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The Short Questions Thread (4)
Awesome, though not a fan of the 50 hour reflux mentioned in the paper when they reduce o-chlorobenz ...
27-4-2024 at 02:42
by: mr_bovinejony
The Short Questions Thread (4)
Very cool, now just gotta find some hydantion or hippuric acid
26-4-2024 at 14:05
by: mr_bovinejony
The Short Questions Thread (4)
Will clemmensen reduce 3 bromo benzaldehyde to 3 bromo toluene or will it remove the bromine?
25-4-2024 at 18:05
by: mr_bovinejony
small companies disappearing
Yes he also mentioned to me about selling his entire stock but never mentioned leaving the business ...
3-4-2024 at 12:22
by: mr_bovinejony
Stainless Steel Reaction Vessels
Recently I found a stainless steel pepper grinder that last 1 run at 900c with some ferrocyanide usi ...
20-3-2024 at 18:58
by: mr_bovinejony
small companies disappearing
Lab alley doesn't sell most of their stuff to individuals unfortunately
20-3-2024 at 05:42
by: mr_bovinejony
small companies disappearing
Yeah I was talking to the owner of labdirect after he got raided and was able to buy products until ...
19-3-2024 at 12:31
by: mr_bovinejony
small companies disappearing
Does anyone know what has happened to LabDIRECT and Synthetika chemicals? These are the last 2 compa ...
19-3-2024 at 09:28
by: mr_bovinejony
The Short Questions Thread (4)
Nope but I do love that book lol. Theres another shortter one called the recent advances in phosgene ...
18-3-2024 at 16:42
by: mr_bovinejony
The Short Questions Thread (4)
Nope but I do love that book lol. Theres another shortter one called the recent advances in phosgene ...
18-3-2024 at 16:41
by: mr_bovinejony
The Short Questions Thread (4)
No, not confusing the two. It also mentioned stopping the reaction was as easy as removing the heat ...
18-3-2024 at 14:31
by: mr_bovinejony
The Short Questions Thread (4)
This is probably a bit of a stretch but I vaguely remember a procedure with triphosgene that says it ...
16-3-2024 at 05:32
by: mr_bovinejony
The Short Questions Thread (4)
https://patents.google.com/patent/US1641005A/en

Why in this patent is mentioned a molar equivalen ...
6-3-2024 at 09:31
by: mr_bovinejony
Fume Hood Construction
For a constant flow bypass is it important to install some kind of metal sheet with a grill? I've re ...
26-2-2024 at 11:38
by: mr_bovinejony
How hazardous is fluorine chemistry?
[rquote=691069&tid=160167&author=teodor]NH4BF4 is quite volatile. I kept it in an open conta ...
25-2-2024 at 06:12
by: mr_bovinejony
2-methoxynaphthalene = 2-naphthol methyl ether = Nerolin I = yara yara
Doesn't look like you're doing this in a hood unless it's just not shown in your pictures, how'd you ...
23-2-2024 at 21:24
by: mr_bovinejony
High yielding and cheap method for the production of Potassium Cyanide
This method works great except for getting it out of the crucible. Would Borax help this problem or ...
17-2-2024 at 19:21
by: mr_bovinejony
Preparation of Hydrogen Cyanide
I have prepared hcn the same way but have not managed to find a solution to the gel is forms when di ...
14-2-2024 at 21:03
by: mr_bovinejony
thermoelectric cooling bath
Well I already have the peltiers laying around and only need to build the rest, but before I waste t ...
6-7-2021 at 05:17
by: mr_bovinejony
thermoelectric cooling bath
I have some of those blue ice things, they melt too quick and recently the ambient temp in my lab ha ...
5-7-2021 at 00:29
by: mr_bovinejony
thermoelectric cooling bath
Clamping with what? Maybe some cheap wood clamps on all 4 corners?
4-7-2021 at 19:16
by: mr_bovinejony
thermoelectric cooling bath
Oh hell yeah those would be perfect! In the video he used silicon around the TECs which seems like a ...
4-7-2021 at 17:57
by: mr_bovinejony
thermoelectric cooling bath
Very interesting! I was thinking to use a small tupperware that holds the water for the heat sinks, ...
4-7-2021 at 16:57
by: mr_bovinejony
thermoelectric cooling bath
https://youtu.be/0xY06PT5JDE

This video shows some peltier device that cools on one side and heat ...
4-7-2021 at 11:05
by: mr_bovinejony
Vilsmeier reagent/POCl3 formation
This method also works no problem with 1,4 dimethoxybenzene. And the product is even more pure based ...
19-6-2021 at 16:22
by: mr_bovinejony
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