
by: monolithic
Problems with wet chemical sodium synthesis
I haven't performed this reaction yet (but I want to!) so take this with a grain of salt, but I thin ...
17-5-2020 at 05:23
by: monolithic
Device that heats at around 40 degrees C?
https://www.briskheat.com/products/heaters/heating-tapes-and-cords.html

You can get knockoff vers ...
17-5-2020 at 05:20
by: monolithic
Mercury cleanup suggestions.
Pipettes or even eye droppers are good for picking up small globules of mercury.
16-5-2020 at 05:11
by: monolithic
Chest freezer cold trap?
Check this out, it might be more in line with what you're trying to do and it's essentially how labo ...
7-5-2020 at 12:10
by: monolithic
Melgar has died
Sad to hear. :(
7-5-2020 at 04:35
by: monolithic
EtOEt leaking out of reagent bottle?
You can buy peroxide test strips on Amazon if you're concerned about peroxides, or you could could d ...
7-5-2020 at 03:53
by: monolithic
Vacuum pump for vacuum distillation.
[rquote=635262&tid=155264&author=mackolol]Ok. Since I have diaphragm pump I won't rather be ...
3-5-2020 at 16:39
by: monolithic
diffusion pump oil diy alternative?
Generic vacuum pump oil. I don't know if it would work, though. Your main concern is vapor pressure. ...
30-4-2020 at 08:37
by: monolithic
Mel-Temp 3.0 - how long do elements last?
Glad to hear the elements don't commonly burn out. I think I have some capillaries sitting around in ...
29-4-2020 at 09:52
by: monolithic
Vacuum pump for vacuum distillation.
[rquote=634970&tid=155264&author=earpain][rquote=634890&tid=155264&author=rockyit98] ...
29-4-2020 at 03:58
by: monolithic
Mel-Temp 3.0 - how long do elements last?
How long do the elements typically last in these machines (or melting apparatuses in general) and ho ...
28-4-2020 at 12:25
by: monolithic
Sources of chemicals ?
[rquote=634885&tid=78963&author=draculic acid69]Alibaba.those Chinese companies actually wan ...
27-4-2020 at 08:18
by: monolithic
Setting up a home Schlenk system
Stirling cryocooler can make liquid air quite easily, if you can find a used one at auction. Check Y ...
25-4-2020 at 14:15
by: monolithic
Got my own NMR
That's incredible. Nice find.
23-4-2020 at 17:38
by: monolithic
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