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Dichromate overoxidation
Oooo don't give me any more ideas! There's already too much on the list :P
24-4-2021 at 16:10
by: mr_bovinejony
Dichromate overoxidation
@carl I do have that paper downloaded like 3 times on my phone, ill have to dig for it. The only rea ...
24-4-2021 at 10:58
by: mr_bovinejony
Dichromate overoxidation
Are there any more mild oxidizing agents other than IBX/DMP/TEMPO that might work for it then? Maybe ...
24-4-2021 at 07:23
by: mr_bovinejony
Dichromate overoxidation
I was thinking of using IBX but I have very little and it took a while to make. Might not have a cho ...
23-4-2021 at 08:34
by: mr_bovinejony
Dichromate overoxidation
Nile red has a video on making propionaldehyde but uses some heated condenser water which adds more ...
23-4-2021 at 08:17
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
Did some more testing, It looks like anhydrous ipa can be used as an alternative to acetone. But due ...
20-4-2021 at 18:45
by: mr_bovinejony
Large scale anthranilic acid prep
My inability to do reactions under a 3 gram scale has been my downfall. But when it works its the gr ...
19-4-2021 at 15:32
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I am very happy to report a kind of pure tryptamine product from the benzoate salt. My thiele tube t ...
19-4-2021 at 10:54
by: mr_bovinejony
Large scale anthranilic acid prep
@oxide I just don't like the reaction, titration of store bought bleach is a pain and temperature co ...
18-4-2021 at 17:45
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
Here is the post washed and filtered paste

https://imgur.com/iP4piBT

And here is some of the p ...
18-4-2021 at 09:50
by: mr_bovinejony
Large scale anthranilic acid prep
The hoffman reaction is bullshit for any chemical lol. I weighed all this yesterday and it was 210 g ...
18-4-2021 at 08:31
by: mr_bovinejony
Large scale anthranilic acid prep
I definitely think so, even with the brown discoloration it had a very sharp melting point.
18-4-2021 at 07:23
by: mr_bovinejony
Large scale anthranilic acid prep
From what I've seen, the hoffman route usually gives a brown product. When I was filtering this prod ...
18-4-2021 at 04:35
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I did this procedure. Heres how it went

20 grams of tryptophan mixed with 150 mls of turpentine a ...
17-4-2021 at 18:40
by: mr_bovinejony
Large scale anthranilic acid prep
Eh that's what happens when its left out in the open for 3 weeks!
17-4-2021 at 14:44
by: mr_bovinejony
Large scale anthranilic acid prep
https://imgur.com/ujQ4mhy

https://imgur.com/tnqXB1u

https://imgur.com/p92ZDLC

Here are some ...
17-4-2021 at 10:58
by: mr_bovinejony
Activating metals post-addition
Hcl won't do anything to the reaction. I reduced benzlin with tin and hcl and it worked just fine
16-4-2021 at 17:15
by: mr_bovinejony
Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
I tried starting from vanillin as well, I gave up after the 3rd attempt. Syringaldehyde is cheap and ...
12-4-2021 at 22:27
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
I'm curious if you plan on using this benzoate salt in some other reactions with tryptamine, or if y ...
8-4-2021 at 02:50
by: mr_bovinejony
Improved Purification Procedure Decarboxylation of L-tryptophan to Tryptamine with Benzoate salt
Thanks for this. I've had minimum luck with trying to isolate fumarate and oxalate salts of tryptami ...
3-4-2021 at 11:30
by: mr_bovinejony
Oxalyl Chloride Challenge
Is there a way from oxalyl bromide to oxalyl chloride? Or is it only possible from chloride to bromi ...
29-3-2021 at 19:07
by: mr_bovinejony
Large scale anthranilic acid prep
I recently did a run of 150 grams of the grape stuff, ill have more product than I'll ever need now. ...
26-3-2021 at 08:59
by: mr_bovinejony
Phencyclidine
Yay another good writeup! Recently I've tried making 3-meo-pyrrolidine? Or however it's called. It w ...
24-3-2021 at 18:00
by: mr_bovinejony
Making a lab stand/rack setup - what is a good design?
I made mine with threaded 1/4 inch rods that are drilled into plywood and held from top and bottom b ...
2-3-2021 at 17:25
by: mr_bovinejony
First mononitrotoluene synthesis - Having some problems (I think?)
Does the quality of water really matter so much? I got sick of buying gallons of distilled water so ...
1-3-2021 at 19:49
by: mr_bovinejony
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