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Nitric Acid Synthesis
Yesterday after completing one distillation I noticed a color change in my pumps oil.

Heres wha ...
27-5-2008 at 13:12
by: mr.pyro
Nitric Acid Synthesis
[quote][i]Originally posted by ADP[/i]
[quote][i]Originally posted by crazyboy[/i]
looks like ADP ...
26-5-2008 at 12:29
by: mr.pyro
Nitric Acid Synthesis
Here is my setup.

200g of nh4no3 was added to 300ml bullzeye drain cleaner sulfuric acid.

Tem ...
26-5-2008 at 11:25
by: mr.pyro
cleaning sulfuric acid
Liquid Fire is good stuff. That should work well for you. It has always worked well for me for nitr ...
24-5-2008 at 21:57
by: mr.pyro
Nitric Acid Synthesis
I have all 19/22 glassware because I bought it as a kit. I hope to upgrade to 24/40 soon however. ...
21-5-2008 at 22:30
by: mr.pyro
Nitric Acid Synthesis
I tried a vac distillation today and ended up sucking out most of my vapors before they condensed. ...
21-5-2008 at 19:20
by: mr.pyro
Nitric Acid Synthesis
excellent post ADP Ive been looking for something like this with pictures. approx what vaccum do yo ...
19-5-2008 at 19:38
by: mr.pyro
Vacuum Nitric Distillation
Is it possible for the vacuum to be to strong, and thus suck out the nitric acid fumes?

The las ...
26-4-2008 at 20:31
by: mr.pyro
determining concentrations from Ka and pH
Yea. Chem dept says .21 is the right one. looks good nerro
8-10-2006 at 17:36
by: mr.pyro
determining concentrations from Ka and pH
Thanks rogue, that helped.
8-10-2006 at 11:12
by: mr.pyro
determining concentrations from Ka and pH
I have this question that I'm really stuck on:
A chemist wanted to determine the concentration of a ...
7-10-2006 at 15:18
by: mr.pyro
Equilbrium reaction help please
Ive been stuck on this and cant find it anywhere in the textbook?

Can anyone offer some help? th ...
25-9-2006 at 13:41
by: mr.pyro
MSE Help Please(Bond Energies)
Ok I understand these concepts just the wording of the question and the maths is what gets me. Mabye ...
4-9-2006 at 16:01
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Well I am not using any iceblocks, but I wrote up a little synthesis, and added some pics.
56k warn ...
4-1-2005 at 18:37
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Let me say, I have just tried the same procedure, with the phorone reaction covered.
I am slowl ...
4-1-2005 at 17:36
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Hideki,
To get these huge yields, your just using Rserts Synthesis, but just very cold and slow H ...
3-1-2005 at 22:27
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Slightly Incorrect Info in this hobby will get you killed. Doesn't matter that its just some m ...
2-1-2005 at 00:08
by: mr.pyro
Diphoronepentaperoxide (DPPP)
I just tried the written synthesis by Rsert. The oily substace appeared after heating for 2 hours a ...
1-1-2005 at 13:04
by: mr.pyro
Diphoronepentaperoxide (DPPP)
I tried today boiling 200mL Acetone + 300 mL HCl at 100 C. After about 15 min it was vaporing off a ...
28-12-2004 at 15:32
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Well good, I was heating that red wine batch at 60 C for about 1 hour, I think it needs more heat? ...
28-12-2004 at 00:40
by: mr.pyro
Diphoronepentaperoxide (DPPP)
Pyro z,

How many ml of reagent do you have there in that jar, it seems you have a fairly large ye ...
28-12-2004 at 00:00
by: mr.pyro

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