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Everyday Chemistry
I didn't have another clean ground glass Erlenmeyer on hand, so a lot of vapor leaked out. My area h ...
19-2-2018 at 17:30
by: ninhydric1
Everyday Chemistry
Distilling diethyl ether from starting fluid. Not a fan of the odor of diethyl ether. Smells a bit l ...
19-2-2018 at 14:27
by: ninhydric1
Remotely monitored distillations using a Pi
It would be handy if we could set this up so that when the distillation reaches a certain temperatur ...
16-2-2018 at 16:50
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
Nope, your sodium carbonate and carbon reaction was never thermodynamically favorable.

G=H-TS (wi ...
16-2-2018 at 10:25
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
BaSO4 (s) <--> Ba2+(aq) + (SO4)2-(aq)

Ba2+(aq) + (CO3)2- (aq) --> BaCO3 (s)

If BaSO4 ...
16-2-2018 at 08:01
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
RawWork, I don't think you understand what OP is trying to do. OP wants to convert BaSO4 to other sa ...
15-2-2018 at 21:12
by: ninhydric1
The Short Questions Thread (4)
Thanks, JJay. I should use a fake email for this, good idea.
15-2-2018 at 16:47
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
I would go with the carbon reduction method, simply because you wouldn't introduce cationic contamin ...
15-2-2018 at 07:52
by: ninhydric1
Questions regarding NaHSO3 synthesis
There is a brand of stump remover that isn't KNO3 but sodium metabisulfite, and I feel like sodium m ...
14-2-2018 at 15:33
by: ninhydric1
Do you think it is immoral to steal chemicals and equipment?
[rquote=507308&tid=80462&author=Melgar]In high school once, there was potassium nitrate solu ...
13-2-2018 at 18:51
by: ninhydric1
triphosgene
1 L of DMC for $30 on Amazon:
https://www.amazon.com/MG-Chemicals-Dimethyl-Carbonate-Metal/dp/B06XS ...
8-2-2018 at 18:40
by: ninhydric1
Carbamazepine Synthesis
There is a phosgene-less synthesis I found that uses MeOH and CO2 with KOMe as a catalyst in the pre ...
7-2-2018 at 22:09
by: ninhydric1
Found some Fisher Chems locally - how are these prices?
I feel like these are overkill for a home lab. Unless you have a GC/MS (some people do), these are w ...
7-2-2018 at 17:39
by: ninhydric1
Are you procedural or model driven?
[rquote=506440&tid=80295&author=aga]Which one is alcohol and which one is money ?[/rquote]
...
7-2-2018 at 17:36
by: ninhydric1
Please replace your passwords-
[rquote=506488&tid=80372&author=j_sum1]qwertyuiop[ is your new friend if you want a truly ra ...
7-2-2018 at 17:34
by: ninhydric1
Carbamazepine Synthesis
This is supposed to be in Beginnings.

https://commons.wikimedia.org/wiki/File:Carbamazepine_syn.p ...
7-2-2018 at 17:28
by: ninhydric1
Are you procedural or model driven?
The feel like I am both; I use a procedure as the foundation of my experimentation, then build my ow ...
7-2-2018 at 11:34
by: ninhydric1
Dealing with NO2 fume residues in vessels.
Cody's Lab has tried that in one of his silver metal refining videos, but the problem is silver cata ...
7-2-2018 at 08:46
by: ninhydric1
Please replace your passwords-
Mine takes 4 thousand years to crack, so it should be relatively safe.
6-2-2018 at 08:48
by: ninhydric1
Nitric Acid from Sodium Bisulfite and nitrates
Chances are you'll just have a solution of both.

Even if your reaction did work, the HNO3 would ...
6-2-2018 at 07:47
by: ninhydric1
Nitric Acid from Sodium Bisulfite and nitrates
HSO3- isn't a strong enough acid to produce HNO3, so I doubt it will work. A weak acid can't produce ...
6-2-2018 at 07:33
by: ninhydric1
The Short Questions Thread (4)
I don't have access to the MSDS for Theochem Sulfuric Acid Drain Opener; it requires me to get an ac ...
5-2-2018 at 19:21
by: ninhydric1
making oleum through contact process
http://www.sciencemadness.org/talk/viewthread.php?tid=13313

Please UTFSE.
5-2-2018 at 09:33
by: ninhydric1
Doable synthesis of F2 in amateur setting?
He probably meant PTFE. woelen is about to do something I wouldn't do in my life (maybe if someone i ...
3-2-2018 at 19:18
by: ninhydric1
Interesting read about extreme and exotic chemistry from a home chemist point of view
Coincidentally, that website is written by former, banned SciMad member Anders Hoveland. If you were ...
3-2-2018 at 18:40
by: ninhydric1
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