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Fischer indole synthesis I am trying to carry out a Fischer indole synthesis to make skatole. I plan to use phenylhydrazine a ...	22-7-2015 at 17:59 by: nb198
Showing how to make illegal chemicals? I wanted to reduce phenylephrine using red P and HI. I found a paper that did it with good success. ...	15-11-2014 at 07:42 by: nb198
Showing how to make illegal chemicals? [rquote=361402&tid=43190&author=Etaoin Shrdlu]This is not illegal. If you're genuinely clean ...	4-11-2014 at 18:25 by: nb198
Showing how to make illegal chemicals? I am under the impression that it isn't illegal but it wouldn't be worth the consequences. I believe ...	4-11-2014 at 14:58 by: nb198
Showing how to make illegal chemicals? Hello, I have a Youtube channel where I like to show some chemistry stuff. For one video, I wante ...	4-11-2014 at 06:46 by: nb198
Hydriodic acid synthesis video (Question) I have made a video showing how to make hydriodic acid using the method outlined by Argox in the Ero ...	7-7-2014 at 17:18 by: nb198
Butyric Acid - Synthesis/Extraction [rquote=336202&tid=6401&author=Magpie]Very nice work, showing good technique and excellent p ...	2-7-2014 at 05:59 by: nb198
Butyric Acid - Synthesis/Extraction [rquote=336179&tid=6401&author=blogfast25]Nice work, nb198! Good video too. Even yield wasn' ...	2-7-2014 at 05:56 by: nb198
Butyric Acid - Synthesis/Extraction I tried the synthesis using KMno4 and it worked! I made a video on it: https://www.youtube.com/wa ...	28-6-2014 at 02:48 by: nb198
How to do KMno4 oxidation workup? Well, I decided to use sodium thiosulfate to neutralize the KMno4. It worked great and cleared every ...	23-5-2014 at 06:35 by: nb198
How to do KMno4 oxidation workup? [rquote=331622&tid=30402&author=blogfast25]Assuming you're in alkaline conditions, hydrogen ...	18-5-2014 at 08:20 by: nb198
How to do KMno4 oxidation workup? I am oxidizing 1-butanol to butyric acid using KMno4. My reaction seemed to work but I have excess k ...	17-5-2014 at 18:21 by: nb198
Ester hydrolysis of ASA to salicylic acid. Recrystalization resulted in a 10% loss and a new M.P. of 157-159C. It was not worth the time at all ...	15-4-2014 at 19:53 by: nb198
Converting amino acid salts to freebase amino acids? [rquote=327863&tid=30121&author=AvBaeyer]Typically, amino acid salts are "freebased" using i ...	15-4-2014 at 19:46 by: nb198
Needed way more HCl to neutralize CaCO3 than calculated [rquote=327851&tid=30134&author=HgDinis25]What was the density for? Hydrochloric Acid is a S ...	15-4-2014 at 16:37 by: nb198
Needed way more HCl to neutralize CaCO3 than calculated [rquote=327851&tid=30134&author=HgDinis25]What was the density for? Hydrochloric Acid is a S ...	15-4-2014 at 16:37 by: nb198
Needed way more HCl to neutralize CaCO3 than calculated Nevermind! Please delete this. I made a horribly embarrassing calculation error. That was all. [E ...	15-4-2014 at 16:28 by: nb198
Converting amino acid salts to freebase amino acids? [rquote=327712&tid=30121&author=DraconicAcid]http://pac.iupac.org/publications/pac/pdf/1997/ ...	15-4-2014 at 04:59 by: nb198
Converting amino acid salts to freebase amino acids? [rquote=327699&tid=30121&author=DraconicAcid]Sodium bicarbonate should do the trick, but you ...	14-4-2014 at 19:12 by: nb198
Converting amino acid salts to freebase amino acids? I would like to convert lysine HCl into freebase lysine. What is the best method to do this? I wa ...	14-4-2014 at 18:13 by: nb198
Ester hydrolysis of ASA to salicylic acid. [rquote=327081&tid=30004&author=HeYBrO][rquote=326946&tid=30004&author=nb198] I thi ...	11-4-2014 at 17:21 by: nb198
Ester hydrolysis of ASA to salicylic acid. [rquote=326928&tid=30004&author=HeYBrO]If you want more work go for it. Just as loss of wate ...	11-4-2014 at 04:59 by: nb198
Ester hydrolysis of ASA to salicylic acid. I went ahead with 325mL of 6M NaOH. I am refluxing it for 1h. [Edited on 10-4-2014 by nb198]	10-4-2014 at 07:36 by: nb198
Ester hydrolysis of ASA to salicylic acid. [rquote=326770&tid=30004&author=HeYBrO]Don't bother with the NaOH just use HCl to directly y ...	10-4-2014 at 06:23 by: nb198
Ester hydrolysis of ASA to salicylic acid. [rquote=326795&tid=30004&author=hyfalcon]ASA is definitely less soluble in acetone then it i ...	10-4-2014 at 06:22 by: nb198
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