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Vanillin chemistry: 3,4,5-trimethoxyphenethylamine
You might want to consider Proline/CuI in DMSO or DMF for this kind of reaction. I don't have the re ...
14-4-2021 at 13:00
by: myr
1-pentylnaphthalene theory
I've had those kinds of professors before, and they are The Worst. It's an ego thing half the time: ...
13-3-2021 at 07:15
by: myr
Most expensive mistakes you've made?
I screwed up an 8k scholarship form and couldn't get the money back in high school. I also messed up ...
11-3-2021 at 18:22
by: myr
1-pentylnaphthalene theory
My hunch is a radical halogenation can do so selectively. Maybe a photoredox bromination with NBS, s ...
10-3-2021 at 06:49
by: myr
FC Alkylation
I browsed through a reference of mine [Perfume And Flavor Chemicals: (Aroma Chemicals), 2 vol. set] ...
7-3-2021 at 13:28
by: myr
FC Alkylation
Anything that makes a carbocation in those conditions, so benzylic alcohols and alkene side-chains w ...
7-3-2021 at 11:34
by: myr
Vanillin chemistry: Piperonal
[rquote=655958&tid=157077&author=AvBaeyer]DraconicAcid,

If you have nickel chloride and z ...
6-3-2021 at 20:13
by: myr
Gamma Amino Butanal from GABA
The sodium would react with the amine to make the amide salt: you would need to protect it first if ...
2-1-2021 at 13:23
by: myr
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638530&tid=155586&author=Boffis]@michaljemco; Thankyou for posting details of your p ...
17-6-2020 at 04:05
by: myr
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638465&tid=155586&author=michalJenco][rquote=638441&tid=155586&author=Boffis ...
16-6-2020 at 12:05
by: myr
bis(chloromethyl)ether from hexamine hydrolysis?
I wouldn't worry, as BCME is toxic due to it's reactivity, so it will react with the amine species i ...
18-5-2020 at 12:54
by: myr
2,4-dihydroxybenzoic acid from resorcinol
Nice reaction! Never heard of it, but worth trying.
Here's a rather old lit. review:
Lindsey, A. ...
15-5-2020 at 14:36
by: myr
Recrystallization solvent for a-methyl dehydrozingerone
Hello,

Recently I prepared a-methyldehydrozingerone in pretty OK yield using putative metaboric a ...
3-5-2020 at 05:16
by: myr
Vanillin ring closure
[rquote=630429&tid=154810&author=njl]I'd like to preface this by saying my question definite ...
3-2-2020 at 11:42
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
The attachment is broken, looks like. Attempt 2.

http://www.filedropper.com/academiedesbpt6k4802 ...
24-12-2019 at 08:48
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
Hello,

After considerable effort I was able to find the following paper (attached below) which de ...
24-12-2019 at 08:45
by: myr
Aspartic Acid Degredation Failure
The reaction did work at first, transient orange color and lots of gas emitted.

Has anyone tried ...
28-11-2019 at 11:17
by: myr
Aspartic Acid Degredation Failure
The following procedure, from the paper 'Biobased synthesis of acrylonitrile from glutamic acid' was ...
28-11-2019 at 11:15
by: myr
Where to get cheap TLC plates?
Hello,

I was looking to buy TLC plates- but all the ones I found were surprisingly expensive, man ...
19-10-2019 at 04:52
by: myr
Sodium Borohydride Group Buy
I would be interested
21-9-2019 at 07:31
by: myr
Help with the workup of 4-methoxyanisole
Hello,

Recently I attempted to prepare the dimethyl ether of hydroquinone, or 1-4 dimethoxybenzen ...
19-6-2019 at 09:09
by: myr
Notre Dame Smoke
The enormity of the tragedy cannot possibly be overstated, and I am only thankful that (to the best ...
15-4-2019 at 18:54
by: myr
3,4,5-trimethoxyphenylacetonitrile hydrogenation problems
Tetrabutylammonium borohydride will work (but doing so is 100% illegal.)
25-1-2019 at 06:55
by: myr
Ideas for Cold Weather Chemistry, Unlimited Chilling is Free in Winter take advantage of it
Trimethylsulfonium bromide!
5-1-2019 at 14:04
by: myr
NaH2PO2 from China on Ebay?
I have now hidden my email address (why it was shown in the first place is beyond me) and your point ...
24-12-2018 at 10:50
by: myr
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